GB1325379A - 2-carbamyl-4,5,6,7-tetrahydro-1,3-diazepines and their manufacture - Google Patents
2-carbamyl-4,5,6,7-tetrahydro-1,3-diazepines and their manufactureInfo
- Publication number
- GB1325379A GB1325379A GB6014070A GB6014070A GB1325379A GB 1325379 A GB1325379 A GB 1325379A GB 6014070 A GB6014070 A GB 6014070A GB 6014070 A GB6014070 A GB 6014070A GB 1325379 A GB1325379 A GB 1325379A
- Authority
- GB
- United Kingdom
- Prior art keywords
- diazepines
- tetrahydro
- carbamyl
- radicals
- diaminoalkane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D243/00—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms
- C07D243/04—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms having the nitrogen atoms in positions 1 and 3
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
- Plural Heterocyclic Compounds (AREA)
Abstract
1325379 Tetrahydro - 1,3 - diazepines BADISCHE ANILIN- & SODA-FABRIK AG 18 Dec 1970 [19 Dec 1969] 60140/70 Heading C2C Novel 2 - carbamyl - 4,5,6,7 - tetrahydro - 1,3- diazepines of the general formula wherein R<SP>1</SP> and R<SP>3</SP> are hydrogen atoms or (C 1 -C 20 ) alkyl radicals, (C 3 -C 8 ) cycloalkyl radicals, (C 7 -C 12 ) aralkyl radicals, phenyl or naphthyl, R<SP>3</SP> are hydrogen atoms or (C 1 -C 3 ) alkyl radicals, or R 1 and R 2 together with the adjacent nitrogen atom is a 5- or 6-membered heterocyclic ring optionally containing a further nitrogen or oxygen atom, are prepared by reacting a haloacetamide of the formula wherein X is a halogen atom and Y is a hydrogen or halogen atom, with a 1,4-diaminoalkane of the general formula and with elementary sulphur. The reaction is preferably carried out at a temperature of from 50‹ to 180‹ C. in the presence of an inert organic solvent and excess of the diaminoalkane and/or sulphur.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19691963609 DE1963609A1 (en) | 1969-12-19 | 1969-12-19 | Process for the preparation of 2-carbamyl-4,5,6,7-tetrahydro-1,3-diazipins |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1325379A true GB1325379A (en) | 1973-08-01 |
Family
ID=5754317
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB6014070A Expired GB1325379A (en) | 1969-12-19 | 1970-12-18 | 2-carbamyl-4,5,6,7-tetrahydro-1,3-diazepines and their manufacture |
Country Status (5)
Country | Link |
---|---|
CH (1) | CH544099A (en) |
DE (1) | DE1963609A1 (en) |
FR (1) | FR2073995A5 (en) |
GB (1) | GB1325379A (en) |
NL (1) | NL7018437A (en) |
-
1969
- 1969-12-19 DE DE19691963609 patent/DE1963609A1/en active Pending
-
1970
- 1970-11-11 CH CH1667770A patent/CH544099A/en not_active IP Right Cessation
- 1970-12-17 NL NL7018437A patent/NL7018437A/xx unknown
- 1970-12-18 GB GB6014070A patent/GB1325379A/en not_active Expired
- 1970-12-18 FR FR7045761A patent/FR2073995A5/fr not_active Expired
Also Published As
Publication number | Publication date |
---|---|
CH544099A (en) | 1973-11-15 |
DE1963609A1 (en) | 1971-06-24 |
FR2073995A5 (en) | 1971-10-01 |
NL7018437A (en) | 1971-06-22 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PLNP | Patent lapsed through nonpayment of renewal fees |