GB1312830A - Production of pure 1-acetoxy-3-methylbut-2-en-4-al - Google Patents
Production of pure 1-acetoxy-3-methylbut-2-en-4-alInfo
- Publication number
- GB1312830A GB1312830A GB3919770A GB3919770A GB1312830A GB 1312830 A GB1312830 A GB 1312830A GB 3919770 A GB3919770 A GB 3919770A GB 3919770 A GB3919770 A GB 3919770A GB 1312830 A GB1312830 A GB 1312830A
- Authority
- GB
- United Kingdom
- Prior art keywords
- methylbut
- acetoxy
- pure
- aug
- stands
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/28—Preparation of carboxylic acid esters by modifying the hydroxylic moiety of the ester, such modification not being an introduction of an ester group
- C07C67/297—Preparation of carboxylic acid esters by modifying the hydroxylic moiety of the ester, such modification not being an introduction of an ester group by splitting-off hydrogen or functional groups; by hydrogenolysis of functional groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1312830 1 - Acetoxy - 3 - methylbut - 2 - en- 4-al BADISCHE ANILIN- & SODA-FABRIK AG 14 Aug 1970 [16 Aug 1969] 39197/70 Heading C2C Pure 1 - acetoxy - 3 - methylbut - 2 - en - 4 - al of formula CH 3 .CO.OCH 2 CH=C(CH 3 ).CHO is prepared by treating a mixture of 1,2-diacetoxy- 3 - methylbutan - 4 - al and 1,2 - diacetoxypentan-5-al at from 50‹ to 180‹ C. with from 0À001 to 10% of its weight of a salt-like catalyst Q+Y- where Q+ stands for an ammonium or alkali metal cation or the equivalent of an alkaline earth metal cation or a polyvalent anion exchanger and Y- stands for a strongly nucleophilic anion or, if this is polyvalent, the equivalent thereof. Suitable catalysts include sodium acetate, barium hydroxide and a basic ion exchanger containing tertiary ammonium groups.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19691941632 DE1941632C (en) | 1969-08-16 | Process for the pure preparation of 1 acetoxy 3 methylbut 2 en 4 al |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1312830A true GB1312830A (en) | 1973-04-11 |
Family
ID=5742907
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB3919770A Expired GB1312830A (en) | 1969-08-16 | 1970-08-14 | Production of pure 1-acetoxy-3-methylbut-2-en-4-al |
Country Status (5)
Country | Link |
---|---|
BE (1) | BE754869A (en) |
CH (1) | CH526505A (en) |
FR (1) | FR2056861A5 (en) |
GB (1) | GB1312830A (en) |
NL (1) | NL159084B (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5344995A (en) * | 1992-07-14 | 1994-09-06 | Basf Aktiengesellschaft | Preparation of cyclic acetals of 3-formyl-2-butenyltriphenylphosphonium chloride |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2621224A1 (en) * | 1975-05-28 | 1976-12-16 | Hoffmann La Roche | METHOD OF PRODUCING A MOLD COMPOUND |
-
0
- BE BE754869D patent/BE754869A/en not_active IP Right Cessation
-
1970
- 1970-07-31 CH CH1162370A patent/CH526505A/en not_active IP Right Cessation
- 1970-08-11 FR FR7029579A patent/FR2056861A5/fr not_active Expired
- 1970-08-14 NL NL7012058A patent/NL159084B/en not_active IP Right Cessation
- 1970-08-14 GB GB3919770A patent/GB1312830A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5344995A (en) * | 1992-07-14 | 1994-09-06 | Basf Aktiengesellschaft | Preparation of cyclic acetals of 3-formyl-2-butenyltriphenylphosphonium chloride |
Also Published As
Publication number | Publication date |
---|---|
NL7012058A (en) | 1971-02-18 |
BE754869A (en) | 1971-02-15 |
CH526505A (en) | 1972-08-15 |
NL159084B (en) | 1979-01-15 |
DE1941632B1 (en) | 1971-05-19 |
FR2056861A5 (en) | 1971-05-14 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PE20 | Patent expired after termination of 20 years |