GB1280106A - Preparations od polyaddition products of polyepoxides, processes for their manufacture and use - Google Patents

Preparations od polyaddition products of polyepoxides, processes for their manufacture and use

Info

Publication number
GB1280106A
GB1280106A GB21596/70A GB2159670A GB1280106A GB 1280106 A GB1280106 A GB 1280106A GB 21596/70 A GB21596/70 A GB 21596/70A GB 2159670 A GB2159670 A GB 2159670A GB 1280106 A GB1280106 A GB 1280106A
Authority
GB
United Kingdom
Prior art keywords
amine
epoxide
group
amino
iii
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB21596/70A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Novartis AG
Original Assignee
Ciba Geigy AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ciba Geigy AG filed Critical Ciba Geigy AG
Publication of GB1280106A publication Critical patent/GB1280106A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/182—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing using pre-adducts of epoxy compounds with curing agents
    • C08G59/184—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing using pre-adducts of epoxy compounds with curing agents with amines
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
    • C08G59/22—Di-epoxy compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
    • C08G59/32—Epoxy compounds containing three or more epoxy groups
    • C08G59/3218—Carbocyclic compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
    • C08G59/32—Epoxy compounds containing three or more epoxy groups
    • C08G59/38—Epoxy compounds containing three or more epoxy groups together with di-epoxy compounds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/55—Epoxy resins
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/02—Material containing basic nitrogen
    • D06P3/04—Material containing basic nitrogen containing amide groups
    • D06P3/14—Wool
    • D06P3/148—Wool using reactive dyes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Paper (AREA)
  • Epoxy Resins (AREA)
  • Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1280106 Epoxy amine reaction products CIBA-GEIGY AG 5 May 1970 [7 May 1969] 21596/70 Heading C3B [Also in Divisions D1 and D2] Stable reaction products are obtained by reacting (I) a polyglycidyl ether of a polyhydric phenol, which is liquid at room temp., with (II) an aliphatic or cycloaliphatic diprimary amine at 100-120‹ C. in the absence of solvents. From 3-5À5 amine group equivalents of II are used per epoxide group equivalent of I. The resultant product is then reacted at <100‹C., in the presence of a solvent (III) with an epoxy compound (IV) in a ratio of 2-5 amine equivalents per epoxide equivalent of IV. Not later than the completion of reaction, an acid, e.g. acetic acid or formic acid, is added so that the product has a pH of 2-8 on dilution with water. I may be a polyglycidyl ether of bisphenol A having an epoxide content of at least 5 epoxide group equivalents per kg. II may be a cycloaliphatic amine containing a saturated 5- or 6-membered carbocyclic ring, a H 2 N-group bonded to a ring carbon atom and a H 2 NCH 2 group bonded to another ring carbon atom, e.g. 3,3,5-trimethyl-1- amino-3-aminomethylcyclohexane or 1-amino-2- aminomethylcyclopentane. III may be solvent which is completely miscible with water, e.g. the n-butyl mono ether of ethylene glycol. The products are useful in rendering wool non-felting and as sizing agents in paper manufacture.
GB21596/70A 1969-05-07 1970-05-05 Preparations od polyaddition products of polyepoxides, processes for their manufacture and use Expired GB1280106A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CH700969A CH509369A (en) 1969-05-07 1969-05-07 Process for the production of stable preparations of reaction products from epoxies and amines

Publications (1)

Publication Number Publication Date
GB1280106A true GB1280106A (en) 1972-07-05

Family

ID=4318491

Family Applications (1)

Application Number Title Priority Date Filing Date
GB21596/70A Expired GB1280106A (en) 1969-05-07 1970-05-05 Preparations od polyaddition products of polyepoxides, processes for their manufacture and use

Country Status (15)

Country Link
JP (1) JPS504238B1 (en)
AT (1) AT301185B (en)
BE (1) BE750051A (en)
BR (1) BR7018853D0 (en)
CH (1) CH509369A (en)
CS (1) CS155238B2 (en)
DE (1) DE2020917A1 (en)
FR (1) FR2047117A5 (en)
GB (1) GB1280106A (en)
NL (1) NL7006627A (en)
NO (1) NO130906C (en)
PL (1) PL71027B1 (en)
SE (1) SE364056B (en)
SU (1) SU433687A3 (en)
ZA (1) ZA702953B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0758660A2 (en) * 1995-08-14 1997-02-19 Air Products And Chemicals, Inc. Advanced polyamine adduct epoxy resin curing agent for use in two component waterborne coating systems

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3147153A1 (en) * 1981-11-27 1983-06-01 Bayer Ag, 5090 Leverkusen COLORING PROCEDURE

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0758660A2 (en) * 1995-08-14 1997-02-19 Air Products And Chemicals, Inc. Advanced polyamine adduct epoxy resin curing agent for use in two component waterborne coating systems
EP0758660A3 (en) * 1995-08-14 1997-05-28 Air Prod & Chem Advanced polyamine adduct epoxy resin curing agent for use in two component waterborne coating systems

Also Published As

Publication number Publication date
NL7006627A (en) 1970-11-10
BR7018853D0 (en) 1973-01-11
PL71027B1 (en) 1974-04-30
AT301185B (en) 1972-08-25
FR2047117A5 (en) 1971-03-12
NO130906C (en) 1975-03-05
NO130906B (en) 1974-11-25
CH509369A (en) 1971-06-30
DE2020917A1 (en) 1970-11-19
ZA702953B (en) 1971-01-27
SU433687A3 (en) 1974-06-25
CS155238B2 (en) 1974-05-30
SE364056B (en) 1974-02-11
JPS504238B1 (en) 1975-02-17
BE750051A (en) 1970-11-06

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Legal Events

Date Code Title Description
PS Patent sealed
PLNP Patent lapsed through nonpayment of renewal fees