GB1268869A - PROCESS FOR THE PREPARATION OF epsilon-CAPROLACTAM - Google Patents
PROCESS FOR THE PREPARATION OF epsilon-CAPROLACTAMInfo
- Publication number
- GB1268869A GB1268869A GB42902/69A GB4290269A GB1268869A GB 1268869 A GB1268869 A GB 1268869A GB 42902/69 A GB42902/69 A GB 42902/69A GB 4290269 A GB4290269 A GB 4290269A GB 1268869 A GB1268869 A GB 1268869A
- Authority
- GB
- United Kingdom
- Prior art keywords
- caprolactam
- salts
- acidic
- sept
- steam
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 title abstract 8
- 230000002378 acidificating effect Effects 0.000 abstract 2
- 150000003839 salts Chemical class 0.000 abstract 2
- 229910002796 Si–Al Inorganic materials 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 150000008043 acidic salts Chemical class 0.000 abstract 1
- 150000007513 acids Chemical class 0.000 abstract 1
- 229960002684 aminocaproic acid Drugs 0.000 abstract 1
- 150000001639 boron compounds Chemical class 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 235000011007 phosphoric acid Nutrition 0.000 abstract 1
- 150000003016 phosphoric acids Chemical class 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- LLZRNZOLAXHGLL-UHFFFAOYSA-J titanic acid Chemical compound O[Ti](O)(O)O LLZRNZOLAXHGLL-UHFFFAOYSA-J 0.000 abstract 1
- 239000010457 zeolite Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/02—Preparation of lactams
- C07D201/08—Preparation of lactams from carboxylic acids or derivatives thereof, e.g. hydroxy carboxylic acids, lactones or nitriles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Other In-Based Heterocyclic Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP6361168A JPS4631539B1 (https=) | 1968-09-04 | 1968-09-04 | |
| JP7104868 | 1968-09-30 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1268869A true GB1268869A (en) | 1972-03-29 |
Family
ID=26404752
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB42902/69A Expired GB1268869A (en) | 1968-09-04 | 1969-08-28 | PROCESS FOR THE PREPARATION OF epsilon-CAPROLACTAM |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3658810A (https=) |
| CH (1) | CH517749A (https=) |
| DE (1) | DE1944910A1 (https=) |
| FR (1) | FR2017388A1 (https=) |
| GB (1) | GB1268869A (https=) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0133590A1 (en) * | 1983-07-04 | 1985-02-27 | Unilever N.V. | Catalytic preparation of carbonamides |
| EP0271817A1 (de) * | 1986-12-17 | 1988-06-22 | BASF Aktiengesellschaft | Verfahren zur Herstellung von Caprolactam aus 6-Aminocapronsäure, deren Estern und Amiden |
| WO2002050026A1 (en) * | 2000-12-21 | 2002-06-27 | National Institute Of Advanced Industrial Science And Technology | Process for synthesizing lactam |
| WO2002050025A1 (fr) * | 2000-12-21 | 2002-06-27 | National Institute Of Advanced Industrial Science And Technology | Procede de synthese de beta-lactamine |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3403574A1 (de) * | 1984-02-02 | 1985-08-08 | Basf Ag, 6700 Ludwigshafen | Verfahren zur gewinnung von caprolactam aus (epsilon)-aminocapronsaeure |
| DE3735904A1 (de) * | 1987-08-15 | 1989-02-23 | Bayer Ag | Verfahren zur herstellung von n-alkylierten caprolactamen |
| DE4422610A1 (de) * | 1994-06-28 | 1996-01-04 | Basf Ag | Verfahren zur Herstellung von cyclischen Lactamen |
| DE19628805A1 (de) * | 1996-07-17 | 1998-01-22 | Basf Ag | Verfahren zur Herstellung von Caprolactam aus 6-Aminocapronitril |
| DE19648747A1 (de) * | 1996-11-25 | 1998-05-28 | Basf Ag | Verfahren zur Rückgewinnung von Caprolactam und seinen Oligomeren aus wässrigen Polycaprolactam-Extrakten |
| KR100516986B1 (ko) | 1997-02-19 | 2005-09-26 | 코닌클리즈케 디에스엠 엔.브이. | 6-아미노카프론산 유도체를 과열 수증기와 접촉시킴으로써 촉매 없이 카프로락탐을 제조하는 방법 |
| EP0860431A1 (en) * | 1997-02-19 | 1998-08-26 | Dsm N.V. | Process to prepare e-caprolactam |
| EP0882710A1 (en) * | 1997-06-03 | 1998-12-09 | Industrial Technology Research Institute | Method for the preparation of caprolactam and preparation of catalysts for this method |
| FR2780401B1 (fr) * | 1998-06-25 | 2001-02-09 | Rhone Poulenc Fibres | Procede de vaporisation d'aminonitrile |
| EP1028109A1 (en) * | 1999-02-12 | 2000-08-16 | Dsm N.V. | Process for the preparation of epsilon-caprolactam |
| US6331624B1 (en) | 2000-04-05 | 2001-12-18 | E.I. Du Pont De Nemours And Company | Process for preparing 6-aminocaproamide |
| FR2833946B1 (fr) * | 2001-12-21 | 2005-08-05 | Rhodia Polyamide Intermediates | Procede de preparation de lactame |
| TWI537386B (zh) | 2009-12-22 | 2016-06-11 | Ｄｓｍ智慧財產有限公司 | 由發酵法獲得的６－胺己酸製備己內醯胺 |
| IT201800021409A1 (it) | 2018-12-28 | 2020-06-28 | Aquafil S P A | Processo per la produzione di epsilon caprolattame dallacido 6-aminocaproico. |
| WO2021100759A1 (ja) | 2019-11-19 | 2021-05-27 | 東レ株式会社 | ε－カプロラクタムの製造方法 |
-
1969
- 1969-08-28 GB GB42902/69A patent/GB1268869A/en not_active Expired
- 1969-08-29 US US854263A patent/US3658810A/en not_active Expired - Lifetime
- 1969-09-03 CH CH1336669A patent/CH517749A/de not_active IP Right Cessation
- 1969-09-04 FR FR6930213A patent/FR2017388A1/fr not_active Withdrawn
- 1969-09-04 DE DE19691944910 patent/DE1944910A1/de active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0133590A1 (en) * | 1983-07-04 | 1985-02-27 | Unilever N.V. | Catalytic preparation of carbonamides |
| EP0271817A1 (de) * | 1986-12-17 | 1988-06-22 | BASF Aktiengesellschaft | Verfahren zur Herstellung von Caprolactam aus 6-Aminocapronsäure, deren Estern und Amiden |
| WO2002050026A1 (en) * | 2000-12-21 | 2002-06-27 | National Institute Of Advanced Industrial Science And Technology | Process for synthesizing lactam |
| WO2002050025A1 (fr) * | 2000-12-21 | 2002-06-27 | National Institute Of Advanced Industrial Science And Technology | Procede de synthese de beta-lactamine |
| US7022842B2 (en) | 2000-12-21 | 2006-04-04 | National Institute Of Advanced Industrial Science And Technology | Process for synthesizing beta-lactam |
Also Published As
| Publication number | Publication date |
|---|---|
| DE1944910A1 (de) | 1970-04-09 |
| US3658810A (en) | 1972-04-25 |
| CH517749A (de) | 1972-01-15 |
| FR2017388A1 (https=) | 1970-05-22 |
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