GB1266092A - - Google Patents

Info

Publication number
GB1266092A
GB1266092A GB1266092DA GB1266092A GB 1266092 A GB1266092 A GB 1266092A GB 1266092D A GB1266092D A GB 1266092DA GB 1266092 A GB1266092 A GB 1266092A
Authority
GB
United Kingdom
Prior art keywords
formula
firmenich
hexadecane
hydroperoxy
oxabicyclo
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from CH819269A external-priority patent/CH523879A/en
Priority claimed from CH786570A external-priority patent/CH557813A/en
Application filed filed Critical
Publication of GB1266092A publication Critical patent/GB1266092A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D315/00—Heterocyclic compounds containing rings having one oxygen atom as the only ring hetero atom according to more than one of groups C07D303/00 - C07D313/00
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/94—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems condensed with rings other than six-membered or with ring systems containing such rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D313/00—Heterocyclic compounds containing rings of more than six members having one oxygen atom as the only ring hetero atom
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0069—Heterocyclic compounds
    • C11B9/0073—Heterocyclic compounds containing only O or S as heteroatoms
    • C11B9/0084—Heterocyclic compounds containing only O or S as heteroatoms the hetero rings containing more than six atoms

Abstract

1,266,092. Peroxy derivatives of bicyclic ethers. R. FIRMENICH, G. FIRMENICH, R. E. FIRMENICH, and F. -H. FIRMENICH, [trading as FIRMENICH & CIE]. 29 May, 1970 [29 May, 1969; 27 May, 1970], No. 3135/71. Divided out of 1,266,091. Heading C2C. Novel peroxy derivatives of bicyclic ethers having the general formula: in which R<SP>1</SP> is a hydrogen atom, a hydrocarbon radical, an acyl group or a group of the formula: wherein each of R<SP>3</SP> and R<SP>4</SP> is a hydrogen atom or one of them is a hydrogen atom and the other is a methyl group and n is 0, 1, 2 or 3, and R<SP>2</SP> is a group of Formula II, provided that when both R<SP>1</SP> and R<SP>2</SP> are groups of Formula II they are identical, are prepared by reacting a bicyclic ether of the formula with hydrogen peroxide or a hydroperoxide of the formula R<SP>1</SP>OOH. The reaction is suitably carried out in the presence of sulphuric acid at a temperature of from 0‹ to 25‹ C. Novel compounds include 12-hydroperoxy-13-oxabicyclo- (10, 4, 0)-hexadecane, 12-tert-butylperoxy-13- oxabicyclo (10,4,0) hexadecane, di-(13-oxabicyclo-( 10,4,0) hexadoc-12-yl) peroxide, 12-hydroperoxy - 13 - oxa - 14 - methylbicycio - (10,4,0)- hexadecane, 12 - hydroperoxy - 13 - oxa - 15- methylbicyclo - (10,4,0) hexadecane, and 12- hydroperoxy - 13 - oxa - 14 - methylbicyclo- (10,3,0) hexadecane. The compounds are useful as starting materials for the preparation of lactones having 14 to 17 ring carbon atoms.
GB1266092D 1969-05-29 1970-05-29 Expired GB1266092A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH819269A CH523879A (en) 1969-05-29 1969-05-29 Lactones with 14 to 17 ring C-atoms - used in perfumery
CH786570A CH557813A (en) 1970-05-27 1970-05-27 METHOD FOR MANUFACTURING LACTONES.

Publications (1)

Publication Number Publication Date
GB1266092A true GB1266092A (en) 1972-03-08

Family

ID=25702364

Family Applications (2)

Application Number Title Priority Date Filing Date
GB1266092D Expired GB1266092A (en) 1969-05-29 1970-05-29
GB1266091D Expired GB1266091A (en) 1969-05-29 1970-05-29

Family Applications After (1)

Application Number Title Priority Date Filing Date
GB1266091D Expired GB1266091A (en) 1969-05-29 1970-05-29

Country Status (5)

Country Link
JP (1) JPS548677B1 (en)
DE (2) DE2065550C2 (en)
FR (1) FR2043784A1 (en)
GB (2) GB1266092A (en)
NL (1) NL164857C (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4906759A (en) * 1986-09-24 1990-03-06 Lonza Ltd. Process for the production of 4-alkoxy-2(5H) thiophenones
US4997957A (en) * 1985-01-16 1991-03-05 Lonza, Ltd. Process for the production of thiotetronic acid
EP2540712A1 (en) 2011-06-30 2013-01-02 Basf Se Process for the preparation of cyclic enolethers
EP2540713A1 (en) 2011-06-30 2013-01-02 Basf Se Macrocyclic lactones
US8410293B2 (en) 2011-06-30 2013-04-02 Basf Se Process for the preparation of cyclic enol ethers
US8648031B2 (en) 2011-06-30 2014-02-11 Basf Se Macrocyclic lactones

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3224707A1 (en) * 1982-07-02 1984-01-05 Chemische Werke Hüls AG, 4370 Marl METHOD FOR PRODUCING MACROCYCLIC KETOLACTONES
DE69028755T2 (en) * 1989-10-27 1997-06-05 Firmenich & Cie Use of unsaturated macrocyclic ketones and perfume ingredients
EP0503312B1 (en) * 1991-03-13 1997-01-08 Firmenich Sa Procedure for preparation of 15-pentadecanolide or mixtures rich in this macrolide
DE10152992A1 (en) * 2001-10-26 2003-05-08 Haarmann & Reimer Gmbh Mixtures for use as musk fragrance
DE10227483A1 (en) * 2002-06-19 2004-01-08 Symrise Gmbh & Co. Kg Process for the preparation of 11 (12) -pentadecen-15-olides
DE10348168A1 (en) * 2003-10-16 2005-05-12 Symrise Gmbh & Co Kg Process for the preparation of 1-hydroperoxy-16-oxabicyclo [40.4.0] hexadecane
US7569535B2 (en) * 2004-04-30 2009-08-04 Soda Aromatic Co., Ltd. 11-methyl-13-tridecanolide, 12-methyl-14-tetradecanolide and 13-methyl-15-pentadecanolide, perfume compositions containing the same, and process for production of compounds including the same
CN104703975A (en) * 2012-09-14 2015-06-10 西姆莱斯股份公司 Unsaturated lactones as odorants
US9783520B2 (en) 2014-05-16 2017-10-10 P2 Science, Inc. Macrocyclic compounds, polymers, and methods for making same
ES2948107T3 (en) 2014-08-29 2023-08-31 P2 Science Inc Polyethers, polyamines, polythioethers and methods for their manufacture
JP2017122101A (en) * 2017-02-17 2017-07-13 シムライズ アーゲー Unsaturated lactone as fragrant substance
EP3661993A4 (en) 2017-07-31 2021-01-20 P2 Science, Inc. Polyether derivatives, uses, and methods of making the same
MX2022010940A (en) 2020-03-05 2022-10-07 P2 Science Inc Cosmetic compositions comprising polyether polymers.

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4997957A (en) * 1985-01-16 1991-03-05 Lonza, Ltd. Process for the production of thiotetronic acid
US5093503A (en) * 1985-01-16 1992-03-03 Lonza Ltd. Process for the production of thiotetronic acid
US4906759A (en) * 1986-09-24 1990-03-06 Lonza Ltd. Process for the production of 4-alkoxy-2(5H) thiophenones
US4906765A (en) * 1986-09-24 1990-03-06 Lonza Ltd. Process for the production of 4-alkoxy-2(5H) thiophenones
US4931570A (en) * 1986-09-24 1990-06-05 Lonza Ltd. Process for the production of 4-alkoxy-2(5H) thiophenones
EP2540712A1 (en) 2011-06-30 2013-01-02 Basf Se Process for the preparation of cyclic enolethers
EP2540713A1 (en) 2011-06-30 2013-01-02 Basf Se Macrocyclic lactones
WO2013000842A1 (en) 2011-06-30 2013-01-03 Basf Se Macrocyclic lactones
WO2013000846A1 (en) 2011-06-30 2013-01-03 Basf Se Method for producing cyclic enol ethers
US8410293B2 (en) 2011-06-30 2013-04-02 Basf Se Process for the preparation of cyclic enol ethers
US8648031B2 (en) 2011-06-30 2014-02-11 Basf Se Macrocyclic lactones
EP2813496A1 (en) 2011-06-30 2014-12-17 Basf Se Macrocyclic lactones

Also Published As

Publication number Publication date
DE2065550C2 (en) 1982-05-06
GB1266091A (en) 1972-03-08
NL7007855A (en) 1970-12-01
NL164857C (en) 1981-02-16
DE2026056B2 (en) 1975-07-10
DE2026056A1 (en) 1970-12-03
JPS548677B1 (en) 1979-04-17
FR2043784A1 (en) 1971-02-19
DE2065551A1 (en) 1974-06-20
NL164857B (en) 1980-09-15
DE2065551C3 (en) 1980-07-03
DE2065551B2 (en) 1979-10-25
DE2065550A1 (en) 1974-06-20

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Legal Events

Date Code Title Description
PS Patent sealed
PCNP Patent ceased through non-payment of renewal fee