GB1254796A - Improvements in the acetylation of textile articles of cellulose - Google Patents

Improvements in the acetylation of textile articles of cellulose

Info

Publication number
GB1254796A
GB1254796A GB54344/69A GB5434469A GB1254796A GB 1254796 A GB1254796 A GB 1254796A GB 54344/69 A GB54344/69 A GB 54344/69A GB 5434469 A GB5434469 A GB 5434469A GB 1254796 A GB1254796 A GB 1254796A
Authority
GB
United Kingdom
Prior art keywords
textile articles
cellulose
bath
acetic anhydride
acetate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB54344/69A
Inventor
Andre Rajon
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rhodiaceta SA
Original Assignee
Rhodiaceta SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rhodiaceta SA filed Critical Rhodiaceta SA
Publication of GB1254796A publication Critical patent/GB1254796A/en
Expired legal-status Critical Current

Links

Classifications

    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/188Monocarboxylic acids; Anhydrides, halides or salts thereof
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F2/00Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
    • D01F2/24Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from cellulose derivatives
    • D01F2/28Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from cellulose derivatives from organic cellulose esters or ethers, e.g. cellulose acetate

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Artificial Filaments (AREA)

Abstract

1,254,796. Acetylation of cellulose textile articles. SOC. RHODIACETA. 5 Nov., 1969 [6 Nov., 1968], No. 54344/69. Heading C3A. Cellulose acetate textile articles having a combined acetic acid content of 50 to 62-5% are prepared by treating regenerated cellulose textile articles at 100‹ to 135‹ C. in the presence of an alkali metal acetate e.g. potassium acetate, with a bath containing more than 95% by weight of acetic anhydride, maintaining the acetic anhydride content of the bath constantly above 95% by weight by removing impurities formed and introducing fresh acetic anhydride in the course of the process, and keeping the constituent filaments of the textile articles at a substantially constant length throughout the process. The cellulose textile articles may be yarns, tows, woven or knitted fabrics of regenerated cellulose fibres which do not possess a fibrillar structure or have a fibrillar and oriented micro-structure. The textile article may be impregnated with 80-180% of potassium acetate, based on the weight of the cellulose. The process may be carried out continuously by passing the regenerated cellulose textile articles through a bath of an aqueous solution of the alkali metal acetate, drying them, passing them into the acetic anhydride bath while keeping their dimensions substantially constant, removing them from the bath, and freeing them substantially from unreacted acetic anhydride and from alkali metal acetate and acetic acid, whether free or combined as a complex salt.
GB54344/69A 1968-11-06 1969-11-05 Improvements in the acetylation of textile articles of cellulose Expired GB1254796A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR172765 1968-11-06

Publications (1)

Publication Number Publication Date
GB1254796A true GB1254796A (en) 1971-11-24

Family

ID=8656548

Family Applications (1)

Application Number Title Priority Date Filing Date
GB54344/69A Expired GB1254796A (en) 1968-11-06 1969-11-05 Improvements in the acetylation of textile articles of cellulose

Country Status (11)

Country Link
US (1) US3655326A (en)
AT (1) AT297657B (en)
BE (1) BE741322A (en)
BR (1) BR6913866D0 (en)
CH (1) CH1646569D (en)
DE (1) DE1955931A1 (en)
ES (1) ES373233A1 (en)
FR (1) FR1590866A (en)
GB (1) GB1254796A (en)
NL (1) NL6916310A (en)
RO (1) RO55880A (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4322965C1 (en) * 1993-07-09 1994-10-06 Rhodia Ag Rhone Poulenc Filter tow, manufacture thereof, and use thereof as tobacco smoke filter element
WO2020082294A1 (en) * 2018-10-25 2020-04-30 深圳大学 Cellulose ester and preparation method therefor and application thereof
CN109485735A (en) * 2018-10-25 2019-03-19 深圳大学 Cellulose esters and its preparation method and application

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1546211A (en) * 1922-02-01 1925-07-14 American Cellulose & Chemical Manufacture of products containing cellulose
US1930895A (en) * 1930-02-13 1933-10-17 Chem Ind Basel Cellulose esters and process of making same
US2348001A (en) * 1941-10-24 1944-05-02 Nat Vulcanized Fibre Company Acetylation of cellulose
BE595632A (en) * 1959-10-02 1900-01-01
US3037902A (en) * 1960-12-22 1962-06-05 Rayonier Inc Partial acetylation of cellulose

Also Published As

Publication number Publication date
ES373233A1 (en) 1971-12-16
CH1646569D (en)
BE741322A (en) 1970-05-05
NL6916310A (en) 1970-05-11
AT297657B (en) 1972-04-10
FR1590866A (en) 1970-04-20
RO55880A (en) 1973-11-20
BR6913866D0 (en) 1973-01-16
DE1955931A1 (en) 1970-06-11
US3655326A (en) 1972-04-11

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