GB1254796A - Improvements in the acetylation of textile articles of cellulose - Google Patents
Improvements in the acetylation of textile articles of celluloseInfo
- Publication number
- GB1254796A GB1254796A GB54344/69A GB5434469A GB1254796A GB 1254796 A GB1254796 A GB 1254796A GB 54344/69 A GB54344/69 A GB 54344/69A GB 5434469 A GB5434469 A GB 5434469A GB 1254796 A GB1254796 A GB 1254796A
- Authority
- GB
- United Kingdom
- Prior art keywords
- textile articles
- cellulose
- bath
- acetic anhydride
- acetate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
- D01F2/24—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from cellulose derivatives
- D01F2/28—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from cellulose derivatives from organic cellulose esters or ethers, e.g. cellulose acetate
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Artificial Filaments (AREA)
Abstract
1,254,796. Acetylation of cellulose textile articles. SOC. RHODIACETA. 5 Nov., 1969 [6 Nov., 1968], No. 54344/69. Heading C3A. Cellulose acetate textile articles having a combined acetic acid content of 50 to 62-5% are prepared by treating regenerated cellulose textile articles at 100‹ to 135‹ C. in the presence of an alkali metal acetate e.g. potassium acetate, with a bath containing more than 95% by weight of acetic anhydride, maintaining the acetic anhydride content of the bath constantly above 95% by weight by removing impurities formed and introducing fresh acetic anhydride in the course of the process, and keeping the constituent filaments of the textile articles at a substantially constant length throughout the process. The cellulose textile articles may be yarns, tows, woven or knitted fabrics of regenerated cellulose fibres which do not possess a fibrillar structure or have a fibrillar and oriented micro-structure. The textile article may be impregnated with 80-180% of potassium acetate, based on the weight of the cellulose. The process may be carried out continuously by passing the regenerated cellulose textile articles through a bath of an aqueous solution of the alkali metal acetate, drying them, passing them into the acetic anhydride bath while keeping their dimensions substantially constant, removing them from the bath, and freeing them substantially from unreacted acetic anhydride and from alkali metal acetate and acetic acid, whether free or combined as a complex salt.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR172765 | 1968-11-06 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1254796A true GB1254796A (en) | 1971-11-24 |
Family
ID=8656548
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB54344/69A Expired GB1254796A (en) | 1968-11-06 | 1969-11-05 | Improvements in the acetylation of textile articles of cellulose |
Country Status (11)
Country | Link |
---|---|
US (1) | US3655326A (en) |
AT (1) | AT297657B (en) |
BE (1) | BE741322A (en) |
BR (1) | BR6913866D0 (en) |
CH (1) | CH1646569D (en) |
DE (1) | DE1955931A1 (en) |
ES (1) | ES373233A1 (en) |
FR (1) | FR1590866A (en) |
GB (1) | GB1254796A (en) |
NL (1) | NL6916310A (en) |
RO (1) | RO55880A (en) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4322965C1 (en) * | 1993-07-09 | 1994-10-06 | Rhodia Ag Rhone Poulenc | Filter tow, manufacture thereof, and use thereof as tobacco smoke filter element |
WO2020082294A1 (en) * | 2018-10-25 | 2020-04-30 | 深圳大学 | Cellulose ester and preparation method therefor and application thereof |
CN109485735A (en) * | 2018-10-25 | 2019-03-19 | 深圳大学 | Cellulose esters and its preparation method and application |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1546211A (en) * | 1922-02-01 | 1925-07-14 | American Cellulose & Chemical | Manufacture of products containing cellulose |
US1930895A (en) * | 1930-02-13 | 1933-10-17 | Chem Ind Basel | Cellulose esters and process of making same |
US2348001A (en) * | 1941-10-24 | 1944-05-02 | Nat Vulcanized Fibre Company | Acetylation of cellulose |
NL256447A (en) * | 1959-10-02 | 1900-01-01 | ||
US3037902A (en) * | 1960-12-22 | 1962-06-05 | Rayonier Inc | Partial acetylation of cellulose |
-
0
- CH CH1646569D patent/CH1646569D/xx unknown
-
1968
- 1968-11-06 FR FR172765A patent/FR1590866A/fr not_active Expired
-
1969
- 1969-10-29 NL NL6916310A patent/NL6916310A/xx unknown
- 1969-11-03 RO RO61448A patent/RO55880A/ro unknown
- 1969-11-03 BR BR213866/69A patent/BR6913866D0/en unknown
- 1969-11-05 BE BE741322D patent/BE741322A/xx unknown
- 1969-11-05 GB GB54344/69A patent/GB1254796A/en not_active Expired
- 1969-11-05 US US874366A patent/US3655326A/en not_active Expired - Lifetime
- 1969-11-06 DE DE19691955931 patent/DE1955931A1/en active Pending
- 1969-11-06 AT AT1044769A patent/AT297657B/en not_active IP Right Cessation
- 1969-11-06 ES ES373233A patent/ES373233A1/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
FR1590866A (en) | 1970-04-20 |
DE1955931A1 (en) | 1970-06-11 |
BR6913866D0 (en) | 1973-01-16 |
ES373233A1 (en) | 1971-12-16 |
NL6916310A (en) | 1970-05-11 |
US3655326A (en) | 1972-04-11 |
BE741322A (en) | 1970-05-05 |
CH1646569D (en) | |
AT297657B (en) | 1972-04-10 |
RO55880A (en) | 1973-11-20 |
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