GB1248855A - Purification of vinyl acetate - Google Patents
Purification of vinyl acetateInfo
- Publication number
- GB1248855A GB1248855A GB52360/69A GB5236069A GB1248855A GB 1248855 A GB1248855 A GB 1248855A GB 52360/69 A GB52360/69 A GB 52360/69A GB 5236069 A GB5236069 A GB 5236069A GB 1248855 A GB1248855 A GB 1248855A
- Authority
- GB
- United Kingdom
- Prior art keywords
- vinyl acetate
- oct
- purification
- extractive distillation
- hydrocarbon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 title abstract 4
- 238000000746 purification Methods 0.000 title 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 abstract 3
- 239000002904 solvent Substances 0.000 abstract 3
- 239000004215 Carbon black (E152) Substances 0.000 abstract 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 abstract 2
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 abstract 2
- 238000000895 extractive distillation Methods 0.000 abstract 2
- 229930195733 hydrocarbon Natural products 0.000 abstract 2
- 150000002430 hydrocarbons Chemical class 0.000 abstract 2
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 abstract 1
- 239000005977 Ethylene Substances 0.000 abstract 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 238000004508 fractional distillation Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 229910052763 palladium Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/04—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides onto unsaturated carbon-to-carbon bonds
- C07C67/05—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides onto unsaturated carbon-to-carbon bonds with oxidation
- C07C67/055—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides onto unsaturated carbon-to-carbon bonds with oxidation in the presence of platinum group metals or their compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US77048068A | 1968-10-25 | 1968-10-25 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1248855A true GB1248855A (en) | 1971-10-06 |
Family
ID=25088686
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB52360/69A Expired GB1248855A (en) | 1968-10-25 | 1969-10-24 | Purification of vinyl acetate |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3616271A (enExample) |
| JP (1) | JPS4812725B1 (enExample) |
| CA (1) | CA934322A (enExample) |
| DE (1) | DE1953750A1 (enExample) |
| FR (1) | FR2021616A1 (enExample) |
| GB (1) | GB1248855A (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112209830A (zh) * | 2020-10-20 | 2021-01-12 | 天津大学 | 醋酸乙烯酯的生产方法 |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2240317C3 (de) * | 1971-08-21 | 1975-07-10 | Asahi Kasei Kogyo K.K., Osaka (Japan) | Verfahren zur Wiedergewinnung erneut einsetzbarer palladiumhaltiger Katalysatoren aus flüssigen Reaktionsgemischen, die bei der Herstellung von Essigsäurearylestern anfallen |
| NL185202C (nl) * | 1972-10-25 | 1990-02-16 | Hoechst Ag | Werkwijze voor het winnen van vinylacetaat en desgewenst van methanol uit mengsels, die hoofdzakelijk vinylacetaat en methanol en als verontreinigingen methylacetaat en aceetaldehyde bevatten. |
| DE2928236C2 (de) * | 1979-07-12 | 1983-05-19 | Wacker-Chemie GmbH, 8000 München | Verfahren zum Trennen von Acetaldehyd aus Gemischen mit Chloroform, Methylenchlorid und Chlorfuran |
| DE3107731A1 (de) * | 1981-02-28 | 1982-09-16 | Basf Ag, 6700 Ludwigshafen | Verfahren zur abtrennung organischer jod-verbindungen von carbonylierungsprodukten des methanols, methylacetates und dimethylethers |
| US4692179A (en) * | 1982-05-03 | 1987-09-08 | Advanced Extraction Technologies, Inc. | Process for using alkyl substituted C8-C10 aromatic hydrocarbons as preferential physical solvents for selective processing of hydrocarbon gas streams |
| US4617038A (en) * | 1985-07-26 | 1986-10-14 | El Paso Hydrocarbons Company | Process for using preferential physical solvents for selective processing of hydrocarbon gas streams |
| US4680042A (en) * | 1985-12-13 | 1987-07-14 | Advanced Extraction Technologies, Inc. | Extractive stripping of inert-rich hydrocarbon gases with a preferential physical solvent |
-
1968
- 1968-10-25 US US770480A patent/US3616271A/en not_active Expired - Lifetime
-
1969
- 1969-09-05 CA CA061314A patent/CA934322A/en not_active Expired
- 1969-10-24 GB GB52360/69A patent/GB1248855A/en not_active Expired
- 1969-10-24 JP JP44084747A patent/JPS4812725B1/ja active Pending
- 1969-10-24 FR FR6936656A patent/FR2021616A1/fr not_active Withdrawn
- 1969-10-24 DE DE19691953750 patent/DE1953750A1/de active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112209830A (zh) * | 2020-10-20 | 2021-01-12 | 天津大学 | 醋酸乙烯酯的生产方法 |
| CN112209830B (zh) * | 2020-10-20 | 2021-08-27 | 天津大学 | 醋酸乙烯酯的生产方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| DE1953750A1 (de) | 1970-05-14 |
| CA934322A (en) | 1973-09-25 |
| JPS4812725B1 (enExample) | 1973-04-23 |
| US3616271A (en) | 1971-10-26 |
| FR2021616A1 (enExample) | 1970-07-24 |
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