GB1222942A - Process for recovering ammonium sulphate from aqueous solutions of ammonium sulphate which contain organic components - Google Patents

Process for recovering ammonium sulphate from aqueous solutions of ammonium sulphate which contain organic components

Info

Publication number
GB1222942A
GB1222942A GB651969A GB651969A GB1222942A GB 1222942 A GB1222942 A GB 1222942A GB 651969 A GB651969 A GB 651969A GB 651969 A GB651969 A GB 651969A GB 1222942 A GB1222942 A GB 1222942A
Authority
GB
United Kingdom
Prior art keywords
ammonium sulphate
caprolactam
aqueous solutions
recovering
organic components
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB651969A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Stamicarbon BV
Original Assignee
Stamicarbon BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Stamicarbon BV filed Critical Stamicarbon BV
Publication of GB1222942A publication Critical patent/GB1222942A/en
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0492—Applications, solvents used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/24—Sulfates of ammonium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1,222,942. Ammonium sulphate recovery. STAMICARBON N.V. 6 Feb., 1969 [8 Feb., 1968], No. 6519/69. Heading C1A. Ammonium sulphate is recovered from aqueous solutions thereof containing organic contaminants and obtained from the preparation of (a) acrylonitrile from propylene; (b) methyl methacrylate from acetone cyanohydrin; or (c) methyl acrylate from acrylonitrile by contacting the contaminated solution in a concentration which is substantially saturated with dioxan, dimethyl formamide, acetonitrile and/or a lactam (e.g. caprolactam) whereby the organic contaminants are concentrated in the organic phase, and recovering the ammonium sulphate from the other phase. The organic extractants are water soluble and may be used in the form of an aqueous solution; the ammonium sulphate may be crystallized in the presence of said extractants. Before extraction the contaminated ammonium sulphate solution may be mixed with one or more ammonium sulphate solutions obtained in the preparation of caprolactam, the latter solutions containing some caprolactam and so reducing the amount of caprolactam which must be added in the extraction.
GB651969A 1968-02-08 1969-02-06 Process for recovering ammonium sulphate from aqueous solutions of ammonium sulphate which contain organic components Expired GB1222942A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
NL6801824A NL162349C (en) 1968-02-08 1968-02-08 PROCESS FOR THE EXTRACTION OF AMMONIUM SULPHATE FROM AN AQUEOUS SOLUTION CONTAINED WITH ORGANIC SUBSTANCES.

Publications (1)

Publication Number Publication Date
GB1222942A true GB1222942A (en) 1971-02-17

Family

ID=19802710

Family Applications (1)

Application Number Title Priority Date Filing Date
GB651969A Expired GB1222942A (en) 1968-02-08 1969-02-06 Process for recovering ammonium sulphate from aqueous solutions of ammonium sulphate which contain organic components

Country Status (5)

Country Link
BE (1) BE727994A (en)
DE (1) DE1906327C3 (en)
FR (1) FR2001591A1 (en)
GB (1) GB1222942A (en)
NL (1) NL162349C (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4341535A (en) * 1981-01-02 1982-07-27 The Standard Oil Co. Ammonium sulfate recovery process

Also Published As

Publication number Publication date
DE1906327C3 (en) 1982-05-06
DE1906327B2 (en) 1979-04-19
BE727994A (en) 1969-08-06
FR2001591A1 (en) 1969-09-26
NL162349B (en) 1979-12-17
NL6801824A (en) 1969-08-12
DE1906327A1 (en) 1969-09-25
NL162349C (en) 1980-05-16

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