GB1208165A - A method of producing unsaturated organic acid glycidyl esters - Google Patents

A method of producing unsaturated organic acid glycidyl esters

Info

Publication number
GB1208165A
GB1208165A GB91268A GB91268A GB1208165A GB 1208165 A GB1208165 A GB 1208165A GB 91268 A GB91268 A GB 91268A GB 91268 A GB91268 A GB 91268A GB 1208165 A GB1208165 A GB 1208165A
Authority
GB
United Kingdom
Prior art keywords
organic acid
unsaturated organic
unsaturated
soap
glycidyl esters
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB91268A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NOF Corp
Original Assignee
Nippon Oil and Fats Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Oil and Fats Co Ltd filed Critical Nippon Oil and Fats Co Ltd
Publication of GB1208165A publication Critical patent/GB1208165A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
    • C07D303/16—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by esterified hydroxyl radicals

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Epoxy Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1,208,165. Unsaturated glycidyl esters. NIPPON YUSHI K.K. 5 Jan., 1968 [7 Jan., 1967], No. 912/68. Heading C2C. A method of producing unsaturated organic acid glycidyl esters is characterized in that a soap of an unsaturated organic acid and epichlorohydrin are reacted in the presence of a catalyst and an aromatic or cyclic aliphatic hydrocarbon solvent in the proportion of ¢ to 6 times by weight of the amount of the soap of the unsaturated organic acid employed and after the reaction water is added at the rate of 100 to 600 gm. of water based on one mole of the soap of unsaturated acid and the resulting aqueous phase is removed and then the resulting organic phase is distilled to obtain the desired ester. Catalysts specified include quaternary ammonium salts, tertiary amines and tertiary amine hydrochloric acid salts. Hydrocarbon solvents specified are benzene, toluene, xylene, cyclohexane and cyclohexene. Polymerization inhibitors may be added to the reaction mixture. The examples describe the preparation of glycidyl acrylate and methacrylate.
GB91268A 1967-01-07 1968-01-05 A method of producing unsaturated organic acid glycidyl esters Expired GB1208165A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP135067 1967-01-07

Publications (1)

Publication Number Publication Date
GB1208165A true GB1208165A (en) 1970-10-07

Family

ID=11499025

Family Applications (1)

Application Number Title Priority Date Filing Date
GB91268A Expired GB1208165A (en) 1967-01-07 1968-01-05 A method of producing unsaturated organic acid glycidyl esters

Country Status (3)

Country Link
DE (1) DE1668512C3 (en)
GB (1) GB1208165A (en)
NL (1) NL6800197A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117777060A (en) * 2023-12-26 2024-03-29 同宇新材料(广东)股份有限公司 Preparation method of linoleic acid glycidyl ester

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117777060A (en) * 2023-12-26 2024-03-29 同宇新材料(广东)股份有限公司 Preparation method of linoleic acid glycidyl ester

Also Published As

Publication number Publication date
DE1668512C3 (en) 1978-08-10
DE1668512B2 (en) 1977-12-08
DE1668512A1 (en) 1972-04-06
NL6800197A (en) 1968-07-08

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Legal Events

Date Code Title Description
PS Patent sealed
PCNP Patent ceased through non-payment of renewal fee