GB1195852A - Hydrogen continuous production method and apparatus - Google Patents
Hydrogen continuous production method and apparatusInfo
- Publication number
- GB1195852A GB1195852A GB31165/67A GB3116567A GB1195852A GB 1195852 A GB1195852 A GB 1195852A GB 31165/67 A GB31165/67 A GB 31165/67A GB 3116567 A GB3116567 A GB 3116567A GB 1195852 A GB1195852 A GB 1195852A
- Authority
- GB
- United Kingdom
- Prior art keywords
- diffusion
- hydrogen
- feedstock
- line
- stream
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000001257 hydrogen Substances 0.000 title abstract 5
- 229910052739 hydrogen Inorganic materials 0.000 title abstract 5
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 title abstract 4
- 238000010924 continuous production Methods 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- 238000009792 diffusion process Methods 0.000 abstract 4
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 abstract 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 abstract 2
- 229910001252 Pd alloy Inorganic materials 0.000 abstract 1
- 239000003463 adsorbent Substances 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000006392 deoxygenation reaction Methods 0.000 abstract 1
- 239000011888 foil Substances 0.000 abstract 1
- 239000007789 gas Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 229930195733 hydrocarbon Natural products 0.000 abstract 1
- 150000002430 hydrocarbons Chemical class 0.000 abstract 1
- 150000002431 hydrogen Chemical class 0.000 abstract 1
- 238000005984 hydrogenation reaction Methods 0.000 abstract 1
- 239000002808 molecular sieve Substances 0.000 abstract 1
- 229910052763 palladium Inorganic materials 0.000 abstract 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
- C01B3/50—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification
- C01B3/501—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification by diffusion
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/22—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by diffusion
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2313/00—Details relating to membrane modules or apparatus
- B01D2313/22—Cooling or heating elements
- B01D2313/221—Heat exchangers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2313/00—Details relating to membrane modules or apparatus
- B01D2313/42—Catalysts within the flow path
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
- C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
- C01B2203/0405—Purification by membrane separation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
- C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
- C01B2203/0465—Composition of the impurity
- C01B2203/048—Composition of the impurity the impurity being an organic compound
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Inorganic Chemistry (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Hydrogen, Water And Hydrids (AREA)
Abstract
1,195,852. Separating hydrogen by diffusion. UNION -CARBIDE CORP..6 July, (1967, No. 31165/67. Heading B1L. Hydrogen of high purity is separated from impunities present in a feedstock by passing the feed gas by line 23 to, a guard chamber 25 filled with an adsorbent, e.g. a molecular sieve, then by lines 27 and 31 to a conditioner 33 containing a hydrogenation or a combined hydrogenation-deoxygenation catalyst, before heating the stream in heater 37 and passing the heated stream, at a temperature adequate for diffusion, e.g. about 400C., by line 39 .to elongated diffuser 43 where the stream is caused to impinge on the 'palladium or palladium alloy foil surfaces of a number of diffusion drum elements. Pure hydrogen which diffuses through these surfaces is taken from the elements by line 89, and depleted feedstock by .line 87. Suitably, both take-off streams are passed in indirect heat exchange with feedstock in a heat exchanger 3.9. In Figs. 2-4 (not shown), constructional details of the diffuser and of the diffusion elements are provided. In the examples, the feedstock comprised 50-60% hydrogen, the remainder comprising mostly methane with very .small amounts of other gaseous hydrocarbons.
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US411928A US3336730A (en) | 1964-11-17 | 1964-11-17 | Hydrogen continuous production method and apparatus |
| GB31165/67A GB1195852A (en) | 1967-07-06 | 1967-07-06 | Hydrogen continuous production method and apparatus |
| FR117384A FR1535060A (en) | 1967-07-06 | 1967-08-09 | Method and apparatus for the continuous production of very pure hydrogen |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB31165/67A GB1195852A (en) | 1967-07-06 | 1967-07-06 | Hydrogen continuous production method and apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1195852A true GB1195852A (en) | 1970-06-24 |
Family
ID=10319004
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB31165/67A Expired GB1195852A (en) | 1964-11-17 | 1967-07-06 | Hydrogen continuous production method and apparatus |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB1195852A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2571270A1 (en) * | 1984-10-04 | 1986-04-11 | Petroles Cie Francaise | Permeation circuit for gas containing hydrocarbons |
| EP0718031A1 (en) * | 1994-12-19 | 1996-06-26 | Bend Research, Inc. | Composite hydrogen separation element and module |
| US5645626A (en) * | 1990-08-10 | 1997-07-08 | Bend Research, Inc. | Composite hydrogen separation element and module |
| EP0854111A2 (en) * | 1997-01-20 | 1998-07-22 | Ngk Insulators, Ltd. | Apparatus for recovering, refining, and storing hydrogen gas |
-
1967
- 1967-07-06 GB GB31165/67A patent/GB1195852A/en not_active Expired
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2571270A1 (en) * | 1984-10-04 | 1986-04-11 | Petroles Cie Francaise | Permeation circuit for gas containing hydrocarbons |
| US5645626A (en) * | 1990-08-10 | 1997-07-08 | Bend Research, Inc. | Composite hydrogen separation element and module |
| EP0718031A1 (en) * | 1994-12-19 | 1996-06-26 | Bend Research, Inc. | Composite hydrogen separation element and module |
| EP0854111A2 (en) * | 1997-01-20 | 1998-07-22 | Ngk Insulators, Ltd. | Apparatus for recovering, refining, and storing hydrogen gas |
| EP0854111A3 (en) * | 1997-01-20 | 1999-03-03 | Ngk Insulators, Ltd. | Apparatus for recovering, refining, and storing hydrogen gas |
| US6179902B1 (en) | 1997-01-20 | 2001-01-30 | Ngk Insulators, Ltd. | Apparatus for recovering, refining, and storing hydrogen gas |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| 429A | Application made for amendment of specification (sect. 29/1949) | ||
| 429H | Application (made) for amendment of specification now open to opposition (sect. 29/1949) | ||
| 429D | Case decided by the comptroller ** specification amended (sect. 29/1949) | ||
| SPA | Amended specification published | ||
| PLNP | Patent lapsed through nonpayment of renewal fees |