GB1165521A - A process for the production of Imidazole-Containing Polyamidoamines - Google Patents

A process for the production of Imidazole-Containing Polyamidoamines

Info

Publication number
GB1165521A
GB1165521A GB813168A GB813168A GB1165521A GB 1165521 A GB1165521 A GB 1165521A GB 813168 A GB813168 A GB 813168A GB 813168 A GB813168 A GB 813168A GB 1165521 A GB1165521 A GB 1165521A
Authority
GB
United Kingdom
Prior art keywords
copolymer
mixture
fatty acid
temperature
imidazoline
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB813168A
Inventor
Hermann Delius
Wilhelm Becker
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Beck Koller and Company England Ltd
Original Assignee
Beck Koller and Company England Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Beck Koller and Company England Ltd filed Critical Beck Koller and Company England Ltd
Publication of GB1165521A publication Critical patent/GB1165521A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/26Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from polyamines and polycarboxylic acids
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F8/00Chemical modification by after-treatment
    • C08F8/30Introducing nitrogen atoms or nitrogen-containing groups
    • C08F8/32Introducing nitrogen atoms or nitrogen-containing groups by reaction with amines
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L63/00Compositions of epoxy resins; Compositions of derivatives of epoxy resins

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
  • Epoxy Resins (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

Abstract

1,165,521. Imidazoline-containing polyamidoamine resins. BECK KOLLER & CO. (ENGLAND) Ltd. 20 Feb., 1968 [22 Feb., 1967], No., 8131/68. Heading C3P. An imidazoline-containing polyamidoamine resin is prepared from a copolymer of a conjugated-unsaturated fatty acid and/or a conjugated unsaturated fatty acid ester or a mixture thereof with one or more ethylenically unsaturated aromatic compounds and one or more amines selected from amines of the formula H(NHCH 2 CH 2 ) x NH 2 , where x is an integer from 1 to 5 inclusive by Ca, preparing the copolymer by continuously adding to the acid and/or ester or mixture thereof from 0.5 to 3 mols. per mol. of the aromatic compound or compound mixture over a period of from 5 to 30 hours, the reaction mixture being stirred and maintained at a temperature of from 150‹ to 250‹ C. in an atmosphere of a gas inert to the reactants, and further heating the reaction mixture at 150‹ to 250‹ C. to complete the reaction; and (b) reacting the resulting copolymer with a substantially equimolar quantity of the amine by heating at a temperature of up to 200‹ C. to form the polyamidoamine; and (c) heating the resulting polyamidoamine resin to a temperature of from 200‹ to 350‹ C. for a sufficient time to convert it to the imidazoline derivative. In the examples dehydrated castor oil fatty acid is copolymerized with styrene in the presence of lauryl mercaptan and di-tertbutyl peroxide and the copolymer treated with diethylene triamine.
GB813168A 1967-02-22 1968-02-20 A process for the production of Imidazole-Containing Polyamidoamines Expired GB1165521A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DER0045343 1967-02-22

Publications (1)

Publication Number Publication Date
GB1165521A true GB1165521A (en) 1969-10-01

Family

ID=7407602

Family Applications (1)

Application Number Title Priority Date Filing Date
GB813168A Expired GB1165521A (en) 1967-02-22 1968-02-20 A process for the production of Imidazole-Containing Polyamidoamines

Country Status (2)

Country Link
DE (1) DE1745322B2 (en)
GB (1) GB1165521A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1716219A2 (en) * 2003-10-30 2006-11-02 Nalco Company Water-soluble polyaminoamides comprising 1,3-diimines as sunscreen agents
WO2018132525A1 (en) * 2017-01-11 2018-07-19 Saudi Arabian Oil Company Emulsifiers for invert emulsion drilling fluids

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1716219A2 (en) * 2003-10-30 2006-11-02 Nalco Company Water-soluble polyaminoamides comprising 1,3-diimines as sunscreen agents
EP1716219A4 (en) * 2003-10-30 2008-05-07 Nalco Co Water-soluble polyaminoamides comprising 1,3-diimines as sunscreen agents
WO2018132525A1 (en) * 2017-01-11 2018-07-19 Saudi Arabian Oil Company Emulsifiers for invert emulsion drilling fluids
CN110191936A (en) * 2017-01-11 2019-08-30 沙特阿拉伯石油公司 Emulsifier for invert emulsion drilling fluid

Also Published As

Publication number Publication date
DE1745322A1 (en) 1972-05-04
DE1745322B2 (en) 1973-02-22

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Legal Events

Date Code Title Description
PS Patent sealed
PLNP Patent lapsed through nonpayment of renewal fees