GB1137054A - A process and apparatus for the production of ultra-pure 1,3,5-trioxane - Google Patents
A process and apparatus for the production of ultra-pure 1,3,5-trioxaneInfo
- Publication number
- GB1137054A GB1137054A GB1688/66A GB168866A GB1137054A GB 1137054 A GB1137054 A GB 1137054A GB 1688/66 A GB1688/66 A GB 1688/66A GB 168866 A GB168866 A GB 168866A GB 1137054 A GB1137054 A GB 1137054A
- Authority
- GB
- United Kingdom
- Prior art keywords
- trioxane
- water
- organic
- pure
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- BGJSXRVXTHVRSN-UHFFFAOYSA-N 1,3,5-trioxane Chemical compound C1OCOCO1 BGJSXRVXTHVRSN-UHFFFAOYSA-N 0.000 title abstract 11
- 238000000034 method Methods 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract 7
- 238000004821 distillation Methods 0.000 abstract 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 abstract 3
- 239000012074 organic phase Substances 0.000 abstract 3
- 239000003960 organic solvent Substances 0.000 abstract 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 abstract 2
- 239000008346 aqueous phase Substances 0.000 abstract 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 abstract 1
- KNIUHBNRWZGIQQ-UHFFFAOYSA-N 7-diethoxyphosphinothioyloxy-4-methylchromen-2-one Chemical compound CC1=CC(=O)OC2=CC(OP(=S)(OCC)OCC)=CC=C21 KNIUHBNRWZGIQQ-UHFFFAOYSA-N 0.000 abstract 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 abstract 1
- 229930040373 Paraformaldehyde Natural products 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 239000008098 formaldehyde solution Substances 0.000 abstract 1
- 235000019253 formic acid Nutrition 0.000 abstract 1
- 238000004508 fractional distillation Methods 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 239000011261 inert gas Substances 0.000 abstract 1
- 229920002866 paraformaldehyde Polymers 0.000 abstract 1
- 238000010992 reflux Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D323/00—Heterocyclic compounds containing more than two oxygen atoms as the only ring hetero atoms
- C07D323/04—Six-membered rings
- C07D323/06—Trioxane
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B60—VEHICLES IN GENERAL
- B60C—VEHICLE TYRES; TYRE INFLATION; TYRE CHANGING; CONNECTING VALVES TO INFLATABLE ELASTIC BODIES IN GENERAL; DEVICES OR ARRANGEMENTS RELATED TO TYRES
- B60C3/00—Tyres characterised by the transverse section
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B60—VEHICLES IN GENERAL
- B60C—VEHICLE TYRES; TYRE INFLATION; TYRE CHANGING; CONNECTING VALVES TO INFLATABLE ELASTIC BODIES IN GENERAL; DEVICES OR ARRANGEMENTS RELATED TO TYRES
- B60C3/00—Tyres characterised by the transverse section
- B60C3/08—Tyres characterised by the transverse section collapsible into storage or non-use condition, e.g. space-saving spare tyres
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B60—VEHICLES IN GENERAL
- B60C—VEHICLE TYRES; TYRE INFLATION; TYRE CHANGING; CONNECTING VALVES TO INFLATABLE ELASTIC BODIES IN GENERAL; DEVICES OR ARRANGEMENTS RELATED TO TYRES
- B60C5/00—Inflatable pneumatic tyres or inner tubes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF0044939 | 1965-01-13 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1137054A true GB1137054A (en) | 1968-12-18 |
Family
ID=27560450
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB1688/66A Expired GB1137054A (en) | 1965-01-13 | 1966-01-13 | A process and apparatus for the production of ultra-pure 1,3,5-trioxane |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US3395157A (en:Method) |
| AT (1) | AT255419B (en:Method) |
| BE (1) | BE674890A (en:Method) |
| CH (1) | CH461529A (en:Method) |
| DE (1) | DE1493688A1 (en:Method) |
| FR (1) | FR1463315A (en:Method) |
| GB (1) | GB1137054A (en:Method) |
| NL (1) | NL149498B (en:Method) |
| SE (1) | SE314383B (en:Method) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111317154A (zh) * | 2020-04-01 | 2020-06-23 | 江西省食品药品安全监控中心 | 一种用于大蒜成分提取的设备及提取工艺 |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4043873A (en) * | 1973-06-15 | 1977-08-23 | Societa' Italiana Resine S.I.R. S.P.A. | Plural stage recovery of trioxane in a process having a molecular distillation step |
| US4332644A (en) * | 1981-06-08 | 1982-06-01 | Asahi Kasei Kogyo Kabushiki Kaisha | Process for separating trioxane |
| US5171407A (en) * | 1989-09-22 | 1992-12-15 | Sulzer Brothers Limited | Distillation plant for producing hydrogen peroxide |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3024170A (en) * | 1959-06-15 | 1962-03-06 | Donald F Othmer | Process of azeotropic distillation of formic acid from acetic acid |
| GB1020812A (en) * | 1961-09-12 | 1966-02-23 | Yawata Chemical Industry Compa | Process for producing trioxane |
| DE1272931B (de) * | 1962-05-04 | 1968-07-18 | Knapsack Ag | Verfahren zur Herstellung von Trioxan |
-
1965
- 1965-01-13 DE DE19651493688 patent/DE1493688A1/de active Pending
- 1965-12-06 CH CH1677065A patent/CH461529A/de unknown
- 1965-12-17 AT AT1135765A patent/AT255419B/de active
- 1965-12-17 NL NL656516508A patent/NL149498B/xx unknown
- 1965-12-28 SE SE16845/65A patent/SE314383B/xx unknown
-
1966
- 1966-01-07 FR FR45253A patent/FR1463315A/fr not_active Expired
- 1966-01-07 US US519248A patent/US3395157A/en not_active Expired - Lifetime
- 1966-01-10 BE BE674890D patent/BE674890A/xx unknown
- 1966-01-13 GB GB1688/66A patent/GB1137054A/en not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111317154A (zh) * | 2020-04-01 | 2020-06-23 | 江西省食品药品安全监控中心 | 一种用于大蒜成分提取的设备及提取工艺 |
| CN111317154B (zh) * | 2020-04-01 | 2022-05-03 | 江西省药品检查员中心(江西省疫苗检查中心) | 一种用于大蒜成分提取的设备及提取工艺 |
Also Published As
| Publication number | Publication date |
|---|---|
| DE1493688A1 (de) | 1969-06-19 |
| SE314383B (en:Method) | 1969-09-08 |
| CH461529A (de) | 1968-08-31 |
| NL149498B (nl) | 1976-05-17 |
| AT255419B (de) | 1967-07-10 |
| NL6516508A (en:Method) | 1966-07-14 |
| BE674890A (en:Method) | 1966-05-03 |
| US3395157A (en) | 1968-07-30 |
| FR1463315A (fr) | 1966-12-23 |
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