GB1129622A - Process for the manufacture of ªß-pinene - Google Patents

Process for the manufacture of ªß-pinene

Info

Publication number
GB1129622A
GB1129622A GB2668/66A GB266866A GB1129622A GB 1129622 A GB1129622 A GB 1129622A GB 2668/66 A GB2668/66 A GB 2668/66A GB 266866 A GB266866 A GB 266866A GB 1129622 A GB1129622 A GB 1129622A
Authority
GB
United Kingdom
Prior art keywords
pinene
catalyst
distillation
suitably
hydrogen
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2668/66A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hoechst AG
Original Assignee
Hoechst AG
Farbwerke Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst AG, Farbwerke Hoechst AG filed Critical Hoechst AG
Publication of GB1129622A publication Critical patent/GB1129622A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C5/00Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
    • C07C5/22Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by isomerisation
    • C07C5/23Rearrangement of carbon-to-carbon unsaturated bonds
    • C07C5/25Migration of carbon-to-carbon double bonds
    • C07C5/2506Catalytic processes
    • C07C5/2556Catalytic processes with metals
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/584Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

1,129,622. #-Pinene. FARBWERKE HOECHST A.G. 20 Jan., 1966 [10 Sept., 1965], No. 2668/66. Heading C5E. #-Pinene is prepared by isomerizing α- pinene in the vapour phase at 140-200‹ C. in the absence of oxygen, in the presence as 1-5 vol. per cent (based on the pinene volume) of hydrogen, and over a palladium/carbon catalyst. The hydrogen serves to regenerate the catalyst and act as a carrier gas. The residence time is suitably 0À1-20 seconds. The feed is suitably a pinene-containing turpentine oil or terpene mixture, or a technical grade α-pinene. The product, after separation from the catalyst, is passed continuously to a distillation column where #-pinene concentrates and α-pinene is taken off overhead and recycled. The distillation is continued until the #-pinene content has reached the desired level, at which point further distillation will yield pure #-pinene and unconverted α-pinene which can be rearranged to camphene with titanic acid.
GB2668/66A 1965-09-10 1966-01-20 Process for the manufacture of ªß-pinene Expired GB1129622A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEF47145A DE1221218B (en) 1965-09-10 1965-09-10 Process for the production of beta-pinene

Publications (1)

Publication Number Publication Date
GB1129622A true GB1129622A (en) 1968-10-09

Family

ID=7101448

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2668/66A Expired GB1129622A (en) 1965-09-10 1966-01-20 Process for the manufacture of ªß-pinene

Country Status (3)

Country Link
DE (1) DE1221218B (en)
FR (1) FR1462791A (en)
GB (1) GB1129622A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104945216A (en) * 2015-05-19 2015-09-30 广西众昌树脂有限公司 Preparation method of beta-pinene

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104945216A (en) * 2015-05-19 2015-09-30 广西众昌树脂有限公司 Preparation method of beta-pinene

Also Published As

Publication number Publication date
FR1462791A (en) 1966-12-16
DE1221218B (en) 1966-07-21

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