GB1084726A - A process for sulphonating and/or sulphating organic compounds and an apparatus for carrying out the process - Google Patents

A process for sulphonating and/or sulphating organic compounds and an apparatus for carrying out the process

Info

Publication number
GB1084726A
GB1084726A GB4558/65A GB455865A GB1084726A GB 1084726 A GB1084726 A GB 1084726A GB 4558/65 A GB4558/65 A GB 4558/65A GB 455865 A GB455865 A GB 455865A GB 1084726 A GB1084726 A GB 1084726A
Authority
GB
United Kingdom
Prior art keywords
controlling
reaction vessel
reaction
mixture
sulphated
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB4558/65A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mo och Domsjo AB
Original Assignee
Mo och Domsjo AB
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mo och Domsjo AB filed Critical Mo och Domsjo AB
Publication of GB1084726A publication Critical patent/GB1084726A/en
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/07—Stirrers characterised by their mounting on the shaft
    • B01F27/072—Stirrers characterised by their mounting on the shaft characterised by the disposition of the stirrers with respect to the rotating axis
    • B01F27/0722—Stirrers characterised by their mounting on the shaft characterised by the disposition of the stirrers with respect to the rotating axis perpendicular with respect to the rotating axis
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B45/00—Formation or introduction of functional groups containing sulfur
    • C07B45/02—Formation or introduction of functional groups containing sulfur of sulfo or sulfonyldioxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
    • C07C303/04—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups
    • C07C303/06—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups by reaction with sulfuric acid or sulfur trioxide
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/24—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of esters of sulfuric acids
    • H—ELECTRICITY
    • H02—GENERATION; CONVERSION OR DISTRIBUTION OF ELECTRIC POWER
    • H02P—CONTROL OR REGULATION OF ELECTRIC MOTORS, ELECTRIC GENERATORS OR DYNAMO-ELECTRIC CONVERTERS; CONTROLLING TRANSFORMERS, REACTORS OR CHOKE COILS
    • H02P29/00—Arrangements for regulating or controlling electric motors, appropriate for both AC and DC motors
    • H02P29/40—Regulating or controlling the amount of current drawn or delivered by the motor for controlling the mechanical load
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00168—Controlling or regulating processes controlling the viscosity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00189—Controlling or regulating processes controlling the stirring velocity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18—Details relating to the spatial orientation of the reactor
    • B01J2219/185—Details relating to the spatial orientation of the reactor vertical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Power Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1,084,726. Controlling chemical reactions; controlling mixing by viscosity. MO OCH DOMSJO A.B. Feb. 2, 1965 [Feb. 4, 1964], No. 4558/65. Headings B1C and B1X. Organic compounds are sulphonated and/or sulphated by reaction with gaseous sulphur trioxide, or a mixture thereof with air, the supply of organic compound to the reaction vessel being controlled automatically by a device which is actuated by changes in the resistance to the motion of a stirring device in the reaction vessel, so as to keep the viscosity of the reaction mixture substantially constant. As shown, a water-jacketted reaction vessel 1 is provided with a cooled stirrer 9 driven by an electric motor 11, the current intensity or power demand of the motor 11 controlling a transducer 12 which actuates a valve 14 controlling admission of organic compound to the reactor 1. Sulphur trioxide mixture is admitted through inlet 5. A temperature control device 8 in the product outlet 7 controls admission of cooling water to the jacket of the reactor. Compounds which may be sulphonated and/or sulphated include fatty alcohols, polyglycol ethers, alkyl benzenes, fatty acids and fat oils.
GB4558/65A 1964-02-04 1965-02-02 A process for sulphonating and/or sulphating organic compounds and an apparatus for carrying out the process Expired GB1084726A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SE1316/64A SE308303B (en) 1964-02-04 1964-02-04

Publications (1)

Publication Number Publication Date
GB1084726A true GB1084726A (en) 1967-09-27

Family

ID=20257987

Family Applications (1)

Application Number Title Priority Date Filing Date
GB4558/65A Expired GB1084726A (en) 1964-02-04 1965-02-02 A process for sulphonating and/or sulphating organic compounds and an apparatus for carrying out the process

Country Status (8)

Country Link
BE (1) BE658275A (en)
CH (1) CH443270A (en)
DE (1) DE1284966B (en)
DK (1) DK116583B (en)
FI (1) FI42540B (en)
GB (1) GB1084726A (en)
NL (2) NL6501304A (en)
SE (1) SE308303B (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105688773A (en) * 2016-03-02 2016-06-22 江苏丰泽生物工程设备制造有限公司 Reactor temperature control integrated device capable of achieving precise temperature control
CN109876756A (en) * 2019-04-01 2019-06-14 天津市科德化工有限公司 Industrial sulfonation production system

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES388435A1 (en) * 1970-02-23 1974-01-16 Mazzoni G Mecc Costr Method for sulphonatizing and/or sulphatizing organic compounds with sulphur trioxide and apparatus therefor
CN112516940A (en) * 2020-10-26 2021-03-19 上海斯诺化学科技有限公司 Waste liquid recovery device for polyurethane rheology modifier synthesis reaction

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105688773A (en) * 2016-03-02 2016-06-22 江苏丰泽生物工程设备制造有限公司 Reactor temperature control integrated device capable of achieving precise temperature control
CN109876756A (en) * 2019-04-01 2019-06-14 天津市科德化工有限公司 Industrial sulfonation production system

Also Published As

Publication number Publication date
CH443270A (en) 1967-09-15
DK116583B (en) 1970-01-26
NL6501304A (en) 1965-08-05
FI42540B (en) 1970-06-01
NL125243C (en)
SE308303B (en) 1969-02-10
DE1284966B (en) 1968-12-12
BE658275A (en) 1965-04-30

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