GB1079391A - Process for increasing the wettability of difficult to wet surfaces - Google Patents
Process for increasing the wettability of difficult to wet surfacesInfo
- Publication number
- GB1079391A GB1079391A GB2832064A GB2832064A GB1079391A GB 1079391 A GB1079391 A GB 1079391A GB 2832064 A GB2832064 A GB 2832064A GB 2832064 A GB2832064 A GB 2832064A GB 1079391 A GB1079391 A GB 1079391A
- Authority
- GB
- United Kingdom
- Prior art keywords
- solution
- detergent
- salt
- aqueous
- immersed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000003599 detergent Substances 0.000 abstract 9
- 239000000243 solution Substances 0.000 abstract 8
- 229910021626 Tin(II) chloride Inorganic materials 0.000 abstract 6
- 239000007864 aqueous solution Substances 0.000 abstract 6
- -1 polypropylene Polymers 0.000 abstract 6
- 150000003839 salts Chemical class 0.000 abstract 6
- 235000011150 stannous chloride Nutrition 0.000 abstract 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 5
- TXUICONDJPYNPY-UHFFFAOYSA-N (1,10,13-trimethyl-3-oxo-4,5,6,7,8,9,11,12,14,15,16,17-dodecahydrocyclopenta[a]phenanthren-17-yl) heptanoate Chemical compound C1CC2CC(=O)C=C(C)C2(C)C2C1C1CCC(OC(=O)CCCCCC)C1(C)CC2 TXUICONDJPYNPY-UHFFFAOYSA-N 0.000 abstract 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 4
- 239000004743 Polypropylene Substances 0.000 abstract 4
- CMOAHYOGLLEOGO-UHFFFAOYSA-N oxozirconium;dihydrochloride Chemical compound Cl.Cl.[Zr]=O CMOAHYOGLLEOGO-UHFFFAOYSA-N 0.000 abstract 4
- 229920000642 polymer Polymers 0.000 abstract 4
- 229920001155 polypropylene Polymers 0.000 abstract 4
- 239000007787 solid Substances 0.000 abstract 4
- 239000001119 stannous chloride Substances 0.000 abstract 4
- 239000004793 Polystyrene Substances 0.000 abstract 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 abstract 3
- 229920002223 polystyrene Polymers 0.000 abstract 3
- ZSLUVFAKFWKJRC-IGMARMGPSA-N 232Th Chemical compound [232Th] ZSLUVFAKFWKJRC-IGMARMGPSA-N 0.000 abstract 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 2
- 239000004677 Nylon Substances 0.000 abstract 2
- 229910052776 Thorium Inorganic materials 0.000 abstract 2
- 229910010062 TiCl3 Inorganic materials 0.000 abstract 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 abstract 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 abstract 2
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 2
- 150000007513 acids Chemical class 0.000 abstract 2
- 150000001412 amines Chemical class 0.000 abstract 2
- 150000002148 esters Chemical class 0.000 abstract 2
- 239000004744 fabric Substances 0.000 abstract 2
- 239000012530 fluid Substances 0.000 abstract 2
- 229910052732 germanium Inorganic materials 0.000 abstract 2
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 abstract 2
- 230000002209 hydrophobic effect Effects 0.000 abstract 2
- 229910017053 inorganic salt Inorganic materials 0.000 abstract 2
- 150000002576 ketones Chemical class 0.000 abstract 2
- 230000008018 melting Effects 0.000 abstract 2
- 238000002844 melting Methods 0.000 abstract 2
- 150000007522 mineralic acids Chemical class 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 238000000465 moulding Methods 0.000 abstract 2
- 229920001778 nylon Polymers 0.000 abstract 2
- 150000007524 organic acids Chemical class 0.000 abstract 2
- 239000003960 organic solvent Substances 0.000 abstract 2
- 239000003791 organic solvent mixture Substances 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- 239000000126 substance Substances 0.000 abstract 2
- AXZWODMDQAVCJE-UHFFFAOYSA-L tin(II) chloride (anhydrous) Chemical compound [Cl-].[Cl-].[Sn+2] AXZWODMDQAVCJE-UHFFFAOYSA-L 0.000 abstract 2
- 229910052719 titanium Inorganic materials 0.000 abstract 2
- 239000010936 titanium Substances 0.000 abstract 2
- YONPGGFAJWQGJC-UHFFFAOYSA-K titanium(iii) chloride Chemical compound Cl[Ti](Cl)Cl YONPGGFAJWQGJC-UHFFFAOYSA-K 0.000 abstract 2
- 229910052726 zirconium Inorganic materials 0.000 abstract 2
- HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 abstract 1
- 239000004698 Polyethylene Substances 0.000 abstract 1
- QHGIKMVOLGCZIP-UHFFFAOYSA-N germanium dichloride Chemical compound Cl[Ge]Cl QHGIKMVOLGCZIP-UHFFFAOYSA-N 0.000 abstract 1
- 229910052735 hafnium Inorganic materials 0.000 abstract 1
- VBJZVLUMGGDVMO-UHFFFAOYSA-N hafnium atom Chemical compound [Hf] VBJZVLUMGGDVMO-UHFFFAOYSA-N 0.000 abstract 1
- 239000000976 ink Substances 0.000 abstract 1
- 229940046892 lead acetate Drugs 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 229920000573 polyethylene Polymers 0.000 abstract 1
- 239000011347 resin Substances 0.000 abstract 1
- 229920005989 resin Polymers 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
- C23C18/18—Pretreatment of the material to be coated
- C23C18/20—Pretreatment of the material to be coated of organic surfaces, e.g. resins
- C23C18/2006—Pretreatment of the material to be coated of organic surfaces, e.g. resins by other methods than those of C23C18/22 - C23C18/30
- C23C18/2046—Pretreatment of the material to be coated of organic surfaces, e.g. resins by other methods than those of C23C18/22 - C23C18/30 by chemical pretreatment
- C23C18/2053—Pretreatment of the material to be coated of organic surfaces, e.g. resins by other methods than those of C23C18/22 - C23C18/30 by chemical pretreatment only one step pretreatment
- C23C18/206—Use of metal other than noble metals and tin, e.g. activation, sensitisation with metals
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/18—Materials not provided for elsewhere for application to surfaces to minimize adherence of ice, mist or water thereto; Thawing or antifreeze materials for application to surfaces
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
- C23C18/18—Pretreatment of the material to be coated
- C23C18/20—Pretreatment of the material to be coated of organic surfaces, e.g. resins
- C23C18/28—Sensitising or activating
- C23C18/285—Sensitising or activating with tin based compound or composition
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
- D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
- D06M11/20—Halides of elements of Groups 4 or 14 of the Periodic Table, e.g. zirconyl chloride
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Textile Engineering (AREA)
- Combustion & Propulsion (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Treatments Of Macromolecular Shaped Articles (AREA)
- Coloring (AREA)
- Detergent Compositions (AREA)
Abstract
The wettability of hydrophobic solid surfaces of synthetic polymeric substances relative to aqueous fluids is increased by applying to the surface at 15-35 DEG C or incorporating in at least the layer adjacent to the surface, at least one inorganic salt of germanium, tin, lead, titanium, zirconium, hafnium or thorium. The salt may be applied to the surface in aqueous solution, which may contain a detergent, or as a solution in an organic solvent e.g. an alcohol, ketone, ester, ether, or amine, which may also contain an inorganic or organic acid, e.g. tartaric or sulphaminic acids, or as a solution in a water/organic solvent mixture. A solvent may be used which has a solvating action upon the surface, and the surface may be electrically charged before application of the salt. Alternatively, solid salt may be scattered upon the surface, which is then heated to a temperature in the region of the melting point of the polymer, or incorporated in a moulding composition of the polymer. In an Example, nylon fabric is immersed in an aqueous detergent solution of stannous chloride and zirconium oxychloride, rinsed with water and dried.ALSO:The wettability of hydrophobic solid surfaces of synthetic polymeric substances relative to aqueous fluids is increased by applying to the surface at 15 - 35 DEG C, or incorporating in at least the layer adjacent to the surface, at least one inorganic salt of germanium, tin, lead, titanium, zirconium, bafnium or thorium. The salt may be applied to the surface in aqueous solution, which may contain a detergent, or as a solution in an organic solvent e.g. an alcohol, ketone, ester, ether, or amine, which may also contain an inorganic or organic acid, e.g. tartaric or sulphaminic acids, or as a solution in a water/organic solvent mixture. A solvent may be used which has a solvating action upon the surface, and the surface may be electrically charged before application of the salt. Alternatively, solid salt may be scattered upon the surface, which is then heated to a temperature in the region of the melting point of the polymer, or incorporated in a moulding composition of the polymer. In Examples (1) polystyrene film is immersed in an aqueous solution of SnCl2, TiCl3 and detergent, rinsed with water and dried; (2) polypropylene film is immersed in an aqueous solution of zirconium oxychloride, TiCl3 and detergent, and rinsed with 1NNaOH and then with water, (3) nylon fabric is treated as in (1) with an aqueous detergent solution of stannous chloride and zirconium oxychloride; (4) a moulded article of vinyl formaldehyde resin is treated as in (1) with an aqueous solution containing SnCl2, lead acetate, hydrochloric acid and detergent; (5) polystyrene film is immersed in aqueous detergent containing zirconium oxychloride, and then rinsed in 1NNaOH; (6) polypropylene film is treated as in (1) with an aqueous solution containing germanium dichloride, hydrochloric acid and detergent; (7) polypropylene film is immersed in a solution of stannous chloride in propylene glycol; (8) polystyrene film is immersed in a solution of stannous chloride in acetone. Surfaces of polymeric materials such as polypropylene and polyethylene thus treated show improved wettability with respect to printing inks.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH883963A CH403708A (en) | 1963-07-16 | 1963-07-16 | Process for making textile materials wettable |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1079391A true GB1079391A (en) | 1967-08-16 |
Family
ID=4345325
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2832064A Expired GB1079391A (en) | 1963-07-16 | 1964-07-09 | Process for increasing the wettability of difficult to wet surfaces |
Country Status (3)
| Country | Link |
|---|---|
| CH (1) | CH403708A (en) |
| DE (1) | DE1519547A1 (en) |
| GB (1) | GB1079391A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4139660A (en) * | 1963-07-16 | 1979-02-13 | Bernhard Joos | Method for increasing solid surface tension |
| EP0164617A1 (en) * | 1984-05-28 | 1985-12-18 | Hoechst Aktiengesellschaft | Process for increasing the wettability of surfaces of plastic substancesfor chemical engineering applications |
| US9453197B2 (en) | 2010-12-16 | 2016-09-27 | General Electric Company | Methods of making cell carrier |
| US9453196B2 (en) | 2010-12-16 | 2016-09-27 | General Electric Company | Cell carrier, methods of making and use |
| US9518249B2 (en) | 2010-12-16 | 2016-12-13 | General Electric Company | Cell carrier, associated methods for making cell carrier and culturing cells using the same |
| US9534206B2 (en) | 2010-12-16 | 2017-01-03 | General Electric Company | Cell carrier, associated methods for making cell carrier and culturing cells using the same |
| US9926523B2 (en) | 2010-12-16 | 2018-03-27 | General Electric Company | Cell carriers and methods for culturing cells |
-
1963
- 1963-07-16 CH CH883963A patent/CH403708A/en unknown
-
1964
- 1964-07-09 GB GB2832064A patent/GB1079391A/en not_active Expired
- 1964-07-11 DE DE19641519547 patent/DE1519547A1/en active Granted
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4139660A (en) * | 1963-07-16 | 1979-02-13 | Bernhard Joos | Method for increasing solid surface tension |
| EP0164617A1 (en) * | 1984-05-28 | 1985-12-18 | Hoechst Aktiengesellschaft | Process for increasing the wettability of surfaces of plastic substancesfor chemical engineering applications |
| US4617197A (en) * | 1984-05-28 | 1986-10-14 | Hoechst Aktiengesellschaft | Process for improving the wetting characteristics of the surface of shaped plastics articles for applications in chemical engineering |
| US9453197B2 (en) | 2010-12-16 | 2016-09-27 | General Electric Company | Methods of making cell carrier |
| US9453196B2 (en) | 2010-12-16 | 2016-09-27 | General Electric Company | Cell carrier, methods of making and use |
| US9518249B2 (en) | 2010-12-16 | 2016-12-13 | General Electric Company | Cell carrier, associated methods for making cell carrier and culturing cells using the same |
| US9534206B2 (en) | 2010-12-16 | 2017-01-03 | General Electric Company | Cell carrier, associated methods for making cell carrier and culturing cells using the same |
| US9926523B2 (en) | 2010-12-16 | 2018-03-27 | General Electric Company | Cell carriers and methods for culturing cells |
| US9957478B2 (en) | 2010-12-16 | 2018-05-01 | General Electric Company | Cell carrier, associated methods for making cell carrier and culturing cells using the same |
Also Published As
| Publication number | Publication date |
|---|---|
| DE1519547B2 (en) | 1973-12-20 |
| CH403708A (en) | 1966-06-15 |
| DE1519547A1 (en) | 1970-03-12 |
| DE1519547C3 (en) | 1974-07-18 |
| CH883963A4 (en) | 1965-08-31 |
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