GB1071184A - Improvements in the production of bonded granular objects - Google Patents

Improvements in the production of bonded granular objects

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Publication number
GB1071184A
GB1071184A GB2863864A GB2863864A GB1071184A GB 1071184 A GB1071184 A GB 1071184A GB 2863864 A GB2863864 A GB 2863864A GB 2863864 A GB2863864 A GB 2863864A GB 1071184 A GB1071184 A GB 1071184A
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GB
United Kingdom
Prior art keywords
alumina
weight
oxide
mesh screen
metals
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2863864A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US294266A external-priority patent/US3296002A/en
Priority claimed from US294238A external-priority patent/US3244539A/en
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Publication of GB1071184A publication Critical patent/GB1071184A/en
Expired legal-status Critical Current

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Abstract

Bonded granular material is prepared by mixing 6-50% by weight of particles of aluminium, or an alloy containing a major proportion of Al, which can pass through an 80-mesh screen (U.S. Sieve series), with at least 0.02% (on the weight of the Al) of fluxing agent and alumina particles (at least 50% by weight of which pass through a 4 mesh screen and are retained on a 100 mesh screen), shaping into a porous body of porosity at least 20% after removal of volatile materials, firing the body in an oxidizing atmosphere, e.g. air, oxygen or a mixture of oxygen and inert gas, at 650-1700 DEG C. for a time sufficient to oxidize at least 40% by weight of Al, the rate of heating being controlled so that the temperature of the body never exceeds the ambient temperature by more than 100 DEG C. The mixture to be shaped may also contain a bonding agent, e.g. ethyl alcohol, ethylene glycol, acetone solutions of carboxy-methyl cellulose, rubber, gum arabic, polyvinyl alcohol and natural glue, which burn off in the firing process. The fluxing agent may be oxides of the alkali metals, the alkaline earth metals, V, Cr, Mo, W, Cu, Ag, Zn, Sb, Bi and precursors of these oxides, i.e. acetates, benzoates, bisulphates, bisulphites, bromates, nitrates, silicates, sulphates, sulphites, or thiosulphites of the metals. The shaped refractory resulting from this process comprises 30-89% by weight of alumina particles bonded by a porous in situ oxidized crystalline phase of alpha-alumina, a compound of alumina with at least one other oxide, or a solid solution of an oxide in alumina or in said compound formed between an oxide and alumina, the bonding phase containing at least 72% Al2O3 by analysis. Reference has been directed by the Comptroller to Specification 989,005.
GB2863864A 1963-07-11 1964-07-10 Improvements in the production of bonded granular objects Expired GB1071184A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US294266A US3296002A (en) 1963-07-11 1963-07-11 Refractory shapes
US294238A US3244539A (en) 1963-07-11 1963-07-11 Bonded alumina refractory

Publications (1)

Publication Number Publication Date
GB1071184A true GB1071184A (en) 1967-06-07

Family

ID=26968417

Family Applications (2)

Application Number Title Priority Date Filing Date
GB2863864A Expired GB1071184A (en) 1963-07-11 1964-07-10 Improvements in the production of bonded granular objects
GB2863964A Expired GB1071185A (en) 1963-07-11 1964-07-10 Improvements relating to refractories

Family Applications After (1)

Application Number Title Priority Date Filing Date
GB2863964A Expired GB1071185A (en) 1963-07-11 1964-07-10 Improvements relating to refractories

Country Status (3)

Country Link
JP (2) JPS4826363B1 (en)
BE (1) BE650167A (en)
GB (2) GB1071184A (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3751682B2 (en) * 1995-06-19 2006-03-01 日本特殊陶業株式会社 Igniter plug
DE19704910C2 (en) * 1997-02-10 2000-07-06 Bayer Ag Liquid-phase sintered, electrically conductive and oxidation-resistant ceramic material, a process for its production and its use

Also Published As

Publication number Publication date
BE650167A (en) 1964-11-03
JPS4826364B1 (en) 1973-08-09
JPS4826363B1 (en) 1973-08-09
GB1071185A (en) 1967-06-07

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