GB1017306A - Improvements relating to the hydrocatalytic refining of lubricating oils - Google Patents

Improvements relating to the hydrocatalytic refining of lubricating oils

Info

Publication number
GB1017306A
GB1017306A GB9257/63A GB925763A GB1017306A GB 1017306 A GB1017306 A GB 1017306A GB 9257/63 A GB9257/63 A GB 9257/63A GB 925763 A GB925763 A GB 925763A GB 1017306 A GB1017306 A GB 1017306A
Authority
GB
United Kingdom
Prior art keywords
catalyst
oil
hydrogen
refining
lubricating oils
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB9257/63A
Inventor
Alfred Champagnat
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BP PLC
Original Assignee
BP PLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BP PLC filed Critical BP PLC
Publication of GB1017306A publication Critical patent/GB1017306A/en
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/88—Molybdenum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/20—Sulfiding
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
    • C10G2400/10—Lubricating oil

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Catalysts (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

In a method of activating a catalyst for the hydrocatalytic refining of lubricating oils which catalysts comprise Fe and Mo oxides and optionally also CoO, the catalyst is contacted at a temperature of at least 300 DEG C. in the presence of hydrogen with from 80 to 120 kg. of CS2 per metric ton of catalyst. In an example a catalyst containing Fe2O3, MoO3, CoO and Al2O3 was subject to treatment with (1) white oil of specified physical characteristics, (2) the same white oil containing 3% CS2 and (3) a Middle East spindle oil known to be effective for activation, under the following conditions: temp. 350 DEG C.; S.V.=1 /v.v/hr.; pressure 20 kg./cm.2. Flow rate of hydrogen= 20 v./v./hr. Time=48 hours. Comparative results of refining the same oil are set forth at a variety of temperatures.ALSO:Catalysts containing oxides of Fe, Mo (and optionally Co) on Al2O3 are activated at a temperature of at least 300 DEG C. in the presence of hydrogen with from 80-120 Kg. of CS2 per metric ton of catalyst. Preferably the CS2 is brought into contact with the catalyst in a carrier oil which does not itself activate the catalyst. Examples are given.
GB9257/63A 1962-04-10 1963-03-08 Improvements relating to the hydrocatalytic refining of lubricating oils Expired GB1017306A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR893991A FR1328373A (en) 1962-04-10 1962-04-10 Improvements relating to hydrocatalytic refining of lubricating oils

Publications (1)

Publication Number Publication Date
GB1017306A true GB1017306A (en) 1966-01-19

Family

ID=8776548

Family Applications (1)

Application Number Title Priority Date Filing Date
GB9257/63A Expired GB1017306A (en) 1962-04-10 1963-03-08 Improvements relating to the hydrocatalytic refining of lubricating oils

Country Status (6)

Country Link
US (1) US3245903A (en)
AT (1) AT242270B (en)
BE (1) BE630732A (en)
FR (1) FR1328373A (en)
GB (1) GB1017306A (en)
NL (1) NL291168A (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3369999A (en) * 1964-12-08 1968-02-20 Gulf Research Development Co Clay finishing of catalytically hydrofinished lubricating oils
US3340181A (en) * 1965-08-05 1967-09-05 Chevron Res Two-stage hydrotreatment for white oil manufacture
US3948763A (en) * 1972-09-27 1976-04-06 Gulf Research & Development Company Sulfiding process for desulfurization catalysts
US4514517A (en) * 1983-07-29 1985-04-30 Exxon Research And Engineering Co. Supported, self-promoted molybdenum and tungsten sulfide catalysts formed from bis(tetrathiometallate) precursors, and their preparation
US4510260A (en) * 1983-07-29 1985-04-09 Exxon Research And Engineering Co. Self-promoted molybdenum and tungsten sulfide hydrotreating catalysts from bis(tetrathiometallate) precursors
US4839326A (en) * 1985-04-22 1989-06-13 Exxon Research And Engineering Company Promoted molybdenum and tungsten sulfide catalysts, their preparation and use

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3020228A (en) * 1958-05-02 1962-02-06 British Petrolcum Company Ltd Upgrading lubricating oils by hydrogenation with a three component catalyst
US2998377A (en) * 1958-08-04 1961-08-29 Gulf Research Development Co Process for decolorizing petroleum ceresin
NL125742C (en) * 1959-02-04
US3078221A (en) * 1959-07-24 1963-02-19 Gulf Research Development Co Hydrogenation process for preparation of lubricating oils
US3072564A (en) * 1959-12-28 1963-01-08 Exxon Research Engineering Co Hydrofining process

Also Published As

Publication number Publication date
US3245903A (en) 1966-04-12
NL291168A (en)
FR1328373A (en) 1963-05-31
AT242270B (en) 1965-09-10
BE630732A (en)

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