FR3122488B1 - Procédé et appareil de séparation d’un débit riche en dioxyde de carbone par distillation pour produire du dioxyde de carbone liquide - Google Patents

Procédé et appareil de séparation d’un débit riche en dioxyde de carbone par distillation pour produire du dioxyde de carbone liquide Download PDF

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Publication number
FR3122488B1
FR3122488B1 FR2104519A FR2104519A FR3122488B1 FR 3122488 B1 FR3122488 B1 FR 3122488B1 FR 2104519 A FR2104519 A FR 2104519A FR 2104519 A FR2104519 A FR 2104519A FR 3122488 B1 FR3122488 B1 FR 3122488B1
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France
Prior art keywords
carbon dioxide
fraction
distillation
pressure
separating
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR2104519A
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English (en)
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FR3122488A1 (fr
Inventor
Michael Tran
Mathieu Leclerc
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
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Application filed by Air Liquide SA, LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude filed Critical Air Liquide SA
Priority to FR2104519A priority Critical patent/FR3122488B1/fr
Priority to EP22711976.5A priority patent/EP4330612A1/fr
Priority to AU2022267658A priority patent/AU2022267658B2/en
Priority to CA3211119A priority patent/CA3211119A1/fr
Priority to PCT/EP2022/056139 priority patent/WO2022228764A1/fr
Publication of FR3122488A1 publication Critical patent/FR3122488A1/fr
Application granted granted Critical
Publication of FR3122488B1 publication Critical patent/FR3122488B1/fr
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Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0266—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of carbon dioxide
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/08—Separating gaseous impurities from gases or gaseous mixtures or from liquefied gases or liquefied gaseous mixtures
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/02—Processes or apparatus using separation by rectification in a single pressure main column system
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/70—Refluxing the column with a condensed part of the feed stream, i.e. fractionator top is stripped or self-rectified
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/30—Processes or apparatus using other separation and/or other processing means using a washing, e.g. "scrubbing" or bubble column for purification purposes
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2210/00—Processes characterised by the type or other details of the feed stream
    • F25J2210/04—Mixing or blending of fluids with the feed stream
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2210/00—Processes characterised by the type or other details of the feed stream
    • F25J2210/06—Splitting of the feed stream, e.g. for treating or cooling in different ways
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2215/00—Processes characterised by the type or other details of the product stream
    • F25J2215/04—Recovery of liquid products
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2215/00—Processes characterised by the type or other details of the product stream
    • F25J2215/80—Carbon dioxide
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2220/00—Processes or apparatus involving steps for the removal of impurities
    • F25J2220/80—Separating impurities from carbon dioxide, e.g. H2O or water-soluble contaminants
    • F25J2220/82—Separating low boiling, i.e. more volatile components, e.g. He, H2, CO, Air gases, CH4
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2235/00—Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams
    • F25J2235/80—Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams the fluid being carbon dioxide
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2245/00—Processes or apparatus involving steps for recycling of process streams
    • F25J2245/02—Recycle of a stream in general, e.g. a by-pass stream
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2280/00—Control of the process or apparatus
    • F25J2280/02—Control in general, load changes, different modes ("runs"), measurements

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Titre : Procédé et appareil de séparation d’un débit riche en dioxyde de carbone par distillation pour produire du dioxyde de carbone liquide Dans un procédé de séparation d’un débit (0) contenant au moins 95% mol de dioxyde de carbone ainsi qu’au moins une impureté plus légère que le dioxyde de carbone par distillation, on refroidit le débit (1) jusqu’à une première température intermédiaire entre celles du bout froid et du bout chaud d’un moyen d’échange de chaleur (10) pour former un débit liquide à une première température et à une première pression et on le divise en au moins deux pour former une première fraction (7) et une deuxième fraction (9), on détend la première fraction jusqu’à la pression d’une colonne de distillation (20) appelée deuxième pression, inférieure à la première pression et on l’envoie à un niveau intermédiaire de la colonne de distillation, on refroidit la deuxième fraction dans le moyen d’échange de chaleur jusqu’au bout froid de celui-ci, on la détend jusqu’à la pression de la colonne de distillation et on l’envoie à un niveau de la colonne de distillation au-dessus du point d’arrivée de la première fraction, on soutire en cuve de la colonne un débit liquide contenant au moins 99% mol de dioxyde de carbone et une fraction (3) du débit liquide est pressurisée dans une pompe (P1) et envoyée en tête de la colonne. Figure de l’abrégé : Fig. 1
FR2104519A 2021-04-29 2021-04-29 Procédé et appareil de séparation d’un débit riche en dioxyde de carbone par distillation pour produire du dioxyde de carbone liquide Active FR3122488B1 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
FR2104519A FR3122488B1 (fr) 2021-04-29 2021-04-29 Procédé et appareil de séparation d’un débit riche en dioxyde de carbone par distillation pour produire du dioxyde de carbone liquide
EP22711976.5A EP4330612A1 (fr) 2021-04-29 2022-03-10 Procédé et appareil de séparation d'un débit riche en dioxyde de carbone par distillation pour produire du dioxyde de carbone liquide
AU2022267658A AU2022267658B2 (en) 2021-04-29 2022-03-10 Method and apparatus for separating a flow rich in carbon dioxide by distillation to produce liquid carbon dioxide
CA3211119A CA3211119A1 (fr) 2021-04-29 2022-03-10 Procede et appareil de separation d'un debit riche en dioxyde de carbone par distillation pour produire du dioxyde de carbone liquide
PCT/EP2022/056139 WO2022228764A1 (fr) 2021-04-29 2022-03-10 Procédé et appareil de séparation d'un débit riche en dioxyde de carbone par distillation pour produire du dioxyde de carbone liquide

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR2104519A FR3122488B1 (fr) 2021-04-29 2021-04-29 Procédé et appareil de séparation d’un débit riche en dioxyde de carbone par distillation pour produire du dioxyde de carbone liquide
FR2104519 2021-04-29

Publications (2)

Publication Number Publication Date
FR3122488A1 FR3122488A1 (fr) 2022-11-04
FR3122488B1 true FR3122488B1 (fr) 2023-03-17

Family

ID=76284000

Family Applications (1)

Application Number Title Priority Date Filing Date
FR2104519A Active FR3122488B1 (fr) 2021-04-29 2021-04-29 Procédé et appareil de séparation d’un débit riche en dioxyde de carbone par distillation pour produire du dioxyde de carbone liquide

Country Status (5)

Country Link
EP (1) EP4330612A1 (fr)
AU (1) AU2022267658B2 (fr)
CA (1) CA3211119A1 (fr)
FR (1) FR3122488B1 (fr)
WO (1) WO2022228764A1 (fr)

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3700679A (en) 1970-06-08 1972-10-24 Hoffmann La Roche Nuclear substituted derivatives of 1-hydroxy-6-methoxyphenazine 5,10-dioxide
JPS5520206A (en) * 1978-07-24 1980-02-13 Showa Tansan Kk Manufacture of saturated liquefied carbon dioxide
US8337587B2 (en) * 2008-05-20 2012-12-25 Lummus Technology Inc. Carbon dioxide purification
FR2975478B1 (fr) * 2011-05-18 2015-05-15 Air Liquide Procede et appareil de liquefaction d'un debit gazeux riche en dioxyde de carbone
CA2984085C (fr) * 2016-11-01 2019-04-09 Jason Michael Ploeger Recuperation d'helium a partir de flux renfermant de l'helium, du dioxyde de carbone et au moins un de l'azote et du methane
US20200318897A1 (en) * 2017-10-11 2020-10-08 Jianguo Xu CO2 Removal or Capture from CO2-rich Gas Mixtures

Also Published As

Publication number Publication date
AU2022267658B2 (en) 2024-03-21
WO2022228764A1 (fr) 2022-11-03
AU2022267658A1 (en) 2023-09-28
EP4330612A1 (fr) 2024-03-06
FR3122488A1 (fr) 2022-11-04
CA3211119A1 (fr) 2022-11-03

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