FR3093169B1 - Installation et procédé de séparation des gaz de l’air mettant en œuvre un adsorbeur de forme parallélépipèdique - Google Patents

Installation et procédé de séparation des gaz de l’air mettant en œuvre un adsorbeur de forme parallélépipèdique Download PDF

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Publication number
FR3093169B1
FR3093169B1 FR1901732A FR1901732A FR3093169B1 FR 3093169 B1 FR3093169 B1 FR 3093169B1 FR 1901732 A FR1901732 A FR 1901732A FR 1901732 A FR1901732 A FR 1901732A FR 3093169 B1 FR3093169 B1 FR 3093169B1
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Prior art keywords
air flow
air
installation
parallelepiped shaped
faces
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FR1901732A
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English (en)
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FR3093169A1 (fr
Inventor
BENOîT DAVIDIAN
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
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Priority to FR1901732A priority Critical patent/FR3093169B1/fr
Application filed by Air Liquide SA, LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude filed Critical Air Liquide SA
Priority to BR112021015733-6A priority patent/BR112021015733A2/pt
Priority to US17/432,897 priority patent/US20220196326A1/en
Priority to EP20710577.6A priority patent/EP3928043A1/fr
Priority to PCT/FR2020/050253 priority patent/WO2020169900A1/fr
Priority to CA3129477A priority patent/CA3129477A1/fr
Priority to CN202080013373.6A priority patent/CN113424004B/zh
Priority to AU2020225422A priority patent/AU2020225422A1/en
Publication of FR3093169A1 publication Critical patent/FR3093169A1/fr
Application granted granted Critical
Publication of FR3093169B1 publication Critical patent/FR3093169B1/fr
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Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151—Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04163—Hot end purification of the feed air
    • F25J3/04169—Hot end purification of the feed air by adsorption of the impurities
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/0407—Constructional details of adsorbing systems
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/0462—Temperature swing adsorption
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763—Start-up or control of the process; Details of the apparatus used
    • F25J3/04769—Operation, control and regulation of the process; Instrumentation within the process
    • F25J3/04775—Air purification and pre-cooling
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763—Start-up or control of the process; Details of the apparatus used
    • F25J3/04866—Construction and layout of air fractionation equipments, e.g. valves, machines
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/50—Carbon oxides
    • B01D2257/504—Carbon dioxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2258/00—Sources of waste gases
    • B01D2258/06—Polluted air
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/60—Processes or apparatus using other separation and/or other processing means using adsorption on solid adsorbents, e.g. by temperature-swing adsorption [TSA] at the hot or cold end
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00—Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/12—Particular process parameters like pressure, temperature, ratios
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02C—CAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
    • Y02C20/00—Capture or disposal of greenhouse gases
    • Y02C20/40—Capture or disposal of greenhouse gases of CO2

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Separation By Low-Temperature Treatments (AREA)

Abstract

Installation de séparation des gaz de l’air comprenant dans le sens de circulation du flux d’air : un moyen de compression (C) permettant de comprimer le flux d’air à une pression P1 comprise entre 1,15 bar abs et 2 bar abs, une unité d’adsorption de type TSA (A), et une unité de distillation cryogénique (D), avec l’unité d’adsorption comprenant au moins deux adsorbeurs A1 et A2 présentant chacun une enveloppe de forme parallélépipèdique disposée horizontalement et comprenant : une entrée et une sortie du flux d’air, deux masses adsorbantes en lit fixe présentant chacune une forme également parallélépipédique dont les faces sont parallèles aux faces de l’enveloppe, et un ensemble de volumes permettant que la traversée des deux masses adsorbantes par le flux d’air s’effectue horizontalement, en parallèle, sur toute la section de chacune des masses adsorbantes et sur toutes leurs épaisseurs. Figure de l’abrégé : Fig. 2
FR1901732A 2019-02-21 2019-02-21 Installation et procédé de séparation des gaz de l’air mettant en œuvre un adsorbeur de forme parallélépipèdique Active FR3093169B1 (fr)

Priority Applications (8)

Application Number Priority Date Filing Date Title
FR1901732A FR3093169B1 (fr) 2019-02-21 2019-02-21 Installation et procédé de séparation des gaz de l’air mettant en œuvre un adsorbeur de forme parallélépipèdique
US17/432,897 US20220196326A1 (en) 2019-02-21 2020-02-12 Plant and process for aerial gas separation using a parallelepipedal adsorber
EP20710577.6A EP3928043A1 (fr) 2019-02-21 2020-02-12 Installation et procédé de séparation des gaz de l'air mettant en oeuvre un adsorbeur de forme parallélépipédique
PCT/FR2020/050253 WO2020169900A1 (fr) 2019-02-21 2020-02-12 Installation et procédé de séparation des gaz de l'air mettant en œuvre un adsorbeur de forme parallélépipédique
BR112021015733-6A BR112021015733A2 (pt) 2019-02-21 2020-02-12 Usina e processo para separação de gás aéreo com o uso de um adsorvedor paralelepipedal
CA3129477A CA3129477A1 (fr) 2019-02-21 2020-02-12 Installation et procede de separation des gaz de l'air mettant en ƒuvre un adsorbeur de forme parallelepipedique
CN202080013373.6A CN113424004B (zh) 2019-02-21 2020-02-12 使用平行六面体吸附器分离空气中所含气体的设备和方法
AU2020225422A AU2020225422A1 (en) 2019-02-21 2020-02-12 Plant and process for aerial gas separation using a parallelepipedal adsorber

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1901732A FR3093169B1 (fr) 2019-02-21 2019-02-21 Installation et procédé de séparation des gaz de l’air mettant en œuvre un adsorbeur de forme parallélépipèdique
FR1901732 2019-02-21

Publications (2)

Publication Number Publication Date
FR3093169A1 FR3093169A1 (fr) 2020-08-28
FR3093169B1 true FR3093169B1 (fr) 2021-01-22

Family

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FR1901732A Active FR3093169B1 (fr) 2019-02-21 2019-02-21 Installation et procédé de séparation des gaz de l’air mettant en œuvre un adsorbeur de forme parallélépipèdique

Country Status (8)

Country Link
US (1) US20220196326A1 (fr)
EP (1) EP3928043A1 (fr)
CN (1) CN113424004B (fr)
AU (1) AU2020225422A1 (fr)
BR (1) BR112021015733A2 (fr)
CA (1) CA3129477A1 (fr)
FR (1) FR3093169B1 (fr)
WO (1) WO2020169900A1 (fr)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3093009B1 (fr) * 2019-02-21 2021-07-23 Air Liquide Procédé et installation de purification d’un flux gazeux de débit élevé
FR3093008B1 (fr) * 2019-02-21 2021-01-22 Air Liquide Installation et procédé de séparation des gaz de l’air à basse pression
FR3128776A3 (fr) 2021-10-28 2023-05-05 L'air Liquide Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Procédé et appareil de séparation d’air par distillation cryogénique

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4049406A (en) * 1976-04-23 1977-09-20 American Air Filter Company, Inc. Fluid filter housing and assembly
FR2667800B1 (fr) * 1990-10-11 1992-12-04 Air Liquide Procede de separation par adsorption, et adsorbeur.
FR2744795B1 (fr) 1996-02-12 1998-06-05 Grenier Maurice Procede et installation de production d'oxygene gazeux sous haute pression
FR2798075B1 (fr) 1999-09-03 2001-11-09 Air Liquide Conduite d'un systeme de purification d'air a regeneration thermique
WO2003101587A1 (fr) * 2002-05-31 2003-12-11 Praxair Technology, Inc. Production de gaz de haute purete et d'ultra-haute purete
FR2856607B1 (fr) * 2003-06-27 2006-08-18 Air Liquide Procede de purification d'air par cycle tsa accelere
US20050217481A1 (en) 2004-03-31 2005-10-06 Dunne Stephen R Rotary adsorbent contactors for drying, purification and separation of gases
FR2949846B1 (fr) * 2009-09-10 2012-02-10 Air Liquide Procede et installation de production d'oxygene par distillation d'air
US8647409B2 (en) * 2012-05-24 2014-02-11 Praxair Technology, Inc. Air compression system and method
FR3019060B1 (fr) * 2014-03-28 2017-12-08 L'air Liquide Sa Pour L'etude Et L'exploitation Des Procedes Georges Claude Installation et procede de purification par adsorption d'un flux gazeux comprenant une impurete corrosive
FR3024376B1 (fr) * 2014-08-01 2020-07-17 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Adsorbeur avec secheur rotatif
DE102015002260A1 (de) * 2015-02-25 2016-08-25 Linde Aktiengesellschaft Verfahren zum Herstellen eines horizontal durchströmten Adsorbers und Trennwandmodul zur Verwendung in diesem Verfahren
FR3052243B1 (fr) * 2016-06-06 2019-06-28 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Assemblage d'elements modulaires de construction d'un appareil d'echange de masse et/ou de chaleur et procede d'echange utilisant un assemblage

Also Published As

Publication number Publication date
WO2020169900A1 (fr) 2020-08-27
FR3093169A1 (fr) 2020-08-28
CN113424004B (zh) 2022-12-13
US20220196326A1 (en) 2022-06-23
AU2020225422A1 (en) 2021-09-09
CN113424004A (zh) 2021-09-21
CA3129477A1 (fr) 2020-08-27
BR112021015733A2 (pt) 2021-10-26
EP3928043A1 (fr) 2021-12-29

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