FR3083231B1 - Procede de production de paraxylene utilisant une etape en lit mobile simule, et une etape de fractionnement de deux fractions - Google Patents
Procede de production de paraxylene utilisant une etape en lit mobile simule, et une etape de fractionnement de deux fractions Download PDFInfo
- Publication number
- FR3083231B1 FR3083231B1 FR1856049A FR1856049A FR3083231B1 FR 3083231 B1 FR3083231 B1 FR 3083231B1 FR 1856049 A FR1856049 A FR 1856049A FR 1856049 A FR1856049 A FR 1856049A FR 3083231 B1 FR3083231 B1 FR 3083231B1
- Authority
- FR
- France
- Prior art keywords
- desorbent
- fractions
- fraction
- ethylbenzene
- paraxylene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- URLKBWYHVLBVBO-UHFFFAOYSA-N Para-Xylene Chemical compound CC1=CC=C(C)C=C1 URLKBWYHVLBVBO-UHFFFAOYSA-N 0.000 title abstract 6
- 238000000034 method Methods 0.000 title abstract 3
- 238000005194 fractionation Methods 0.000 title abstract 2
- VJYFKVYYMZPMAB-UHFFFAOYSA-N ethoprophos Chemical compound CCCSP(=O)(OCC)SCCC VJYFKVYYMZPMAB-UHFFFAOYSA-N 0.000 title 1
- YNQLUTRBYVCPMQ-UHFFFAOYSA-N Ethylbenzene Chemical compound CCC1=CC=CC=C1 YNQLUTRBYVCPMQ-UHFFFAOYSA-N 0.000 abstract 8
- IVSZLXZYQVIEFR-UHFFFAOYSA-N m-xylene Chemical group CC1=CC=CC(C)=C1 IVSZLXZYQVIEFR-UHFFFAOYSA-N 0.000 abstract 6
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical group CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 abstract 4
- 238000004821 distillation Methods 0.000 abstract 2
- 238000000926 separation method Methods 0.000 abstract 2
- 239000008096 xylene Substances 0.000 abstract 2
- 150000003738 xylenes Chemical class 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- 229910021536 Zeolite Inorganic materials 0.000 abstract 1
- 239000003463 adsorbent Substances 0.000 abstract 1
- 150000001491 aromatic compounds Chemical class 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract 1
- 229930195733 hydrocarbon Natural products 0.000 abstract 1
- 150000002430 hydrocarbons Chemical class 0.000 abstract 1
- 238000002347 injection Methods 0.000 abstract 1
- 239000007924 injection Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000010457 zeolite Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/005—Processes comprising at least two steps in series
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
- B01D15/1814—Recycling of the fraction to be distributed
- B01D15/1821—Simulated moving beds
- B01D15/1828—Simulated moving beds characterised by process features
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
- B01D15/1814—Recycling of the fraction to be distributed
- B01D15/1821—Simulated moving beds
- B01D15/185—Simulated moving beds characterised by the components to be separated
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
- C07C15/02—Monocyclic hydrocarbons
- C07C15/067—C8H10 hydrocarbons
- C07C15/08—Xylenes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
- C07C5/22—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by isomerisation
- C07C5/27—Rearrangement of carbon atoms in the hydrocarbon skeleton
- C07C5/2767—Changing the number of side-chains
- C07C5/277—Catalytic processes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/04—Purification; Separation; Use of additives by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
- C07C7/13—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers by molecular-sieve technique
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Water Supply & Treatment (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Sustainable Development (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1856049A FR3083231B1 (fr) | 2018-06-29 | 2018-06-29 | Procede de production de paraxylene utilisant une etape en lit mobile simule, et une etape de fractionnement de deux fractions |
| KR1020207036182A KR102773808B1 (ko) | 2018-06-29 | 2019-06-21 | 유사 이동층 단계, 및 2 섹션 칼럼에서 2개의 분획을 분별하는 단계를 사용하여 파라자일렌을 제조하는 방법 |
| JP2020572983A JP7361057B2 (ja) | 2018-06-29 | 2019-06-21 | 疑似移動床段階を用いてパラキシレンを製造する方法、及び、一の２セクションカラムにおける二の留分の分留段階 |
| EP19731299.4A EP3814307B1 (fr) | 2018-06-29 | 2019-06-21 | Procede de production de paraxylene utilisant une etape en lit mobile simule, et une etape de fractionnement de deux fractions dans une colonnes de 2 coupes |
| US17/256,290 US11242302B2 (en) | 2018-06-29 | 2019-06-21 | Method for producing paraxylene using a simulated moving-bed step, and a step of fractionating two fractions in a two-section column |
| CN201980043987.6A CN112585107B (zh) | 2018-06-29 | 2019-06-21 | 使用模拟移动床步骤和在双馏份塔中分级两个级分的步骤生产对二甲苯的方法 |
| PCT/EP2019/066445 WO2020002142A1 (fr) | 2018-06-29 | 2019-06-21 | Procede de production de paraxylene utilisant une etape en lit mobile simule, et une etape de fractionnement de deux fractions dans une colonnes de 2 coupes |
| PT197312994T PT3814307T (pt) | 2018-06-29 | 2019-06-21 | Processo para a produção de paraxileno utilizando uma fase em leito móvel simulado, e uma fase de fracionamento de duas frações numa coluna de cortes |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1856049A FR3083231B1 (fr) | 2018-06-29 | 2018-06-29 | Procede de production de paraxylene utilisant une etape en lit mobile simule, et une etape de fractionnement de deux fractions |
| FR1856049 | 2018-06-29 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR3083231A1 FR3083231A1 (fr) | 2020-01-03 |
| FR3083231B1 true FR3083231B1 (fr) | 2020-07-17 |
Family
ID=63312144
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR1856049A Expired - Fee Related FR3083231B1 (fr) | 2018-06-29 | 2018-06-29 | Procede de production de paraxylene utilisant une etape en lit mobile simule, et une etape de fractionnement de deux fractions |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US11242302B2 (enExample) |
| EP (1) | EP3814307B1 (enExample) |
| JP (1) | JP7361057B2 (enExample) |
| KR (1) | KR102773808B1 (enExample) |
| CN (1) | CN112585107B (enExample) |
| FR (1) | FR3083231B1 (enExample) |
| PT (1) | PT3814307T (enExample) |
| WO (1) | WO2020002142A1 (enExample) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11673848B2 (en) * | 2020-02-27 | 2023-06-13 | Exxonmobil Chemical Patents Inc. | Xylene separation processes using a membrane separator |
| CN112843788B (zh) * | 2021-01-19 | 2022-10-28 | 温州大学新材料与产业技术研究院 | 一种采用流动相独立环外置换的温度梯度模拟移动床装置及其分离方法 |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3700744A (en) * | 1970-09-18 | 1972-10-24 | Universal Oil Prod Co | Simultaneous recovery and production of pure xylenes from a c aromatic mixture |
| TW200454B (enExample) * | 1991-09-05 | 1993-02-21 | Inst Of France Petroleum | |
| FR2773149B1 (fr) * | 1997-12-26 | 2000-02-18 | Inst Francais Du Petrole | Procede de coproduction et de separation d'ethylbenzene et de paraxylene |
| US6627783B2 (en) * | 2000-07-10 | 2003-09-30 | Bp Corporation North America Inc. | Pressure swing adsorption process for separating para-xylene and ethylbenzene from mixed C8 aromatics |
| TWI240716B (en) * | 2000-07-10 | 2005-10-01 | Bp Corp North America Inc | Pressure swing adsorption process for separating paraxylene and ethylbenzene from mixed C8 aromatics |
| US6573418B2 (en) * | 2000-07-10 | 2003-06-03 | Bp Corporation North America Inc. | Process for production of para-xylene incorporating pressure swing adsorption and simulated moving bed adsorption |
| US6483002B1 (en) * | 2000-09-26 | 2002-11-19 | Uop Llc | Integrated fractional distillation for adsorptive separation process |
| FR2844790B1 (fr) | 2002-09-20 | 2004-10-22 | Inst Francais Du Petrole | Procede de coproduction de paraxylene et de styrene |
| FR2862638B1 (fr) | 2003-11-26 | 2005-12-30 | Inst Francais Du Petrole | Procede de production de paraxylene comprenant une etape d'adsorption et deux etapes d'isomerisation |
| US7553998B2 (en) * | 2006-06-21 | 2009-06-30 | Uop Llc | Energy-efficient process for para-xylene production |
| FR2922547B1 (fr) | 2007-10-18 | 2012-09-21 | Inst Francais Du Petrole | Procede de separation d'aromatiques en c8 avec recyclage limite |
| US8557028B2 (en) * | 2011-03-31 | 2013-10-15 | Uop Llc | Binderless zeolitic adsorbents, methods for producing binderless zeolitic adsorbents, and adsorptive separation processes using the binderless zeolitic adsorbents |
| US8802914B2 (en) | 2011-12-15 | 2014-08-12 | Uop Llc | Process and apparatus for para-xylene production using multiple adsorptive separation units and a split fractionating column |
| CN103373891B (zh) * | 2012-04-26 | 2015-07-29 | 中国石油化工股份有限公司 | 从c8芳烃中吸附分离生产对二甲苯和乙苯的方法 |
| FR3002461B1 (fr) * | 2013-02-22 | 2016-12-09 | Ifp Energies Now | Procede de separation des xylenes en lit mobile simule au moyen d'un solide adsorbant zeolithique de granulometrie comprise entre 150 et 500 microns |
| FR3010911B1 (fr) * | 2013-09-20 | 2017-06-09 | Ifp Energies Now | Procede de separation des xylenes par contre courant simule traitant une charge contenant des impuretes oxygenees aromatiques de type phenols |
| FR3023841B1 (fr) * | 2014-07-18 | 2016-07-15 | Ifp Energies Now | Procede de production de paraxylene comprenant deux unites de separation en lit mobile simule et deux unites d'isomerisation dont l'une en phase gaz |
| JP6615888B2 (ja) * | 2014-08-15 | 2019-12-04 | エクソンモービル・ケミカル・パテンツ・インク | 芳香族の製造方法 |
| WO2016133589A1 (en) * | 2015-02-19 | 2016-08-25 | Exxonmobil Chemical Patents Inc. | Xylene separation process |
| KR101974770B1 (ko) * | 2015-04-30 | 2019-05-02 | 엑손모빌 케미칼 패턴츠 인코포레이티드 | 파라-자일렌의 제조를 위한 방법 및 장치 |
| FR3083230B1 (fr) * | 2018-06-29 | 2021-04-23 | Axens | Procede de production de paraxylene utilisant une etape en lit mobile simule, et une etape de fractionnement via une colonne de 3 coupes |
-
2018
- 2018-06-29 FR FR1856049A patent/FR3083231B1/fr not_active Expired - Fee Related
-
2019
- 2019-06-21 PT PT197312994T patent/PT3814307T/pt unknown
- 2019-06-21 KR KR1020207036182A patent/KR102773808B1/ko active Active
- 2019-06-21 JP JP2020572983A patent/JP7361057B2/ja active Active
- 2019-06-21 EP EP19731299.4A patent/EP3814307B1/fr active Active
- 2019-06-21 US US17/256,290 patent/US11242302B2/en active Active
- 2019-06-21 WO PCT/EP2019/066445 patent/WO2020002142A1/fr not_active Ceased
- 2019-06-21 CN CN201980043987.6A patent/CN112585107B/zh active Active
Also Published As
| Publication number | Publication date |
|---|---|
| JP7361057B2 (ja) | 2023-10-13 |
| JP2021528468A (ja) | 2021-10-21 |
| US20210261483A1 (en) | 2021-08-26 |
| EP3814307A1 (fr) | 2021-05-05 |
| KR20210030273A (ko) | 2021-03-17 |
| EP3814307B1 (fr) | 2022-04-20 |
| PT3814307T (pt) | 2022-05-30 |
| CN112585107A (zh) | 2021-03-30 |
| FR3083231A1 (fr) | 2020-01-03 |
| US11242302B2 (en) | 2022-02-08 |
| WO2020002142A1 (fr) | 2020-01-02 |
| CN112585107B (zh) | 2024-04-02 |
| KR102773808B1 (ko) | 2025-02-26 |
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