FR3069538B1 - Procede de purification d'esters (meth)acryliques. - Google Patents
Procede de purification d'esters (meth)acryliques. Download PDFInfo
- Publication number
- FR3069538B1 FR3069538B1 FR1757038A FR1757038A FR3069538B1 FR 3069538 B1 FR3069538 B1 FR 3069538B1 FR 1757038 A FR1757038 A FR 1757038A FR 1757038 A FR1757038 A FR 1757038A FR 3069538 B1 FR3069538 B1 FR 3069538B1
- Authority
- FR
- France
- Prior art keywords
- column
- meth
- purification
- acrylic esters
- contiguous
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/141—Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/06—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton from hydroxy amines by reactions involving the etherification or esterification of hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/10—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/02—Preparation of carboxylic acid esters by interreacting ester groups, i.e. transesterification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Priority Applications (9)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1757038A FR3069538B1 (fr) | 2017-07-25 | 2017-07-25 | Procede de purification d'esters (meth)acryliques. |
| EP18749024.8A EP3658249B1 (fr) | 2017-07-25 | 2018-07-03 | Procede de purification d'esters (meth)acryliques |
| CN201880035815.XA CN110709149A (zh) | 2017-07-25 | 2018-07-03 | 纯化(甲基)丙烯酸酯的方法 |
| JP2019563593A JP7079272B2 (ja) | 2017-07-25 | 2018-07-03 | （メタ）アクリル酸エステルの精製方法 |
| US16/616,528 US11261150B2 (en) | 2017-07-25 | 2018-07-03 | Method for purifying (meth)acrylic esters |
| PCT/FR2018/051645 WO2019020889A1 (fr) | 2017-07-25 | 2018-07-03 | Procede de purification d'esters (meth)acryliques |
| KR1020197035333A KR102610677B1 (ko) | 2017-07-25 | 2018-07-03 | (메트)아크릴산 에스테르를 정제하기 위한 방법 |
| BR112019024485-9A BR112019024485B1 (pt) | 2017-07-25 | 2018-07-03 | Processo de purificação de ésteres metacrílicos |
| SA519410648A SA519410648B1 (ar) | 2017-07-25 | 2019-11-27 | طريقة لتنقية استرات (ميث) أكريليك |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1757038A FR3069538B1 (fr) | 2017-07-25 | 2017-07-25 | Procede de purification d'esters (meth)acryliques. |
| FR1757038 | 2017-07-25 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR3069538A1 FR3069538A1 (fr) | 2019-02-01 |
| FR3069538B1 true FR3069538B1 (fr) | 2020-05-15 |
Family
ID=60138503
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR1757038A Active FR3069538B1 (fr) | 2017-07-25 | 2017-07-25 | Procede de purification d'esters (meth)acryliques. |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US11261150B2 (https=) |
| EP (1) | EP3658249B1 (https=) |
| JP (1) | JP7079272B2 (https=) |
| KR (1) | KR102610677B1 (https=) |
| CN (1) | CN110709149A (https=) |
| FR (1) | FR3069538B1 (https=) |
| SA (1) | SA519410648B1 (https=) |
| WO (1) | WO2019020889A1 (https=) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102900665B1 (ko) * | 2021-09-14 | 2025-12-15 | 주식회사 엘지화학 | 다성분 혼합물 분리 시스템 |
| EP4652152A1 (en) * | 2023-01-20 | 2025-11-26 | Kemira OYJ | Surfactant compositions derived from waste streams, and methods |
| WO2026024279A1 (en) * | 2024-07-24 | 2026-01-29 | Kemira Oyj | Surfactant compositions derived from waste streams, and methods |
| WO2026080677A1 (en) * | 2024-10-09 | 2026-04-16 | Braskem S.A. | Monomer recovery system and process for obtaining a purified branched vinyl ester stream |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5035214A (en) * | 1990-02-16 | 1991-07-30 | Siemens Automotive L.P. | Engine throttle blade sealing |
| JPH0613462B2 (ja) * | 1990-09-25 | 1994-02-23 | 東亞合成化学工業株式会社 | ジメチルアミノエチルアクリレートの貯蔵方法 |
| FR2777561B1 (fr) | 1998-04-21 | 2000-06-02 | Atochem Elf Sa | Procede de fabrication en continu de (meth)acrylates de dialkylaminoalkyle |
| DE10127938A1 (de) | 2001-06-08 | 2002-07-25 | Basf Ag | Verfahren zur Herstellung von (Meth)acrylsäureestern |
| DE10127939A1 (de) | 2001-06-08 | 2002-05-29 | Basf Ag | Verfahren zur Herstellung von (Meth)acrylsäureestern |
| US6930206B1 (en) * | 2001-07-05 | 2005-08-16 | Catalytic Distillation Technologies | Process and apparatus for catalytic distillations |
| JP2005239564A (ja) * | 2004-02-24 | 2005-09-08 | Mitsubishi Rayon Co Ltd | （メタ）アクリル酸エステルの製造方法 |
| US20090139852A1 (en) * | 2007-12-04 | 2009-06-04 | Vannuland Marco L | Separation Method And Apparatus |
| AU2010326267B2 (en) * | 2009-12-01 | 2015-07-16 | Exxonmobil Research And Engineering Company | Two stage hydroprocessing with divided wall column fractionator |
| WO2012071158A1 (en) * | 2010-11-22 | 2012-05-31 | Rohm And Haas Company | Acrylate production process |
| KR101496488B1 (ko) * | 2010-12-29 | 2015-02-26 | 주식회사 엘지화학 | 고순도 2-에틸헥실-아크릴레이트 생산을 위한 분리벽형 증류탑 및 이를 이용한 제조방법 |
| FR2985999B1 (fr) | 2012-01-23 | 2014-01-31 | Arkema France | Procede de production d'acrylate de 2-octyle par transesterification |
| FR2999572B1 (fr) | 2012-12-17 | 2014-11-28 | Arkema France | Procede de production d'acrylate d'alkyle. |
| CN105555380B (zh) * | 2013-07-18 | 2017-11-14 | Lg化学株式会社 | 蒸馏装置 |
| CN203494195U (zh) * | 2013-09-24 | 2014-03-26 | 中国石油化工股份有限公司 | 用于共沸精馏的分壁精馏塔 |
| CN106861353A (zh) * | 2015-12-14 | 2017-06-20 | 财团法人工业技术研究院 | 分离装置 |
| CN106748758A (zh) * | 2016-12-21 | 2017-05-31 | 常州大学 | 热泵分隔壁反应精馏塔制备乙酸异丙酯的装置 |
-
2017
- 2017-07-25 FR FR1757038A patent/FR3069538B1/fr active Active
-
2018
- 2018-07-03 JP JP2019563593A patent/JP7079272B2/ja active Active
- 2018-07-03 CN CN201880035815.XA patent/CN110709149A/zh active Pending
- 2018-07-03 US US16/616,528 patent/US11261150B2/en active Active
- 2018-07-03 WO PCT/FR2018/051645 patent/WO2019020889A1/fr not_active Ceased
- 2018-07-03 KR KR1020197035333A patent/KR102610677B1/ko active Active
- 2018-07-03 EP EP18749024.8A patent/EP3658249B1/fr active Active
-
2019
- 2019-11-27 SA SA519410648A patent/SA519410648B1/ar unknown
Also Published As
| Publication number | Publication date |
|---|---|
| JP2020528398A (ja) | 2020-09-24 |
| BR112019024485A2 (pt) | 2020-06-16 |
| KR102610677B1 (ko) | 2023-12-05 |
| KR20200033797A (ko) | 2020-03-30 |
| SA519410648B1 (ar) | 2023-01-10 |
| EP3658249A1 (fr) | 2020-06-03 |
| US20210300857A1 (en) | 2021-09-30 |
| FR3069538A1 (fr) | 2019-02-01 |
| US11261150B2 (en) | 2022-03-01 |
| JP7079272B2 (ja) | 2022-06-01 |
| CN110709149A (zh) | 2020-01-17 |
| EP3658249B1 (fr) | 2021-10-27 |
| WO2019020889A1 (fr) | 2019-01-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PLSC | Publication of the preliminary search report |
Effective date: 20190201 |
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| PLFP | Fee payment |
Year of fee payment: 3 |
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| PLFP | Fee payment |
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| PLFP | Fee payment |
Year of fee payment: 9 |
|
| CA | Change of address |
Effective date: 20250718 |