FR2937324B1 - Procede de preparation d'un materiau composite a base de nanotubes, notamment de carbone - Google Patents

Procede de preparation d'un materiau composite a base de nanotubes, notamment de carbone

Info

Publication number
FR2937324B1
FR2937324B1 FR0857173A FR0857173A FR2937324B1 FR 2937324 B1 FR2937324 B1 FR 2937324B1 FR 0857173 A FR0857173 A FR 0857173A FR 0857173 A FR0857173 A FR 0857173A FR 2937324 B1 FR2937324 B1 FR 2937324B1
Authority
FR
France
Prior art keywords
nanotubes
preparation
composite material
material based
particular carbon
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR0857173A
Other languages
English (en)
Other versions
FR2937324A1 (fr
Inventor
Alexander Korzhenko
Benoit Brule
Aude Chiquot
Patrick Piccione
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Arkema France SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Arkema France SA filed Critical Arkema France SA
Priority to FR0857173A priority Critical patent/FR2937324B1/fr
Priority to FR0951843A priority patent/FR2937323B1/fr
Priority to US13/125,629 priority patent/US20110201731A1/en
Priority to KR1020117009003A priority patent/KR20110057254A/ko
Priority to PCT/FR2009/052034 priority patent/WO2010046606A1/fr
Priority to EP09760201A priority patent/EP2344575A1/fr
Priority to JP2011532692A priority patent/JP2012506475A/ja
Priority to CN2009801517690A priority patent/CN102264809A/zh
Publication of FR2937324A1 publication Critical patent/FR2937324A1/fr
Application granted granted Critical
Publication of FR2937324B1 publication Critical patent/FR2937324B1/fr
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/005—Reinforced macromolecular compounds with nanosized materials, e.g. nanoparticles, nanofibres, nanotubes, nanowires, nanorods or nanolayered materials
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/03—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor characterised by the shape of the extruded material at extrusion
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/20—Compounding polymers with additives, e.g. colouring
    • C08J3/203—Solid polymers with solid and/or liquid additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/20—Compounding polymers with additives, e.g. colouring
    • C08J3/22—Compounding polymers with additives, e.g. colouring using masterbatch techniques
    • C08J3/226—Compounding polymers with additives, e.g. colouring using masterbatch techniques using a polymer as a carrier
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/02—Elements
    • C08K3/04—Carbon
    • C08K3/041—Carbon nanotubes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L95/00—Compositions of bituminous materials, e.g. asphalt, tar, pitch
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B1/00—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
    • H01B1/20—Conductive material dispersed in non-conductive organic material
    • H01B1/24—Conductive material dispersed in non-conductive organic material the conductive material comprising carbon-silicon compounds, carbon or silicon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/022—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor characterised by the choice of material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/25—Component parts, details or accessories; Auxiliary operations
    • B29C48/285—Feeding the extrusion material to the extruder
    • B29C48/29—Feeding the extrusion material to the extruder in liquid form
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2105/00—Condition, form or state of moulded material or of the material to be shaped
    • B29K2105/0005—Condition, form or state of moulded material or of the material to be shaped containing compounding ingredients
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2105/00—Condition, form or state of moulded material or of the material to be shaped
    • B29K2105/0005—Condition, form or state of moulded material or of the material to be shaped containing compounding ingredients
    • B29K2105/0038—Plasticisers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2351/00—Characterised by the use of graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives of such polymers
    • C08J2351/04—Characterised by the use of graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives of such polymers grafted on to rubbers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2353/00—Characterised by the use of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives of such polymers
    • C08J2353/02—Characterised by the use of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives of such polymers of vinyl aromatic monomers and conjugated dienes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2369/00—Characterised by the use of polycarbonates; Derivatives of polycarbonates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2371/00—Characterised by the use of polyethers obtained by reactions forming an ether link in the main chain; Derivatives of such polymers
    • C08J2371/02—Polyalkylene oxides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2377/00—Characterised by the use of polyamides obtained by reactions forming a carboxylic amide link in the main chain; Derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2395/00—Bituminous materials, e.g. asphalt, tar or pitch
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2451/00—Characterised by the use of graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2453/00—Characterised by the use of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2469/00—Characterised by the use of polycarbonates; Derivatives of polycarbonates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2471/00—Characterised by the use of polyethers obtained by reactions forming an ether link in the main chain; Derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2477/00—Characterised by the use of polyamides obtained by reactions forming a carboxylic amide link in the main chain; Derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L21/00—Compositions of unspecified rubbers

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Nanotechnology (AREA)
  • Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Dispersion Chemistry (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Mechanical Engineering (AREA)
  • Composite Materials (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Civil Engineering (AREA)
  • Structural Engineering (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
FR0857173A 2008-10-22 2008-10-22 Procede de preparation d'un materiau composite a base de nanotubes, notamment de carbone Expired - Fee Related FR2937324B1 (fr)

Priority Applications (8)

Application Number Priority Date Filing Date Title
FR0857173A FR2937324B1 (fr) 2008-10-22 2008-10-22 Procede de preparation d'un materiau composite a base de nanotubes, notamment de carbone
FR0951843A FR2937323B1 (fr) 2008-10-22 2009-03-23 Procede de preparation d'un materiau composite thermoplastique a base de nanotubes, notamment de carbone
KR1020117009003A KR20110057254A (ko) 2008-10-22 2009-10-22 나노튜브, 특히 탄소 나노튜브를 함유하는 열가소성 복합 재료의 제조 방법
PCT/FR2009/052034 WO2010046606A1 (fr) 2008-10-22 2009-10-22 Procédé de préparation d'un matériau composite thermoplastique à base de nanotubes, notamment de carbone
US13/125,629 US20110201731A1 (en) 2008-10-22 2009-10-22 Method for preparing a thermoplastic composite material containing nanotubes particularly carbon nanotubes
EP09760201A EP2344575A1 (fr) 2008-10-22 2009-10-22 Procédé de préparation d'un matériau composite thermoplastique à base de nanotubes, notamment de carbone
JP2011532692A JP2012506475A (ja) 2008-10-22 2009-10-22 ナノチューブ、特にカーボンナノチューブを含む熱可塑性複合材料の製造方法
CN2009801517690A CN102264809A (zh) 2008-10-22 2009-10-22 制备含有纳米管、特别是碳纳米管的热塑性复合材料的方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR0857173A FR2937324B1 (fr) 2008-10-22 2008-10-22 Procede de preparation d'un materiau composite a base de nanotubes, notamment de carbone

Publications (2)

Publication Number Publication Date
FR2937324A1 FR2937324A1 (fr) 2010-04-23
FR2937324B1 true FR2937324B1 (fr) 2012-03-16

Family

ID=40622289

Family Applications (2)

Application Number Title Priority Date Filing Date
FR0857173A Expired - Fee Related FR2937324B1 (fr) 2008-10-22 2008-10-22 Procede de preparation d'un materiau composite a base de nanotubes, notamment de carbone
FR0951843A Expired - Fee Related FR2937323B1 (fr) 2008-10-22 2009-03-23 Procede de preparation d'un materiau composite thermoplastique a base de nanotubes, notamment de carbone

Family Applications After (1)

Application Number Title Priority Date Filing Date
FR0951843A Expired - Fee Related FR2937323B1 (fr) 2008-10-22 2009-03-23 Procede de preparation d'un materiau composite thermoplastique a base de nanotubes, notamment de carbone

Country Status (7)

Country Link
US (1) US20110201731A1 (fr)
EP (1) EP2344575A1 (fr)
JP (1) JP2012506475A (fr)
KR (1) KR20110057254A (fr)
CN (1) CN102264809A (fr)
FR (2) FR2937324B1 (fr)
WO (1) WO2010046606A1 (fr)

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FR2959231B1 (fr) * 2010-04-22 2012-04-20 Arkema France Materiau composite thermoplastique et/ou elastomerique a base de nanotubes de carbone et de graphenes
TW201219447A (en) * 2010-10-12 2012-05-16 Solvay Polymer compositions comprising poly(arylether ketone)s and graphene materials
DE102010043473A1 (de) * 2010-11-05 2012-05-10 Evonik Degussa Gmbh Carbon Nanotubes enthaltende Polyamid 12-Zusammensetzung
DE102010043470A1 (de) * 2010-11-05 2012-05-10 Evonik Degussa Gmbh Zusammensetzung aus Polyamiden mit niedriger Konzentration an Carbonsäureamidgruppen und elektrisch leitfähigem Kohlenstoff
FR2968676B1 (fr) 2010-12-14 2012-12-07 Arkema France Procede d'introduction de nanocharges d'origine carbonique dans un metal ou un alliage
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FR2991332B1 (fr) 2012-06-04 2015-04-24 Arkema France Utilisation de nanocharges carbonees a tres faible taux pour la stabilisation uv de materiaux composites
FR2991333B1 (fr) 2012-06-04 2015-04-03 Arkema France Utilisation de nanocharges carbonees a tres faible taux pour le renfort mecanique de materiaux composites eventuellement charges
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RU2496812C1 (ru) * 2012-08-01 2013-10-27 Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Белгородский государственный технологический университет им. В.Г. Шухова" Полимерно-битумное вяжущее и способ его получения
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KR101539608B1 (ko) * 2013-03-14 2015-08-17 에치투엘 주식회사 폴리비닐리덴플루오라이드 중공사 분리막과 그 제조방법
RU2602798C2 (ru) * 2013-04-15 2016-11-20 Общество с ограниченной ответственностью "Новые структуры и технологии" (ООО "НоваСТ") Способ получения полимерного композита с наномодифицированным наполнителем (варианты).
CN103304996A (zh) * 2013-06-24 2013-09-18 苏州新区佳合塑胶有限公司 一种含有聚癸二酰己二胺的阻燃耐热塑胶
US9115266B2 (en) 2013-07-31 2015-08-25 E I Du Pont De Nemours And Company Carbon nanotube-polymer composite and process for making same
JP6573793B2 (ja) * 2014-07-23 2019-09-11 日信工業株式会社 熱可塑性樹脂組成物の製造方法
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FR3029926B1 (fr) * 2014-12-16 2018-07-13 Arkema France Dispositif de melange pour la fabrication d'un materiau composite a partir d'une poudre comprenant des nanocharges carbonees et d'une resine elastomere
CN104593901B (zh) * 2014-12-25 2016-08-17 东华大学 一种聚酰胺接枝碳纳米管复合纤维的制备方法
FR3033327B1 (fr) * 2015-03-05 2018-10-12 Arkema France Composition solide de nanocharges carbonees pour les formulations utilisees dans les batteries au plomb.
CN107736085B (zh) * 2015-06-09 2019-11-29 3M创新有限公司 高频电磁干扰（emi）复合材料
CN105070531B (zh) * 2015-08-05 2017-09-29 暨南大学 一种基于聚氨酯碳纳米管复合材料的可拉伸式线状超级电容器的制备方法
US9555291B1 (en) * 2015-08-25 2017-01-31 Acushnet Company Multi-layered cores for golf balls based on thermoplastic compositions containing non-acid polymers
JP6095761B1 (ja) * 2015-12-28 2017-03-15 三菱商事株式会社 炭素系導電材料が添着した顆粒状組成物及びその製造方法
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CN102264809A (zh) 2011-11-30
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FR2937323B1 (fr) 2011-02-25
EP2344575A1 (fr) 2011-07-20
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KR20110057254A (ko) 2011-05-31
FR2937323A1 (fr) 2010-04-23

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