FR2858620B1 - Cristallisation a haute temperature du 2,4,6,8,10,12 -hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.0 0]- dodecane - Google Patents

Cristallisation a haute temperature du 2,4,6,8,10,12 -hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.0 0]- dodecane

Info

Publication number
FR2858620B1
FR2858620B1 FR0408611A FR0408611A FR2858620B1 FR 2858620 B1 FR2858620 B1 FR 2858620B1 FR 0408611 A FR0408611 A FR 0408611A FR 0408611 A FR0408611 A FR 0408611A FR 2858620 B1 FR2858620 B1 FR 2858620B1
Authority
FR
France
Prior art keywords
hexaazatetracyclo
hexanitro
dodecane
high temperature
temperature crystallization
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR0408611A
Other languages
English (en)
Other versions
FR2858620A1 (fr
Inventor
R Scott Hamilton
Vincent Mancini
Clint Nelson
Sharon Yeung Dressen
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Northrop Grumman Innovation Systems LLC
Original Assignee
Alliant Techsystems Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Alliant Techsystems Inc filed Critical Alliant Techsystems Inc
Publication of FR2858620A1 publication Critical patent/FR2858620A1/fr
Application granted granted Critical
Publication of FR2858620B1 publication Critical patent/FR2858620B1/fr
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D487/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00
    • C07D487/22—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00 in which the condensed system contains four or more hetero rings
    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B25/00—Compositions containing a nitrated organic compound
    • C06B25/34—Compositions containing a nitrated organic compound the compound being a nitrated acyclic, alicyclic or heterocyclic amine

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
FR0408611A 2003-08-06 2004-08-04 Cristallisation a haute temperature du 2,4,6,8,10,12 -hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.0 0]- dodecane Expired - Fee Related FR2858620B1 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US10/636,373 US7288648B2 (en) 2000-10-06 2003-08-06 High temperature crystallization of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.05,903,11]-dodecane

Publications (2)

Publication Number Publication Date
FR2858620A1 FR2858620A1 (fr) 2005-02-11
FR2858620B1 true FR2858620B1 (fr) 2006-11-17

Family

ID=34080743

Family Applications (1)

Application Number Title Priority Date Filing Date
FR0408611A Expired - Fee Related FR2858620B1 (fr) 2003-08-06 2004-08-04 Cristallisation a haute temperature du 2,4,6,8,10,12 -hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.0 0]- dodecane

Country Status (3)

Country Link
US (1) US7288648B2 (fr)
JP (1) JP4336268B2 (fr)
FR (1) FR2858620B1 (fr)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ITSV20040044A1 (it) * 2004-12-07 2005-03-07 Tn & Co Di Lucio Righetto Suola per calzature e calzatura avente detta suola
FR2950623B1 (fr) * 2009-09-29 2011-10-21 Snpe Materiaux Energetiques Suspension de cristaux d'hexanitrohexaazaisowurtzitane, obtention desdites suspensions et fabrication d'objets pyrotechniques.
FR2973799B1 (fr) * 2011-04-08 2013-05-10 Sme Procede d'obtention d'une charge de cristaux d'hexanitrohexaazaisowurtzitane a morphologie arrondie ; charge et materiau energetique correspondant
CN102898429B (zh) * 2012-09-18 2016-01-13 北京理工大学 一种控制ε-HNIW晶形和窄粒度分布的重结晶方法
CN103539800B (zh) * 2013-10-18 2015-07-29 中国工程物理研究院化工材料研究所 大颗粒六硝基六氮杂异伍兹烷炸药的制备方法
CN103936534B (zh) * 2014-05-09 2016-07-06 北京理工大学 一种特质细化hmx晶体及制备方法
CN104193564B (zh) * 2014-09-09 2017-01-11 中国工程物理研究院化工材料研究所 细颗粒高能低感炸药复合物及其制备方法
CN106478322B (zh) * 2016-10-13 2018-04-17 西南科技大学 一种微纳米cl‑20基热固化炸药乳液制备方法
CN111233589B (zh) * 2020-02-13 2021-10-22 山西北化关铝化工有限公司 一种超大颗粒六硝基六氮杂异伍兹烷的制备方法

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5693794A (en) * 1988-09-30 1997-12-02 The United States Of America As Represented By The Secretary Of The Navy Caged polynitramine compound
US5099008A (en) * 1991-05-20 1992-03-24 The United States Of America As Represented By The Secretary Of The Army Process of reducing shock sensitivity of explosive nitramine compounds by crystal modification
US5587553A (en) * 1994-11-07 1996-12-24 Thiokol Corporation High performance pressable explosive compositions
WO1996023792A1 (fr) 1995-02-01 1996-08-08 Asahi Kasei Kogyo Kabushiki Kaisha Derives d'hexaazaisowurtzitane et leur procede de production
US5723604A (en) * 1995-06-22 1998-03-03 Thiokol Corporation Synthesis of 2,4,6,8,10,12-hexabenzyl-2,4,6,8,10,12-hexaazatetracyclo 5.5.0.05,9.03,11!dodecane
US5739325A (en) * 1995-12-07 1998-04-14 Thiokol Corporation Hydrogenolysis of 2,4,6,8,10,12-Hexabenzyl-2,4,6,8,10,12-Hexaazatetracyclo 5.5.0.05,9.03,11 !dodecane
WO1997042138A1 (fr) * 1996-05-03 1997-11-13 Eastman Chemical Company Compositions explosives
WO1998027072A1 (fr) 1996-12-17 1998-06-25 Cordant Technologies, Inc. Procede de cristallisation par relargage de 2,4,6,8,10,12,-hexanitro-2,4,6,8,10,12,-hexaazatetracyclo[5.5.0.0?5,903,11¿]-dodecane
US5712511A (en) * 1997-03-03 1998-01-27 The United States Of America As Represented By The Secretary Of The Navy Preparation of fine particulate CL-20
US5750921A (en) * 1997-07-07 1998-05-12 Chan; May L. Waste-free method of making molding powder
US6217799B1 (en) * 1997-10-07 2001-04-17 Cordant Technologies Inc. Method for making high performance explosive formulations containing CL-20
FR2770216B1 (fr) * 1997-10-29 1999-12-03 Poudres & Explosifs Ste Nale Procede d'obtention de la forme polymorphe epsilon de l'hexanitrohexaazaisowurtzitane
US6015898A (en) * 1998-05-01 2000-01-18 The United States Of America, As Represented By The Secretary Of The Army Processes and compositions for nitration of N-substituted isowurtzitane compounds with concentrated nitric acid at elevated temperatures to form HNIW and recovery of gamma HNIW with high yields and purities
US6350871B1 (en) * 2000-03-31 2002-02-26 Alliant Techsystems Inc. Crystallization of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.05,903,11]-dodecane
US6992185B2 (en) 2002-01-09 2006-01-31 Alliant Techsystems Inc. Crystallization of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.05,903,11]-dodecane

Also Published As

Publication number Publication date
JP2005097262A (ja) 2005-04-14
US7288648B2 (en) 2007-10-30
FR2858620A1 (fr) 2005-02-11
JP4336268B2 (ja) 2009-09-30
US20070225493A1 (en) 2007-09-27

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Effective date: 20150430