FR2638449A1 - Process and device for the production of a multilayer laminated glass - Google Patents

Process and device for the production of a multilayer laminated glass Download PDF

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Publication number
FR2638449A1
FR2638449A1 FR8814971A FR8814971A FR2638449A1 FR 2638449 A1 FR2638449 A1 FR 2638449A1 FR 8814971 A FR8814971 A FR 8814971A FR 8814971 A FR8814971 A FR 8814971A FR 2638449 A1 FR2638449 A1 FR 2638449A1
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France
Prior art keywords
energy
glass
laminated glass
multilayer laminated
production
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FR8814971A
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French (fr)
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FR2638449B1 (en
Inventor
Christian Lumpp
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FRANCE RAYONNEMENT
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FRANCE RAYONNEMENT
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Priority to FR8814971A priority Critical patent/FR2638449B1/en
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Publication of FR2638449B1 publication Critical patent/FR2638449B1/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B17/00Layered products essentially comprising sheet glass, or glass, slag, or like fibres
    • B32B17/06Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
    • B32B17/10Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
    • B32B17/10005Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
    • B32B17/10807Making laminated safety glass or glazing; Apparatus therefor
    • B32B17/10816Making laminated safety glass or glazing; Apparatus therefor by pressing
    • B32B17/10871Making laminated safety glass or glazing; Apparatus therefor by pressing in combination with particular heat treatment

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  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Joining Of Glass To Other Materials (AREA)

Abstract

Process for integrally joining, by a heat energy input, a plurality of successive layers of glass and of a thermoplastic intermediate binder, characterised in that the energy is introduced by an energy flow of short infrared defined in relation to the peak of maximum wavelength at 1.2 microns according to Wien's law.

Description

La présente invention a pour objet un procédé et un dispositif pour la solidarisation par apport d'énergie thermique d'une pluralité de couches alternées de verre et d'un liant intermédiaire thermoplastique, en particulier pour la réalisation d'un verre feuilleté multicouches. The present invention relates to a method and a device for the joining by thermal energy supply of a plurality of alternating layers of glass and a thermoplastic intermediate binder, in particular for the production of a multilayer laminated glass.

Pour l'obtention d'un verre feuilleté de ce type, dont la finition nécessite un certain nombre d'opérations telles que calandrage, etc... qui n'interviennent pas pour la compréhension de la présente invention et ne seront donc pas décrites, il est nécessaire d'apporter une énergie thermique de la manière la plus uniforme et intense possible sur une surface étendue et sur une épaisseur relativement importante de matière. To obtain a laminated glass of this type, the finishing of which requires a certain number of operations such as calendering, etc. which are not involved in understanding the present invention and will therefore not be described, it is necessary to provide thermal energy in the most uniform and intense manner possible over a large area and over a relatively large thickness of material.

En mettant en oeuvre des méthodes à fluide caloporteur, le gradient de température est tel que la partie centrale n'est quasiment pas traitée, ce qui entraine, dans un processus industriel, un rejet important de produits non conformes. By implementing methods with heat transfer fluid, the temperature gradient is such that the central part is almost untreated, which causes, in an industrial process, a significant rejection of non-conforming products.

Avec des processus mettant en oeuvre un apport thermique par infra rouge moyen le résultat est quasi identique contrairement à ce que l'homme de l'art aurait pu penser, car l'absorption des I.R. moyens par le liant intermédiaire et le verre est très importante. Le flux de rayonnement parvenu au centre de la structure à traiter est donc minime et dans la pratique insuffisant. With processes using a thermal input using medium infrared, the result is almost identical, contrary to what a person skilled in the art would have thought, because the absorption of average IR by the intermediate binder and the glass is very high. . The radiation flux reaching the center of the structure to be treated is therefore minimal and in practice insufficient.

On admet que 1'I.R. moyen correspond en l'espèce à une longueur d'onde moyenne correspondant au pic maximum à 2,7 microns selon la loi de Wien. We admit that the I.R. mean corresponds in this case to an average wavelength corresponding to the maximum peak at 2.7 microns according to Wien's law.

De manière surprenante, on a constaté que ce problème pouvait être résolu, permettant donc - une répartition quasi homogène en surface et en profondeur de l'énergie calorifique - en conséquence, une industrialisation optimale du procédé avec des coûts moindres au niveau matière et investissements. Surprisingly, it was found that this problem could be solved, thus allowing - an almost homogeneous distribution on the surface and in depth of the heat energy - consequently, an optimal industrialization of the process with lower costs in terms of material and investments.

Conformément à l'invention on propose, en effet, un procédé pour la solidarisation par apport d'énergie thermique d'une pluralité de couches successives de verre et d'un liant intermédiaire thermoplastique, en particulier pour la réalisation d'un verre feuilleté multicouches, caractérisé en ce que l'énergie est apportée par un flux énergétique d'infra rouge court, défini par rapport au pic de longueur d'onde maximum à 1,2 microns selon la loi de Wien. According to the invention, in fact, a method is proposed for securing by the supply of thermal energy a plurality of successive layers of glass and a thermoplastic intermediate binder, in particular for producing a multilayer laminated glass. , characterized in that the energy is provided by a short infrared energy flux, defined with respect to the peak of maximum wavelength at 1.2 microns according to Wien's law.

De ce fait, on constate que l'énergie est libérée de manière plus uniforme dans les différentes couches de liant intermédiaire thermoplastique, en particulier du P.V.B. se caractérisant par une température beaucoup plus uniforme des différentes couches de liant thermoplastique. As a result, it can be seen that the energy is released more uniformly in the different layers of thermoplastic intermediate binder, in particular of P.V.B. characterized by a much more uniform temperature of the different layers of thermoplastic binder.

De plus, 1'I.R. court permet, du fait des appareils utilisés, une libération très rapide de l'énergie (quelques secondes) alors que par les fluides caloporteurs il faut un temps de préparation et de montée en température de plusieurs heures. In addition, the I.R. short allows, due to the devices used, a very rapid release of energy (a few seconds) while by heat transfer fluids it takes a preparation time and temperature rise of several hours.

On comprendra mieux l'invention à l'aide de- la description faite ci-après en référence aux dessins annexés dans lesquels - la figure 1 schématise le gradient thermique par fluide caloporteur - la figure 2 schématise le gradient thermique par I.R. moyen - la figure 3 schématise le gradient thermique par I.R. court. The invention will be better understood with the aid of the description given below with reference to the appended drawings in which - FIG. 1 diagrams the thermal gradient by heat transfer fluid - FIG. 2 diagrams the thermal gradient by average IR - FIG. 3 diagrams the thermal gradient by short IR.

La description ci-après doit être considère comme schématique, prenant en compte certaines approximations théoriques permettant une explication compréhensible de l'invention. The description below should be considered as schematic, taking into account certain theoretical approximations allowing an understandable explanation of the invention.

Si l'on se réfère à la figure 1, on y a représenté une pluralité de couches alternées de verre (1) et d'un liant thermoplastique (2).  Referring to Figure 1, there is shown a plurality of alternating layers of glass (1) and a thermoplastic binder (2).

Le système chauffant à gaz caloporteur schématisé par (3) et (3') sur les deux faces de l'empilage génère dans ledit empilage un gradient de température tel que le maximum est obtenu sur les extrémités externes de l'empilage et que la partie la plus faible est le point de coeur (4) de celui-ci. The heat transfer gas heating system shown diagrammatically by (3) and (3 ') on the two faces of the stack generates in said stack a temperature gradient such that the maximum is obtained on the external ends of the stack and that the part the weakest is the heart point (4) of it.

De la même manière (figure 2) avec un rayonnement I.R. moyen, si l'on suppose une transparence à 100 % du verre par rapport à celui-ci, l'absorption par le P.V.B. est très importante. Le gradient de température reste identique à celui d'un fluide caloporteur. In the same way (figure 2) with an average IR radiation, if we suppose a 100% transparency of the glass compared to this one, the absorption by the P.V.B. is very important. The temperature gradient remains identical to that of a heat transfer fluid.

Avec de l'I.R. court, comme représente à la figure 3, l'absorption (toujours supposée à O % par le verre, donc une transparence de 100 %) est de 20 à 30 % par le P.V.B., à chaque passage d'une couche. With I.R. short, as shown in Figure 3, the absorption (always assumed to be 0% by the glass, therefore 100% transparency) is 20 to 30% by the P.V.B., each time a layer is passed.

La portion de flux énergétique parvenant au cours de l'empilage reste donc importante et recouvre également une surface de flux importante. The portion of energy flow arriving during stacking therefore remains large and also covers a large flow area.

Pour un dispositif comportant une pluralité de générateurs d'I.R. court disposés en outre de chaque côté de l'empilage, on obtient donc un résultat tout à fait satisfaisant d'un point de vue énergétique, donc qualitatif, sur l'ensemble des surfaces et de l'épaisseur de l'empilage à traiter. For a device comprising a plurality of I.R generators. short additionally arranged on each side of the stack, one therefore obtains a completely satisfactory result from an energy point of view, therefore qualitative, on all of the surfaces and the thickness of the stack to be treated.

La mise en oeuvre de l'I.R. court permet - un meilleur rendement, - une émission de puissance instantanée garantissant une rapidité de production et un gain d'énergie. The implementation of the I.R. short allows - a better output, - an instantaneous emission of power guaranteeing a speed of production and an energy saving.

Les investissements sont nettement plus faibles et la maintenance très faible. Investments are significantly lower and maintenance very low.

Les sources d'I.R. utilisées peuvent être par exemple du type décrit dans le brevet EP 0127496 au nom de l'inventeur. The sources of I.R. used can for example be of the type described in patent EP 0127496 in the name of the inventor.

L'invention trouve une application particulièrement intéressante dans la fabrication de vitrages feuilletés à très haute résistance.  The invention finds a particularly advantageous application in the manufacture of laminated glazing with very high resistance.

Claims (2)

REVENDICATIONS 1. Procédé pour la solidarisation par apport d'énergie thermique d'une pluralité de couches successives de verre et d'un liant intermédiaire thermoplastique, en particulier pour la réalisation d'un verre feuilleté multicouches, caractérisé en ce que l'énergie est apportée par un flux énergétique d'infra rouge court, défini par rapport au pic de longueur d'onde maximum à 1,2 microns selon la loi de Wien.1. Method for securing by supplying thermal energy to a plurality of successive layers of glass and a thermoplastic intermediate binder, in particular for producing a multilayer laminated glass, characterized in that the energy is supplied by a short infrared energy flow, defined with respect to the maximum wavelength peak at 1.2 microns according to Wien's law. 2. Dispositif pour la mise en oeuvre du procédé selon la revendication 1, caractérisé en ce qu'il comporte une pluralité de générateurs d'Infra-Rouge court disposés de chaque côté des couches de verre et de liant, 2. Device for implementing the method according to claim 1, characterized in that it comprises a plurality of short infrared generators arranged on each side of the layers of glass and binder,
FR8814971A 1988-10-27 1988-10-27 PROCESS AND DEVICE FOR PRODUCING A MULTILAYERED LAMINATED GLASS Expired - Fee Related FR2638449B1 (en)

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FR8814971A FR2638449B1 (en) 1988-10-27 1988-10-27 PROCESS AND DEVICE FOR PRODUCING A MULTILAYERED LAMINATED GLASS

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0707950A3 (en) * 1994-10-20 1996-09-11 Tamglass Eng Oy Method and apparatus for laminating glass sheets
WO2020099800A1 (en) * 2018-11-16 2020-05-22 Saint-Gobain Glass France Method for producing a laminated glazing, where at least one face of the stack of constituents is exposed to radiation with a spectrum chosen from two narrowly defined ranges

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2075726A (en) * 1935-05-04 1937-03-30 Duplate Corp Method of heating safety glass assemblies
DE2029657A1 (en) * 1970-06-16 1971-12-23 Gustav Ruth Temperol-Werke, Chemische und Lackfabriken, 2000 Hamburg Process for curing lacquers or lacquer paints based on unsaturated polyester or polyurethane systems on wooden substrates, in particular for furniture
DE2040888A1 (en) * 1970-08-18 1972-03-02 Wiederhold Fa Hermann Drying transparent polyester varnishes - of unsatd type with phosphor-coated mercury vapour low pressure lamp
GB2056885A (en) * 1979-08-08 1981-03-25 Blundell Permoglaze Ltd Powder coating cellulose fibre substrates
WO1988003517A1 (en) * 1986-11-06 1988-05-19 Colin Maxwell Finch Process and apparatus for producing a laminate

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2075726A (en) * 1935-05-04 1937-03-30 Duplate Corp Method of heating safety glass assemblies
DE2029657A1 (en) * 1970-06-16 1971-12-23 Gustav Ruth Temperol-Werke, Chemische und Lackfabriken, 2000 Hamburg Process for curing lacquers or lacquer paints based on unsaturated polyester or polyurethane systems on wooden substrates, in particular for furniture
DE2040888A1 (en) * 1970-08-18 1972-03-02 Wiederhold Fa Hermann Drying transparent polyester varnishes - of unsatd type with phosphor-coated mercury vapour low pressure lamp
GB2056885A (en) * 1979-08-08 1981-03-25 Blundell Permoglaze Ltd Powder coating cellulose fibre substrates
WO1988003517A1 (en) * 1986-11-06 1988-05-19 Colin Maxwell Finch Process and apparatus for producing a laminate

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0707950A3 (en) * 1994-10-20 1996-09-11 Tamglass Eng Oy Method and apparatus for laminating glass sheets
US5853516A (en) * 1994-10-20 1998-12-29 Tamglass Engineering Oy Method and apparatus for laminating glass sheets
WO2020099800A1 (en) * 2018-11-16 2020-05-22 Saint-Gobain Glass France Method for producing a laminated glazing, where at least one face of the stack of constituents is exposed to radiation with a spectrum chosen from two narrowly defined ranges
FR3088577A1 (en) * 2018-11-16 2020-05-22 Saint-Gobain Glass France PROCESS FOR THE MANUFACTURE OF A LAMINATED GLAZING OF WHICH A SIDE AT LEAST OF THE STACKING OF THE CONSTITUENTS IS EXPOSED TO A RADIATION OF SELECTED SPECTRUM IN TWO NARROW DEFINED AREAS

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