FR2526273A1 - Mixing heat sensitive food and medicinal substances - with material that melts above 40 deg. C and is solid below 30 Deg. C. - Google Patents
Mixing heat sensitive food and medicinal substances - with material that melts above 40 deg. C and is solid below 30 Deg. C. Download PDFInfo
- Publication number
- FR2526273A1 FR2526273A1 FR8207715A FR8207715A FR2526273A1 FR 2526273 A1 FR2526273 A1 FR 2526273A1 FR 8207715 A FR8207715 A FR 8207715A FR 8207715 A FR8207715 A FR 8207715A FR 2526273 A1 FR2526273 A1 FR 2526273A1
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- France
- Prior art keywords
- solid phase
- phase
- celsius
- composition
- salts
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- 238000002156 mixing Methods 0.000 title claims abstract description 8
- 235000013305 food Nutrition 0.000 title claims abstract description 6
- 239000007787 solid Substances 0.000 title claims abstract description 5
- 239000000126 substance Substances 0.000 title claims abstract description 5
- 239000000463 material Substances 0.000 title abstract 2
- 239000000155 melt Substances 0.000 title 1
- 239000007790 solid phase Substances 0.000 claims abstract description 12
- 229940024606 amino acid Drugs 0.000 claims abstract description 10
- 235000001014 amino acid Nutrition 0.000 claims abstract description 10
- 150000001413 amino acids Chemical class 0.000 claims abstract description 10
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 9
- 239000011707 mineral Substances 0.000 claims abstract description 9
- 235000000346 sugar Nutrition 0.000 claims abstract description 9
- 239000007791 liquid phase Substances 0.000 claims abstract description 8
- 150000008163 sugars Chemical class 0.000 claims abstract description 7
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims abstract description 6
- CKLJMWTZIZZHCS-UWTATZPHSA-N L-Aspartic acid Natural products OC(=O)[C@H](N)CC(O)=O CKLJMWTZIZZHCS-UWTATZPHSA-N 0.000 claims abstract description 5
- 239000012071 phase Substances 0.000 claims abstract description 5
- 229940126601 medicinal product Drugs 0.000 claims abstract description 4
- CKLJMWTZIZZHCS-UHFFFAOYSA-N D-OH-Asp Natural products OC(=O)C(N)CC(O)=O CKLJMWTZIZZHCS-UHFFFAOYSA-N 0.000 claims abstract description 3
- 229960005261 aspartic acid Drugs 0.000 claims abstract description 3
- 229910001629 magnesium chloride Inorganic materials 0.000 claims abstract description 3
- 239000000600 sorbitol Substances 0.000 claims abstract description 3
- LXNHXLLTXMVWPM-UHFFFAOYSA-N pyridoxine Chemical compound CC1=NC=C(CO)C(CO)=C1O LXNHXLLTXMVWPM-UHFFFAOYSA-N 0.000 claims abstract 6
- 229940011671 vitamin b6 Drugs 0.000 claims abstract 3
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 claims abstract 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims abstract 2
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims abstract 2
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims abstract 2
- 229930091371 Fructose Natural products 0.000 claims abstract 2
- 239000005715 Fructose Substances 0.000 claims abstract 2
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims abstract 2
- OUYCCCASQSFEME-QMMMGPOBSA-N L-tyrosine Chemical compound OC(=O)[C@@H](N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-QMMMGPOBSA-N 0.000 claims abstract 2
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 claims abstract 2
- JZRWCGZRTZMZEH-UHFFFAOYSA-N Thiamine Natural products CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N JZRWCGZRTZMZEH-UHFFFAOYSA-N 0.000 claims abstract 2
- WQZGKKKJIJFFOK-PHYPRBDBSA-N alpha-D-galactose Chemical compound OC[C@H]1O[C@H](O)[C@H](O)[C@@H](O)[C@H]1O WQZGKKKJIJFFOK-PHYPRBDBSA-N 0.000 claims abstract 2
- 239000001110 calcium chloride Substances 0.000 claims abstract 2
- 229910001628 calcium chloride Inorganic materials 0.000 claims abstract 2
- 229930182830 galactose Natural products 0.000 claims abstract 2
- 239000008101 lactose Substances 0.000 claims abstract 2
- 235000011837 pasties Nutrition 0.000 claims abstract 2
- RADKZDMFGJYCBB-UHFFFAOYSA-N pyridoxal hydrochloride Natural products CC1=NC=C(CO)C(C=O)=C1O RADKZDMFGJYCBB-UHFFFAOYSA-N 0.000 claims abstract 2
- 239000011721 thiamine Substances 0.000 claims abstract 2
- KYMBYSLLVAOCFI-UHFFFAOYSA-N thiamine Chemical compound CC1=C(CCO)SCN1CC1=CN=C(C)N=C1N KYMBYSLLVAOCFI-UHFFFAOYSA-N 0.000 claims abstract 2
- 229960003495 thiamine Drugs 0.000 claims abstract 2
- 235000019157 thiamine Nutrition 0.000 claims abstract 2
- OUYCCCASQSFEME-UHFFFAOYSA-N tyrosine Natural products OC(=O)C(N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-UHFFFAOYSA-N 0.000 claims abstract 2
- 239000011726 vitamin B6 Substances 0.000 claims abstract 2
- 235000019158 vitamin B6 Nutrition 0.000 claims abstract 2
- 239000000203 mixture Substances 0.000 claims description 21
- 238000000034 method Methods 0.000 claims description 15
- 150000003839 salts Chemical class 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 7
- 229930003231 vitamin Natural products 0.000 claims description 7
- 235000013343 vitamin Nutrition 0.000 claims description 7
- 229940088594 vitamin Drugs 0.000 claims description 7
- 239000011782 vitamin Substances 0.000 claims description 7
- 239000000843 powder Substances 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 239000004475 Arginine Substances 0.000 claims description 2
- ODKSFYDXXFIFQN-UHFFFAOYSA-N arginine Natural products OC(=O)C(N)CCCNC(N)=N ODKSFYDXXFIFQN-UHFFFAOYSA-N 0.000 claims description 2
- 239000000470 constituent Substances 0.000 claims description 2
- 241001465754 Metazoa Species 0.000 claims 3
- 241000282412 Homo Species 0.000 claims 1
- ODKSFYDXXFIFQN-BYPYZUCNSA-P L-argininium(2+) Chemical compound NC(=[NH2+])NCCC[C@H]([NH3+])C(O)=O ODKSFYDXXFIFQN-BYPYZUCNSA-P 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 229960005336 magnesium citrate Drugs 0.000 claims 1
- 235000002538 magnesium citrate Nutrition 0.000 claims 1
- 239000004337 magnesium citrate Substances 0.000 claims 1
- 235000008160 pyridoxine Nutrition 0.000 claims 1
- 239000011677 pyridoxine Substances 0.000 claims 1
- IFGCUJZIWBUILZ-UHFFFAOYSA-N sodium 2-[[2-[[hydroxy-(3,4,5-trihydroxy-6-methyloxan-2-yl)oxyphosphoryl]amino]-4-methylpentanoyl]amino]-3-(1H-indol-3-yl)propanoic acid Chemical compound [Na+].C=1NC2=CC=CC=C2C=1CC(C(O)=O)NC(=O)C(CC(C)C)NP(O)(=O)OC1OC(C)C(O)C(O)C1O IFGCUJZIWBUILZ-UHFFFAOYSA-N 0.000 claims 1
- PLSARIKBYIPYPF-UHFFFAOYSA-H trimagnesium dicitrate Chemical compound [Mg+2].[Mg+2].[Mg+2].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O PLSARIKBYIPYPF-UHFFFAOYSA-H 0.000 claims 1
- 229940110456 cocoa butter Drugs 0.000 abstract description 11
- 235000019868 cocoa butter Nutrition 0.000 abstract description 11
- QIVBCDIJIAJPQS-VIFPVBQESA-N L-tryptophane Chemical compound C1=CC=C2C(C[C@H](N)C(O)=O)=CNC2=C1 QIVBCDIJIAJPQS-VIFPVBQESA-N 0.000 abstract description 9
- 235000010755 mineral Nutrition 0.000 abstract description 6
- 238000010438 heat treatment Methods 0.000 abstract description 2
- 235000015110 jellies Nutrition 0.000 abstract description 2
- 238000002844 melting Methods 0.000 abstract description 2
- GHOKWGTUZJEAQD-ZETCQYMHSA-N (D)-(+)-Pantothenic acid Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCC(O)=O GHOKWGTUZJEAQD-ZETCQYMHSA-N 0.000 abstract 2
- GHOKWGTUZJEAQD-UHFFFAOYSA-N Chick antidermatitis factor Natural products OCC(C)(C)C(O)C(=O)NCCC(O)=O GHOKWGTUZJEAQD-UHFFFAOYSA-N 0.000 abstract 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 abstract 1
- ODKSFYDXXFIFQN-BYPYZUCNSA-N L-arginine Chemical compound OC(=O)[C@@H](N)CCCN=C(N)N ODKSFYDXXFIFQN-BYPYZUCNSA-N 0.000 abstract 1
- 229930064664 L-arginine Natural products 0.000 abstract 1
- 235000014852 L-arginine Nutrition 0.000 abstract 1
- CKLJMWTZIZZHCS-REOHCLBHSA-N L-aspartic acid Chemical compound OC(=O)[C@@H](N)CC(O)=O CKLJMWTZIZZHCS-REOHCLBHSA-N 0.000 abstract 1
- 235000011148 calcium chloride Nutrition 0.000 abstract 1
- 239000004615 ingredient Substances 0.000 abstract 1
- 239000011777 magnesium Substances 0.000 abstract 1
- 239000011713 pantothenic acid Substances 0.000 abstract 1
- 229940055726 pantothenic acid Drugs 0.000 abstract 1
- 235000019161 pantothenic acid Nutrition 0.000 abstract 1
- 235000010356 sorbitol Nutrition 0.000 abstract 1
- 229960004799 tryptophan Drugs 0.000 abstract 1
- 235000002374 tyrosine Nutrition 0.000 abstract 1
- QIVBCDIJIAJPQS-UHFFFAOYSA-N Tryptophan Natural products C1=CC=C2C(CC(N)C(O)=O)=CNC2=C1 QIVBCDIJIAJPQS-UHFFFAOYSA-N 0.000 description 8
- 239000000047 product Substances 0.000 description 5
- 238000003756 stirring Methods 0.000 description 4
- 235000005911 diet Nutrition 0.000 description 3
- 230000006866 deterioration Effects 0.000 description 2
- 230000000378 dietary effect Effects 0.000 description 2
- 239000000546 pharmaceutical excipient Substances 0.000 description 2
- 235000017060 Arachis glabrata Nutrition 0.000 description 1
- 244000105624 Arachis hypogaea Species 0.000 description 1
- 235000010777 Arachis hypogaea Nutrition 0.000 description 1
- 235000018262 Arachis monticola Nutrition 0.000 description 1
- 244000299461 Theobroma cacao Species 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 235000019219 chocolate Nutrition 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 235000020232 peanut Nutrition 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G1/00—Cocoa; Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/30—Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/32—Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds
- A23G1/42—Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds containing microorganisms or enzymes; containing paramedical or dietetical agents, e.g. vitamins
- A23G1/426—Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds containing microorganisms or enzymes; containing paramedical or dietetical agents, e.g. vitamins containing vitamins, antibiotics
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/362—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/364—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing microorganisms or enzymes; containing paramedical or dietetical agents, e.g. vitamins
- A23G3/368—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing microorganisms or enzymes; containing paramedical or dietetical agents, e.g. vitamins containing vitamins, antibiotics
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/44—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing peptides or proteins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/17—Amino acids, peptides or proteins
- A23L33/175—Amino acids
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
Description
La présente invention a pour objet un procédé de fabrication de produits alimentaires, diététiques ou médicamenteux dans lesquels on ajoute pour en modifier certaines de leurs propriétés nutritionnelles des acides aminés, des vitamines, des sels minéraux ou des sucres particuliers. The present invention relates to a process for the manufacture of food, dietetic or medicinal products in which, to modify some of their nutritional properties, amino acids, vitamins, mineral salts or particular sugars are added.
I1 est bien connu que de nombreux produits entrant couramment dans l'alimentation contenant des vitamines, des acides aminés, certains sels minéraux et certains sucres perdent une partie de ceux-ci du fait d'un chauffage excessif lors de leur préparation ou par la mise à leur contact de substances chimiques qui en entraînent la détérioration. It is well known that many products commonly entering the diet containing vitamins, amino acids, certain mineral salts and certain sugars lose part of these due to excessive heating during their preparation or by on contact with chemicals which cause deterioration.
Le but de notre procédé est de protéger ces éléments cités plus haut en les mélangeant dans des conditions particulières avec un produit qui, de par ses caractéristiques physicochimiques, constitue un excipient "inerte" vis à vis des molécules qui nous intéressent. The aim of our process is to protect these elements mentioned above by mixing them under special conditions with a product which, by its physicochemical characteristics, constitutes an "inert" excipient with respect to the molecules which interest us.
Le mélange de deux phases, l'une liquide à une température égale ou supérieure à 400 Celsius et inférieure ou égale à 1000 Celsius et l'autre solide et présentée sous forme de poudre fine à une température égale ou inférieure à 300 Celsius permet de protéger les éléments de la phase solide des effets de l'excès de température vis à vis des produits thermosensibles. The mixture of two phases, one liquid at a temperature equal to or higher than 400 Celsius and lower or equal to 1000 Celsius and the other solid and presented in the form of fine powder at a temperature equal or lower than 300 Celsius allows to protect the elements of the solid phase of the effects of excess temperature with respect to heat-sensitive products.
Le procédé de mélange par simple passage de la phase liquide dans la phase solide poudreuse sous agitation constante permet d'éviter tout risque. The mixing process by simple passage of the liquid phase into the powdery solid phase with constant stirring avoids any risk.
de grumeaux que l'on obtiendrait inévitablement si le mélange se faisait en sens inverse meme sous agitation énergique.of lumps that would inevitably be obtained if the mixing was done in the opposite direction even with vigorous stirring.
L'utilisation d'un produit excipient dont le point de fusion est inférieur ou égal à 400 Celsius constitue une sécurité empêchant toute mauvaise utilisation du produit alimentaire, diététique ou médicamenteux et en particulier de destruction des acides aminés .., des vitamines, des sucres ou sels minéra 2 - eaht dans la composition selon le procédé décrit. The use of an excipient product whose melting point is less than or equal to 400 Celsius constitutes a security preventing any improper use of the food, dietetic or medicinal product and in particular of destruction of amino acids, vitamins, sugars or mineral salts 2 - eaht in the composition according to the process described.
Description du procédé :
Dans un récipient A un prémélange de poudres a est effectué, ces poudres étant constituées par au moins un acide aminé, une vitamine, un sucre ou un sel minéral thermosensible. Ce prémélange est établi de façon à être le plus homogène possible par simple action mécanique et à la température ambiante, dans ure enceinte permettant de limiter le taux d'humidité et à une température ne dépassant pas 300 Celsius.Description of the process:
In a container A, a premix of powders a is carried out, these powders consisting of at least one amino acid, a vitamin, a sugar or a heat-sensitive mineral salt. This premix is established so as to be as homogeneous as possible by simple mechanical action and at room temperature, in an enclosure allowing the humidity to be limited and at a temperature not exceeding 300 Celsius.
Dans un récipient B la phase liquide b constituée elle-même par un mélange préétabli et dont l'un des constituants est un produit solide à la température de 300 Celsius et liquide à une température égale ou supérieure à 500 Celsius, - Nous utiliserons des produits de type pâte à glacer, beurre de cacao, gelées diverses... In a container B the liquid phase b itself constituted by a predetermined mixture and one of the constituents of which is a solid product at the temperature of 300 Celsius and liquid at a temperature equal to or greater than 500 Celsius, - We will use products icing dough, cocoa butter, various jellies ...
Le contenu du récipient B est peu à peu versé à une température constante et au moins égale à 4O0Celsius dans le récipient A de façon progressive et sous agitation constante afin d'éviter la formation de grumeaux. La pâte épaisse obtenue dans un premier temps tendra peu à peu à se ramollir au fur et à mesure que le liquide initialement contenu dans le récipient B passe dans le récipient A et que la température de ce dernier s'élève. The contents of container B are gradually poured at a constant temperature and at least equal to 40 ° C. into container A in a progressive manner and with constant agitation in order to avoid the formation of lumps. The thick paste obtained initially will gradually tend to soften as the liquid initially contained in container B passes into container A and the temperature of the latter rises.
L'opération est poursuivie jusqu'à ce que l'ensemble du contenu du récipient B soit versé dans le récipient A. L'agitation est maintenue pendant toute la durée de l'opération qui ne doit pas durer plus de quelques minutes. On maintiendra la température du récipient A à un niveau tel que l'ensemble du mélange a-b soit piteux ou liquide mais ne se solidifie pas. The operation is continued until the entire content of container B is poured into container A. Stirring is maintained throughout the duration of the operation which should not last more than a few minutes. The temperature of the container A will be maintained at a level such that the whole of the mixture a-b is pitiful or liquid but does not solidify.
C'est cette masse qui pourra être soit versée dans des moules, soit projetée sur un support comestible, et qui constituera la composition selon notre procédé. It is this mass which can either be poured into molds or projected onto an edible support, and which will constitute the composition according to our process.
Il suffira alors de laisser refroidir le mélange final, ou le faire passer dans un tunnel réfrigérant, ou abaisser sa température par tout autre moyen pour obtenir une composition contenant des molécules thermosensibles, des acides aminés, des vitamines, des 21s minéraux ou sucres fragiles ; protégés lors de la fabrication et garanties contre toute détérioration chimique ou physique selon le procédé décrit par le présent brevet. It will then suffice to let the final mixture cool, or pass it through a cooling tunnel, or lower its temperature by any other means to obtain a composition containing heat-sensitive molecules, amino acids, vitamins, minerals or fragile sugars; protected during manufacture and guaranteed against any chemical or physical deterioration according to the process described by this patent.
Exemple 1 : Mélange beurre de cacao / L tryptophane. Example 1: Cocoa butter / L tryptophan mixture.
Un acileaminé, le L tryptophane est mélangé au batteur avec du beurre de cacao liquide à la température de 450 Celsius. An acileaminé, L tryptophan is mixed with a beater with liquid cocoa butter at a temperature of 450 Celsius.
On verse petit à petit sous agitation constante le beurre de cacao chaud (45 C) dans un récipient contenant préalablement du L tryptophane en poudre, et ce, à une température ambiante de 200C. The hot cocoa butter (45 ° C) is gradually poured in with constant stirring into a container previously containing L tryptophan powder, at an ambient temperature of 200C.
Cette opération est effectuée en continu jusqu'à l'obtention d'une pâte homogène semi-liquide à une température de l'ordre de 400C. Lorsque les porportions de L tryptophane/ beurre de cacao sont l'ordre de 0,20 la masse est mélangée dans un tank thermostaté à une température de 450C contenant la quantité de beurre de cacao telle que la concentration de L tryptophane dans le beurre de cacao corresponde à la concentration désirée. This operation is carried out continuously until a homogeneous semi-liquid paste is obtained at a temperature of the order of 400C. When the portions of L tryptophan / cocoa butter are of the order of 0.20 the mass is mixed in a thermostated tank at a temperature of 450C containing the quantity of cocoa butter such as the concentration of L tryptophan in cocoa butter corresponds to the desired concentration.
Exemple 2 :On opère dans les mêmes conditions mais le beurre de cacao est remplacé par de la crème d'arachide et le L tryptophane est remplacé par un mélange isomolaire d'acide L aspartique et de L arginine. Example 2: The operation is carried out under the same conditions, but the cocoa butter is replaced by peanut cream and the L tryptophan is replaced by an isomolar mixture of L aspartic acid and L arginine.
Exemple 3 : Mêmes conditions que dans l'exemple 1 mais où le L tryptophane est remplacé par du chlorure de magnésium et le beurre de cacao par du chocolat. Example 3: Same conditions as in Example 1 but where L tryptophan is replaced by magnesium chloride and cocoa butter by chocolate.
Exemple 4 : Mêmes conditions que dans l'exemple 1 mais où le L tryptophane est remplacé par un mélange isomolaire fructose-sorbitol et où le beurre de cacao est remplacé par une pâte de fruit gél-ifiée. Example 4: Same conditions as in Example 1 but where the L tryptophan is replaced by an isomolar mixture of fructose-sorbitol and where the cocoa butter is replaced by a jellied fruit paste.
Claims (13)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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FR8207715A FR2526273A1 (en) | 1982-05-04 | 1982-05-04 | Mixing heat sensitive food and medicinal substances - with material that melts above 40 deg. C and is solid below 30 Deg. C. |
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FR8207715A FR2526273A1 (en) | 1982-05-04 | 1982-05-04 | Mixing heat sensitive food and medicinal substances - with material that melts above 40 deg. C and is solid below 30 Deg. C. |
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FR2526273A1 true FR2526273A1 (en) | 1983-11-10 |
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FR8207715A Pending FR2526273A1 (en) | 1982-05-04 | 1982-05-04 | Mixing heat sensitive food and medicinal substances - with material that melts above 40 deg. C and is solid below 30 Deg. C. |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0184121A2 (en) * | 1984-12-04 | 1986-06-11 | Biodyn AG | Saccharose-containing, orally administered, foodstuffs, beverages, delicacies and pharmaceutical preparations |
FR2603460A1 (en) * | 1986-09-04 | 1988-03-11 | Duvert Jacqueline | Food product which can be used as supplement and process for preparing it |
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NL296020A (en) * | 1962-08-16 | |||
US2933392A (en) * | 1953-04-15 | 1960-04-19 | Nat Dairy Prod Corp | Composition containing vitamin a |
FR2181462A1 (en) * | 1972-04-25 | 1973-12-07 | Johnson & Johnson | Low residue dietetic mixts - contg amino acids and caloric substances |
US3992556A (en) * | 1973-05-07 | 1976-11-16 | Vitamins, Inc. | Supplemented food product |
FR2353234A1 (en) * | 1976-06-01 | 1977-12-30 | Ueno Seiyaku Oyo Kenkyujo Kk | CARBOHYDRATE ADDITIVE FOR FOOD AND ITS PREPARATION |
FR2392675A1 (en) * | 1976-11-23 | 1978-12-29 | Unilever Nv | PREPARATION OF PREMIXES USEFUL FOR THE MANUFACTURE OF FOODSTUFFS |
EP0034034A1 (en) * | 1980-02-08 | 1981-08-19 | Ajinomoto Co., Inc. | Nutrient composition |
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US2933392A (en) * | 1953-04-15 | 1960-04-19 | Nat Dairy Prod Corp | Composition containing vitamin a |
NL296020A (en) * | 1962-08-16 | |||
FR2181462A1 (en) * | 1972-04-25 | 1973-12-07 | Johnson & Johnson | Low residue dietetic mixts - contg amino acids and caloric substances |
US3992556A (en) * | 1973-05-07 | 1976-11-16 | Vitamins, Inc. | Supplemented food product |
FR2353234A1 (en) * | 1976-06-01 | 1977-12-30 | Ueno Seiyaku Oyo Kenkyujo Kk | CARBOHYDRATE ADDITIVE FOR FOOD AND ITS PREPARATION |
FR2392675A1 (en) * | 1976-11-23 | 1978-12-29 | Unilever Nv | PREPARATION OF PREMIXES USEFUL FOR THE MANUFACTURE OF FOODSTUFFS |
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Publication number | Priority date | Publication date | Assignee | Title |
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EP0184121A2 (en) * | 1984-12-04 | 1986-06-11 | Biodyn AG | Saccharose-containing, orally administered, foodstuffs, beverages, delicacies and pharmaceutical preparations |
EP0184121A3 (en) * | 1984-12-04 | 1988-03-02 | Biodyn Ag | Dental saving additive for saccharose-containing foodstuffs, beverages, delicacies and pharmaceutical preparations, process for their preparation, products containing it and process for preparing a beverage |
FR2603460A1 (en) * | 1986-09-04 | 1988-03-11 | Duvert Jacqueline | Food product which can be used as supplement and process for preparing it |
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