FR2442794A1 - Alkaline orthophosphate soln. prodn. - by continuous neutralisation of phosphoric acid in single multicompartment reaction vessel - Google Patents
Alkaline orthophosphate soln. prodn. - by continuous neutralisation of phosphoric acid in single multicompartment reaction vesselInfo
- Publication number
- FR2442794A1 FR2442794A1 FR7835131A FR7835131A FR2442794A1 FR 2442794 A1 FR2442794 A1 FR 2442794A1 FR 7835131 A FR7835131 A FR 7835131A FR 7835131 A FR7835131 A FR 7835131A FR 2442794 A1 FR2442794 A1 FR 2442794A1
- Authority
- FR
- France
- Prior art keywords
- prodn
- phosphoric acid
- reaction vessel
- soln
- continuous
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1862—Stationary reactors having moving elements inside placed in series
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0086—Processes carried out with a view to control or to change the pH-value; Applications of buffer salts; Neutralisation reactions
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/30—Alkali metal phosphates
- C01B25/301—Preparation from liquid orthophosphoric acid or from an acid solution or suspension of orthophosphates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
- B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
- B01J2219/00058—Temperature measurement
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00164—Controlling or regulating processes controlling the flow
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00182—Controlling or regulating processes controlling the level of reactants in the reactor vessel
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Luminescent Compositions (AREA)
Abstract
Prodn. of solns. of alkaline orthophosphates effected by continuous neutralisation of thermic or wet process phosphoric acid in a single reaction vessel used for prepn. of polyphosphates e.g. sodium tripolyphosphate which is a basic material for the preparation of washing powders, liqs. etc. Process allows rigorous control of the ratio of acid to base to give the desired polyphosphate after calcination of the orthophosphate; in the past this control has usually necessitated batch processing or when a continuous process was employed has necessitated several (a cascade) reaction vessels.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7835131A FR2442794A1 (en) | 1978-12-01 | 1978-12-01 | Alkaline orthophosphate soln. prodn. - by continuous neutralisation of phosphoric acid in single multicompartment reaction vessel |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7835131A FR2442794A1 (en) | 1978-12-01 | 1978-12-01 | Alkaline orthophosphate soln. prodn. - by continuous neutralisation of phosphoric acid in single multicompartment reaction vessel |
Publications (1)
Publication Number | Publication Date |
---|---|
FR2442794A1 true FR2442794A1 (en) | 1980-06-27 |
Family
ID=9216081
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7835131A Withdrawn FR2442794A1 (en) | 1978-12-01 | 1978-12-01 | Alkaline orthophosphate soln. prodn. - by continuous neutralisation of phosphoric acid in single multicompartment reaction vessel |
Country Status (1)
Country | Link |
---|---|
FR (1) | FR2442794A1 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1298147A2 (en) * | 2001-09-28 | 2003-04-02 | Nippon Shokubai Co., Ltd. | Apparatus and method for preparation and supply of polymerization inhibitor |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB841416A (en) * | 1958-04-26 | 1960-07-13 | Drew & Co Inc E F | Improvements in or relating to apparatus for carrying out chemical reactions |
US3125420A (en) * | 1964-03-17 | Compact reactor for production of fertilizer solids | ||
US3251657A (en) * | 1962-05-11 | 1966-05-17 | Hoechst Ag | Reactor for the manufacture of polyethylene phthalates |
FR2074119A5 (en) * | 1969-12-23 | 1971-10-01 | Sir Soc Italiana Resine Spa | |
FR2087779A5 (en) * | 1970-02-09 | 1971-12-31 | Parkson Corp | |
FR2211282A1 (en) * | 1972-12-21 | 1974-07-19 | Perstorp Ab | |
GB1377360A (en) * | 1970-12-08 | 1974-12-11 | Fisons Ltd | Reactor |
JPS5278770A (en) * | 1975-12-26 | 1977-07-02 | Nobuko Asayama | Closed square curving reactor |
-
1978
- 1978-12-01 FR FR7835131A patent/FR2442794A1/en not_active Withdrawn
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3125420A (en) * | 1964-03-17 | Compact reactor for production of fertilizer solids | ||
GB841416A (en) * | 1958-04-26 | 1960-07-13 | Drew & Co Inc E F | Improvements in or relating to apparatus for carrying out chemical reactions |
US3251657A (en) * | 1962-05-11 | 1966-05-17 | Hoechst Ag | Reactor for the manufacture of polyethylene phthalates |
FR2074119A5 (en) * | 1969-12-23 | 1971-10-01 | Sir Soc Italiana Resine Spa | |
FR2087779A5 (en) * | 1970-02-09 | 1971-12-31 | Parkson Corp | |
GB1377360A (en) * | 1970-12-08 | 1974-12-11 | Fisons Ltd | Reactor |
FR2211282A1 (en) * | 1972-12-21 | 1974-07-19 | Perstorp Ab | |
JPS5278770A (en) * | 1975-12-26 | 1977-07-02 | Nobuko Asayama | Closed square curving reactor |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1298147A2 (en) * | 2001-09-28 | 2003-04-02 | Nippon Shokubai Co., Ltd. | Apparatus and method for preparation and supply of polymerization inhibitor |
EP1298147A3 (en) * | 2001-09-28 | 2004-02-04 | Nippon Shokubai Co., Ltd. | Apparatus and method for preparation and supply of polymerization inhibitor |
US6899452B2 (en) | 2001-09-28 | 2005-05-31 | Nippon Shokubai Co., Inc. | Apparatus and method for preparation and supply of polymerization inhibitor |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ST | Notification of lapse |