FR2421847A1 - INTEGRATED AMMONIA-UREE SYNTHESIS PROCESS - Google Patents

INTEGRATED AMMONIA-UREE SYNTHESIS PROCESS

Info

Publication number
FR2421847A1
FR2421847A1 FR7907848A FR7907848A FR2421847A1 FR 2421847 A1 FR2421847 A1 FR 2421847A1 FR 7907848 A FR7907848 A FR 7907848A FR 7907848 A FR7907848 A FR 7907848A FR 2421847 A1 FR2421847 A1 FR 2421847A1
Authority
FR
France
Prior art keywords
ammonia
urea
carbon dioxide
solution
carbamate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7907848A
Other languages
French (fr)
Other versions
FR2421847B1 (en
Inventor
Vincenzo Lagana
Francesco Saviano
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SnamProgetti SpA
Original Assignee
SnamProgetti SpA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SnamProgetti SpA filed Critical SnamProgetti SpA
Publication of FR2421847A1 publication Critical patent/FR2421847A1/en
Application granted granted Critical
Publication of FR2421847B1 publication Critical patent/FR2421847B1/fr
Granted legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C07C273/04Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds from carbon dioxide and ammonia

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Procédé intégré de synthèse ammoniac-urée. Ce procédé consiste à épurer l'anhydride carbonique d'un courant gazeux provenant de la reformation de vapeur d'hydrocarbures, par action d'une solution d'ammoniac très concentrée, puis par action d'une solution ammoniaquée de carbonate d'ammonium, à envoyer la solution de carbamate obtenue au réacteur d'urée, à décharger de celui-ci la solution d'urée contenant du carbamate non converti et de l'ammoniac en excès, à décomposer ledit carbamate et à envoyer l'ammoniac dégagé au réacteur d'urée en même temps que l'anhydride carbonique à décharger la solution d'urée à un épurateur adiabatique, ou le gaz d'épuration est essentiellement composé par l'hydrogène et l'azote, à éliminer l'ammoniac et l'anhydride carbonique avec l'eau de l'épurateur adiabatique et à condenser l'ammoniac et l'anhydride carbonique par échange thermique, à envoyer le courant d'hydrogène et d'azote à la méthanisation et à la synthèse de l'ammoniac et à concentrer la solution d'urée directement jusqu'à obtention d'une masse fondue d'urée.Integrated ammonia-urea synthesis process. This process consists in purifying carbon dioxide from a gas stream originating from the reformation of hydrocarbon vapor, by the action of a highly concentrated ammonia solution, then by the action of an ammonia-based solution of ammonium carbonate, sending the carbamate solution obtained to the urea reactor, discharging therefrom the urea solution containing unconverted carbamate and excess ammonia, decomposing said carbamate and sending the ammonia released to the reactor of urea at the same time as carbon dioxide to discharge the urea solution to an adiabatic scrubber, or the scrubbing gas is mainly composed of hydrogen and nitrogen, to remove ammonia and anhydride carbon dioxide with the water from the adiabatic scrubber and to condense the ammonia and carbon dioxide by heat exchange, to send the stream of hydrogen and nitrogen to the methanization and the synthesis of ammonia and to concentrate the urea solution directly until a urea melt.

FR7907848A 1978-04-05 1979-03-28 INTEGRATED AMMONIA-UREE SYNTHESIS PROCESS Granted FR2421847A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
IT21993/78A IT1094295B (en) 1978-04-05 1978-04-05 INTEGRATED AMMONIA-UREA PROCEDURE

Publications (2)

Publication Number Publication Date
FR2421847A1 true FR2421847A1 (en) 1979-11-02
FR2421847B1 FR2421847B1 (en) 1982-10-22

Family

ID=11189914

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7907848A Granted FR2421847A1 (en) 1978-04-05 1979-03-28 INTEGRATED AMMONIA-UREE SYNTHESIS PROCESS

Country Status (23)

Country Link
JP (1) JPS54132525A (en)
AU (1) AU519817B2 (en)
BE (1) BE875346A (en)
BR (1) BR7902122A (en)
CA (1) CA1110659A (en)
CH (1) CH637633A5 (en)
CS (1) CS230563B2 (en)
DD (1) DD142709A5 (en)
DE (1) DE2913793C3 (en)
DK (1) DK139179A (en)
EG (1) EG13847A (en)
ES (1) ES479940A1 (en)
FR (1) FR2421847A1 (en)
GB (1) GB2018249B (en)
IE (1) IE48099B1 (en)
IN (1) IN150631B (en)
IT (1) IT1094295B (en)
LU (1) LU81113A1 (en)
MX (1) MX151216A (en)
NL (1) NL7902566A (en)
PL (1) PL116665B1 (en)
SE (1) SE432591B (en)
SU (1) SU1225485A3 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61109760A (en) * 1984-11-02 1986-05-28 Toyo Eng Corp Production of urea

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1907025A1 (en) * 1968-02-12 1969-09-18 Sumitomo Chemical Co Process for the production of urea
DE1903117A1 (en) * 1968-01-23 1969-11-27 Sumitomo Chemical Co Process for the production of urea
FR2274610A1 (en) * 1974-06-12 1976-01-09 Snam Progetti INTEGRATED PROCESS FOR THE PREPARATION OF UREA AND AMMONIA
FR2305391A1 (en) * 1975-03-28 1976-10-22 Snam Progetti FLEXIBLE INTEGRATED PROCESS FOR MANUFACTURING AMMONIA AND UREA
FR2375198A1 (en) * 1976-12-23 1978-07-21 Snam Progetti INTEGRATED PROCESS FOR MANUFACTURING AMMONIA AND UREA, FOR THE PRODUCTION OF UREA

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1903117A1 (en) * 1968-01-23 1969-11-27 Sumitomo Chemical Co Process for the production of urea
DE1907025A1 (en) * 1968-02-12 1969-09-18 Sumitomo Chemical Co Process for the production of urea
FR2274610A1 (en) * 1974-06-12 1976-01-09 Snam Progetti INTEGRATED PROCESS FOR THE PREPARATION OF UREA AND AMMONIA
FR2305391A1 (en) * 1975-03-28 1976-10-22 Snam Progetti FLEXIBLE INTEGRATED PROCESS FOR MANUFACTURING AMMONIA AND UREA
FR2375198A1 (en) * 1976-12-23 1978-07-21 Snam Progetti INTEGRATED PROCESS FOR MANUFACTURING AMMONIA AND UREA, FOR THE PRODUCTION OF UREA

Also Published As

Publication number Publication date
BR7902122A (en) 1979-12-04
ES479940A1 (en) 1979-12-01
IE48099B1 (en) 1984-09-19
GB2018249A (en) 1979-10-17
CS230563B2 (en) 1984-08-13
SE432591B (en) 1984-04-09
FR2421847B1 (en) 1982-10-22
PL214649A1 (en) 1979-12-17
DD142709A5 (en) 1980-07-09
IT1094295B (en) 1985-07-26
GB2018249B (en) 1982-09-02
JPS54132525A (en) 1979-10-15
SU1225485A3 (en) 1986-04-15
CA1110659A (en) 1981-10-13
CH637633A5 (en) 1983-08-15
PL116665B1 (en) 1981-06-30
NL7902566A (en) 1979-10-09
DE2913793B2 (en) 1980-06-04
IN150631B (en) 1982-11-20
IE790706L (en) 1979-10-05
AU4487679A (en) 1979-10-18
MX151216A (en) 1984-10-11
DK139179A (en) 1979-10-06
SE7903018L (en) 1979-10-06
DE2913793C3 (en) 1981-05-27
LU81113A1 (en) 1979-06-19
EG13847A (en) 1982-12-31
IT7821993A0 (en) 1978-04-05
DE2913793A1 (en) 1979-10-11
BE875346A (en) 1979-10-05
AU519817B2 (en) 1981-12-24

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Legal Events

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