FR2386519A1 - Procede de preparation de l'acide naphtalene-1,3,6-trisulfonique par sulfonation du naphtalene a l'aide d'acide sulfurique et d'oleum - Google Patents

Procede de preparation de l'acide naphtalene-1,3,6-trisulfonique par sulfonation du naphtalene a l'aide d'acide sulfurique et d'oleum

Info

Publication number
FR2386519A1
FR2386519A1 FR7810428A FR7810428A FR2386519A1 FR 2386519 A1 FR2386519 A1 FR 2386519A1 FR 7810428 A FR7810428 A FR 7810428A FR 7810428 A FR7810428 A FR 7810428A FR 2386519 A1 FR2386519 A1 FR 2386519A1
Authority
FR
France
Prior art keywords
naphthalene
oleum
temperature
sulfuric acid
sulphonation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7810428A
Other languages
English (en)
Other versions
FR2386519B1 (fr
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer AG filed Critical Bayer AG
Publication of FR2386519A1 publication Critical patent/FR2386519A1/fr
Application granted granted Critical
Publication of FR2386519B1 publication Critical patent/FR2386519B1/fr
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

On introduit simultanément du naphtalène et une partie de l'oléum, la plus grande partie de la quantité totale d'oléum mise en oeuvre, à une température de 140 à 240 degrés C dans de l'acide sulfurique ou de l'oléum à basse concentration, on maintient la température pendant quelque temps entre 140 et 240 degrés C, on ajoute le restant d'oléum à une température de 140 à 240 degrés C et on agite encore quelque temps à ce niveau de température. Ce procédé donne de meilleurs rendements et consomme moins d'énergie que les procédés de la technique antérieure.
FR7810428A 1977-04-09 1978-04-07 Procede de preparation de l'acide naphtalene-1,3,6-trisulfonique par sulfonation du naphtalene a l'aide d'acide sulfurique et d'oleum Granted FR2386519A1 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE2716029A DE2716029C2 (de) 1977-04-09 1977-04-09 Verfahren zur Herstellung von Naphthalin-1,3,6-trisulfonsäure

Publications (2)

Publication Number Publication Date
FR2386519A1 true FR2386519A1 (fr) 1978-11-03
FR2386519B1 FR2386519B1 (fr) 1983-11-18

Family

ID=6006076

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7810428A Granted FR2386519A1 (fr) 1977-04-09 1978-04-07 Procede de preparation de l'acide naphtalene-1,3,6-trisulfonique par sulfonation du naphtalene a l'aide d'acide sulfurique et d'oleum

Country Status (9)

Country Link
US (1) US4180521A (fr)
JP (1) JPS53127449A (fr)
BE (1) BE865773A (fr)
BR (1) BR7802174A (fr)
CH (1) CH634043A5 (fr)
DE (1) DE2716029C2 (fr)
FR (1) FR2386519A1 (fr)
GB (1) GB1577696A (fr)
IT (1) IT1102569B (fr)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0012260A1 (fr) * 1978-12-09 1980-06-25 Bayer Ag Produits de sulfurisation du naphtalène, procédé pour leur préparation et leur utilisation
EP0013558A1 (fr) * 1979-01-13 1980-07-23 Bayer Ag Procédé de préparation de l'acide naphtalène-1,3,5-trisulfonique

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5110981A (en) * 1991-06-18 1992-05-05 Henkel Corporation Process for making alkyl naphthalene sulfonate surfactants

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5096552A (fr) * 1973-12-28 1975-07-31

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1311090A (en) * 1919-07-22 Lestee albert pratt
JPS5629862B2 (fr) * 1974-05-08 1981-07-10
JPS524575A (en) * 1975-07-01 1977-01-13 Asahi Chemical Ind Manufacturing of mono dimensional elongation poly ethylene film

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5096552A (fr) * 1973-12-28 1975-07-31

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
CA1975 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0012260A1 (fr) * 1978-12-09 1980-06-25 Bayer Ag Produits de sulfurisation du naphtalène, procédé pour leur préparation et leur utilisation
EP0013558A1 (fr) * 1979-01-13 1980-07-23 Bayer Ag Procédé de préparation de l'acide naphtalène-1,3,5-trisulfonique

Also Published As

Publication number Publication date
JPS53127449A (en) 1978-11-07
IT7848790A0 (it) 1978-04-07
FR2386519B1 (fr) 1983-11-18
BE865773A (fr) 1978-10-09
IT1102569B (it) 1985-10-07
DE2716029C2 (de) 1986-01-09
BR7802174A (pt) 1978-12-19
CH634043A5 (de) 1983-01-14
GB1577696A (en) 1980-10-29
US4180521A (en) 1979-12-25
DE2716029A1 (de) 1978-10-19

Similar Documents

Publication Publication Date Title
FR2457880A1 (fr)
FR2386519A1 (fr) Procede de preparation de l'acide naphtalene-1,3,6-trisulfonique par sulfonation du naphtalene a l'aide d'acide sulfurique et d'oleum
Yoshimori et al. Preparation of sulphamic acid single crystals and their assay by precise coulometric titration
Kharasch et al. Derivatives of Sulfenic Acids. XVII. The Hydrolysis of 2, 4-Dinitrobenzenesulfenyl Chloride
FR2470808A1 (fr) Procede d'obtention d'hydrogene par electrolyse et cellule d'electrolyse adaptee a ce procede
ATE40881T1 (de) Verfahren zur herstellung von acyloxibenzolsulfonsaeuren und deren salzen.
GB1468647A (en) Process for the preparation of 2-nitro-4,6-dichloro-5-methyl phenol
SE7714689L (sv) Forfarande for framstellning av fluorvete fran en vattenlosning av fluorvete och svavelsyra
FR2372151A1 (fr) Preparation de sels d'acides monoalcoyl sulfuriques secondaires
GB1393929A (en) Production of di-4-chlorophenyl sulphone
FR2362159A1 (fr) Sels metalliques cristallises de b-nicotinamide-adenine-dinucleotide et leur procede de preparation
JPS5748961A (en) Preparation of 2,4-diaminobenzenesulfonic acid
Suter et al. The Sulfonation of Isobutylene. I. 2-Methylpropene-1, 3-disulfonic Acid and Related Compounds
US3243454A (en) Process of preparing alkali metal isethionates
US2693487A (en) Monosulfonation of benzene
US4710322A (en) Process for the preparation of alkali metal and alkaline earth salts of benzaldehyde-2,4-di-sulfonic acid
FR2385684A1 (fr) Procede de preparation de la 1-amino-2-bromo-4-hydroxyanthraquinone
FR2398722A1 (fr) Perfectionnements a la preparation de solutions aqueuses de sels alcalins de l'acide 2-hydroxy-1-naphtalenesulfonique
FR2403972A1 (fr) Procede de concentration et de purification de solutions aqueuses d'acide sulfurique
SU740758A1 (ru) Способ получени метаниловой кислоты
JPS54130620A (en) Preparation of alpha-quinacridone pigment
SU290684A1 (ru) Способ разделени стабильных изотопов
Chase et al. 8. A spectroscopic method for the determination of the ortho: para-ratio in phenolsulphonates
SU218911A1 (ru) Способ получени -полисульфокислот антрахинона и хлорантрахинона
SU296768A1 (ru) Способ получения натриевых солей моносульфокислот диметиланилина

Legal Events

Date Code Title Description
ST Notification of lapse