FR2318822A1 - Procede de fabrication de particules exactement spheriques de gel de silice ayant une grosseur reglee et des dimensions de pores reglees - Google Patents

Procede de fabrication de particules exactement spheriques de gel de silice ayant une grosseur reglee et des dimensions de pores reglees

Info

Publication number
FR2318822A1
FR2318822A1 FR7622471A FR7622471A FR2318822A1 FR 2318822 A1 FR2318822 A1 FR 2318822A1 FR 7622471 A FR7622471 A FR 7622471A FR 7622471 A FR7622471 A FR 7622471A FR 2318822 A1 FR2318822 A1 FR 2318822A1
Authority
FR
France
Prior art keywords
regulated
manufacturing
silica gel
spherical particles
pore dimensions
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7622471A
Other languages
English (en)
French (fr)
Other versions
FR2318822B1 (show.php
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Czech Academy of Sciences CAS
Original Assignee
Czech Academy of Sciences CAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Czech Academy of Sciences CAS filed Critical Czech Academy of Sciences CAS
Publication of FR2318822A1 publication Critical patent/FR2318822A1/fr
Application granted granted Critical
Publication of FR2318822B1 publication Critical patent/FR2318822B1/fr
Granted legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/103—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate comprising silica
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/152—Preparation of hydrogels
    • C01B33/154—Preparation of hydrogels by acidic treatment of aqueous silicate solutions
    • C01B33/1546—Preparation of hydrogels by acidic treatment of aqueous silicate solutions the first formed hydrosol being converted to a hydrogel by introduction into an organic medium immiscible or only partly miscible with water

Landscapes

  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Silicon Compounds (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
FR7622471A 1975-07-25 1976-07-23 Procede de fabrication de particules exactement spheriques de gel de silice ayant une grosseur reglee et des dimensions de pores reglees Granted FR2318822A1 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CS7500005256A CS179184B1 (en) 1975-07-25 1975-07-25 Method for preparation of precisely spherical particles of silica gel with controlled size and controled size pores.

Publications (2)

Publication Number Publication Date
FR2318822A1 true FR2318822A1 (fr) 1977-02-18
FR2318822B1 FR2318822B1 (show.php) 1982-12-17

Family

ID=5397101

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7622471A Granted FR2318822A1 (fr) 1975-07-25 1976-07-23 Procede de fabrication de particules exactement spheriques de gel de silice ayant une grosseur reglee et des dimensions de pores reglees

Country Status (6)

Country Link
US (1) US4104363A (show.php)
JP (1) JPS5229498A (show.php)
CS (1) CS179184B1 (show.php)
DE (1) DE2633198C2 (show.php)
FR (1) FR2318822A1 (show.php)
SE (1) SE418074B (show.php)

Families Citing this family (42)

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CS196794B1 (en) * 1977-09-23 1980-04-30 Dusan Berek Method of preparation of spherical microelements
CA1177811A (en) 1981-04-13 1984-11-13 Theo G. Spek Process for the preparation of silica particles; silica particles with a narrow pore diameter distribution, catalysts made therefrom and use of these catalysts
JPS5926911A (ja) * 1982-08-04 1984-02-13 Toyo Soda Mfg Co Ltd 球状多孔性シリカゲルおよびその製造法
JPS6021802A (ja) * 1983-07-15 1985-02-04 Daido Sanso Kk 均一な細孔を有する金属酸化物、その製造方法およびその金属酸化物からなる触媒用担体
DK251984D0 (da) * 1984-05-22 1984-05-22 Niro Atomizer As Fremgangsmaade til fremstilling af polymerpartikler
CS253971B1 (en) * 1984-12-11 1987-12-17 Peter Hermann Production method of high active biological effective compounds immobilized on carrier
US4649037A (en) * 1985-03-29 1987-03-10 Allied Corporation Spray-dried inorganic oxides from non-aqueous gels or solutions
DE3616133A1 (de) * 1985-09-25 1987-11-19 Merck Patent Gmbh Kugelfoermige sio(pfeil abwaerts)2(pfeil abwaerts)-partikel
GB8529970D0 (en) * 1985-12-05 1986-01-15 Unilever Plc Spheroidal silica
CA1311737C (en) * 1986-07-28 1992-12-22 The Dow Chemical Company Process of making uniform size porous silica spheres
US5145578A (en) * 1987-07-03 1992-09-08 Shiseido Company Ltd. Packing material for liquid chromatography
US5200471A (en) * 1990-11-05 1993-04-06 Minnesota Mining And Manufacturing Company Biomolecules covalently immobilized with a high bound specific biological activity and method of preparing same
IT1275412B (it) * 1995-06-01 1997-08-05 Enichem Spa Procedimento per la preparazione di ossidi misti silice-allumina porosi in forma sferica
US5807607A (en) * 1995-11-16 1998-09-15 Texas Instruments Incorporated Polyol-based method for forming thin film aerogels on semiconductor substrates
US6380105B1 (en) 1996-11-14 2002-04-30 Texas Instruments Incorporated Low volatility solvent-based method for forming thin film nanoporous aerogels on semiconductor substrates
US6130152A (en) 1995-11-16 2000-10-10 Texas Instruments Incorporated Aerogel thin film formation from multi-solvent systems
US6319852B1 (en) 1995-11-16 2001-11-20 Texas Instruments Incorporated Nanoporous dielectric thin film formation using a post-deposition catalyst
US6686035B2 (en) 1999-02-05 2004-02-03 Waters Investments Limited Porous inorganic/organic hybrid particles for chromatographic separations and process for their preparation
US6528167B2 (en) 2001-01-31 2003-03-04 Waters Investments Limited Porous hybrid particles with organic groups removed from the surface
US7250214B2 (en) 2001-08-09 2007-07-31 Waters Investments Limited Porous inorganic/organic hybrid monolith materials for chromatographic separations and process for their preparation
US7026362B2 (en) 2001-10-09 2006-04-11 Simax Technologies, Inc. Sol-gel process utilizing reduced mixing temperatures
US7125912B2 (en) * 2001-10-09 2006-10-24 Simax Technologies, Inc. Doped sol-gel materials and method of manufacture utilizing reduced mixing temperatures
US7000885B2 (en) * 2002-02-01 2006-02-21 Simax Technologies, Inc. Apparatus and method for forming a sol-gel monolith utilizing multiple casting
US20040194511A1 (en) * 2002-02-01 2004-10-07 Chih-Hsing Cheng Sol-gel-derived halogen-doped glass
US20030147606A1 (en) * 2002-02-01 2003-08-07 Shiho Wang Sol-gel-based optical preforms and methods of manufacture
US6928220B2 (en) * 2002-02-01 2005-08-09 Simax Technologies, Inc. Sol-gel-derived optical fiber preform and method of manufacture
US7001568B2 (en) * 2002-02-01 2006-02-21 Simax Technologies, Inc. Method of removing liquid from pores of a sol-gel monolith
WO2004041398A2 (en) 2002-10-30 2004-05-21 Waters Investments Limited Porous inorganic/organic hybrid materials and preparation thereof
EP1585574A4 (en) * 2002-12-20 2006-04-26 Cardiac Inv S Unltd Inc DEVICE AND METHOD FOR IMPLANTING LEFT-VATRICULAR PIPE MACHINE IN KORONARSINUS
DE112005000269T5 (de) * 2004-02-17 2007-01-25 Waters Investments Ltd., New Castle Poröse Hybridmonolithmaterialien mit von der Oberfläche entfernten organischen Gruppen
WO2005096785A2 (en) * 2004-04-09 2005-10-20 Synergy Innovations, Inc. System and method of manufacturing mono-sized-disbursed spherical particles
JP5308665B2 (ja) 2004-07-30 2013-10-09 ウオーターズ・テクノロジーズ・コーポレイシヨン クロマトグラフィー分離用の秩序領域を有する多孔質無機／有機のハイブリッド材料およびこれらの調製方法
US10773186B2 (en) 2004-07-30 2020-09-15 Waters Technologies Corporation Porous inorganic/organic hybrid materials with ordered domains for chromatographic separations and processes for their preparation
JP2010515804A (ja) 2007-01-12 2010-05-13 ウオーターズ・テクノロジーズ・コーポレイシヨン クロマトグラフ分離用多孔質炭素−ヘテロ原子−ケイ素ハイブリッド無機／有機材料およびその調製のための方法
WO2012018596A2 (en) 2010-07-26 2012-02-09 Waters Technologies Corporation Superficially porous materials comprising a substantially nonporous hybrid core having narrow particle size distribution; process for the preparation thereof; and use thereof for chromatographic separations
WO2010141426A1 (en) 2009-06-01 2010-12-09 Waters Technologies Corporation Hybrid material for chromatographic separations
US11439977B2 (en) 2009-06-01 2022-09-13 Waters Technologies Corporation Hybrid material for chromatographic separations comprising a superficially porous core and a surrounding material
MY178616A (en) 2012-09-17 2020-10-19 Grace W R & Co Chromatography media and devices
PL3094390T3 (pl) 2014-01-16 2021-12-06 W.R. Grace & Co. - Conn. Nośniki do chromatografii powinowactwa i urządzenia do chromatografii
PL3137209T3 (pl) 2014-05-02 2023-01-02 W.R. Grace & Co. - Conn. Funkcjonalizowany materiał nośnikowy i sposoby wytwarzania oraz stosowania funkcjonalizowanego materiału nośnikowego
CN107921407B (zh) 2015-06-05 2022-07-05 格雷斯公司 生物处理吸附澄清剂及其制备和使用方法
CN109414681A (zh) 2016-03-06 2019-03-01 沃特世科技公司 用于色谱分离的包含表面多孔芯和周围材料的杂化材料

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2765242A (en) * 1952-02-29 1956-10-02 Du Pont Process of making reinforced silica gel and esterified silica gel
FR1169013A (fr) * 1955-12-23 1958-12-19 Columbia Southern Chem Corp Perfectionnements à la silice finement divisée

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1772055A (en) * 1927-03-12 1930-08-05 Silica Gel Corp Gel and method of preparing same
US2395524A (en) * 1941-07-22 1946-02-26 Houdry Process Corp Method of preparing porous silica
US2474910A (en) * 1944-03-04 1949-07-05 Standard Oil Dev Co Preparation of spherical gel particles
US2782869A (en) * 1951-07-02 1957-02-26 Phillips Petroleum Co Preparation of silica gels
US3321276A (en) * 1965-10-23 1967-05-23 Owens Illinois Inc Preparation of silica gel
DE1667078B2 (de) * 1967-10-31 1979-07-19 W.R. Grace & Co., New York, N.Y. (V.St.A.) Verfahren zur Herstellung von kugelförmigen Kieselsäurehydrogelen
US3819811A (en) * 1968-08-06 1974-06-25 Nat Petro Chem Preparation of silica gels
GB1285714A (en) * 1968-11-25 1972-08-16 Bp Chem Int Ltd Production of silica gels

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2765242A (en) * 1952-02-29 1956-10-02 Du Pont Process of making reinforced silica gel and esterified silica gel
FR1169013A (fr) * 1955-12-23 1958-12-19 Columbia Southern Chem Corp Perfectionnements à la silice finement divisée

Also Published As

Publication number Publication date
SE418074B (sv) 1981-05-04
US4104363A (en) 1978-08-01
DE2633198C2 (de) 1986-03-20
JPS5229498A (en) 1977-03-05
CS179184B1 (en) 1977-10-31
DE2633198A1 (de) 1977-02-10
FR2318822B1 (show.php) 1982-12-17
SE7608313L (sv) 1977-01-26

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