FR2309564A1 - Procede de preparation d'hydroxocobalamine et de ses sels - Google Patents
Procede de preparation d'hydroxocobalamine et de ses selsInfo
- Publication number
- FR2309564A1 FR2309564A1 FR7514219A FR7514219A FR2309564A1 FR 2309564 A1 FR2309564 A1 FR 2309564A1 FR 7514219 A FR7514219 A FR 7514219A FR 7514219 A FR7514219 A FR 7514219A FR 2309564 A1 FR2309564 A1 FR 2309564A1
- Authority
- FR
- France
- Prior art keywords
- cyanocobalamin
- redn
- prepn
- absence
- borohydride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- RMRCNWBMXRMIRW-BYFNXCQMSA-M cyanocobalamin Chemical compound N#C[Co+]N([C@]1([H])[C@H](CC(N)=O)[C@]\2(CCC(=O)NC[C@H](C)OP(O)(=O)OC3[C@H]([C@H](O[C@@H]3CO)N3C4=CC(C)=C(C)C=C4N=C3)O)C)C/2=C(C)\C([C@H](C/2(C)C)CCC(N)=O)=N\C\2=C\C([C@H]([C@@]/2(CC(N)=O)C)CCC(N)=O)=N\C\2=C(C)/C2=N[C@]1(C)[C@@](C)(CC(N)=O)[C@@H]2CCC(N)=O RMRCNWBMXRMIRW-BYFNXCQMSA-M 0.000 title abstract 8
- 235000000639 cyanocobalamin Nutrition 0.000 title abstract 4
- 239000011666 cyanocobalamin Substances 0.000 title abstract 4
- 229960002104 cyanocobalamin Drugs 0.000 title abstract 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 title abstract 2
- 229910052760 oxygen Inorganic materials 0.000 title abstract 2
- 239000001301 oxygen Substances 0.000 title abstract 2
- 239000002253 acid Substances 0.000 title 1
- FDJOLVPMNUYSCM-WZHZPDAFSA-L cobalt(3+);[(2r,3s,4r,5s)-5-(5,6-dimethylbenzimidazol-1-yl)-4-hydroxy-2-(hydroxymethyl)oxolan-3-yl] [(2r)-1-[3-[(1r,2r,3r,4z,7s,9z,12s,13s,14z,17s,18s,19r)-2,13,18-tris(2-amino-2-oxoethyl)-7,12,17-tris(3-amino-3-oxopropyl)-3,5,8,8,13,15,18,19-octamethyl-2 Chemical compound [Co+3].N#[C-].N([C@@H]([C@]1(C)[N-]\C([C@H]([C@@]1(CC(N)=O)C)CCC(N)=O)=C(\C)/C1=N/C([C@H]([C@@]1(CC(N)=O)C)CCC(N)=O)=C\C1=N\C([C@H](C1(C)C)CCC(N)=O)=C/1C)[C@@H]2CC(N)=O)=C\1[C@]2(C)CCC(=O)NC[C@@H](C)OP([O-])(=O)O[C@H]1[C@@H](O)[C@@H](N2C3=CC(C)=C(C)C=C3N=C2)O[C@@H]1CO FDJOLVPMNUYSCM-WZHZPDAFSA-L 0.000 title 1
- 238000005286 illumination Methods 0.000 title 1
- 230000001590 oxidative effect Effects 0.000 title 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- LVFFZQQWIZURIO-UHFFFAOYSA-N 2-phenylbutanedioic acid Chemical compound OC(=O)CC(C(O)=O)C1=CC=CC=C1 LVFFZQQWIZURIO-UHFFFAOYSA-N 0.000 abstract 2
- YOZNUFWCRFCGIH-BYFNXCQMSA-L hydroxocobalamin Chemical compound O[Co+]N([C@]1([H])[C@H](CC(N)=O)[C@]\2(CCC(=O)NC[C@H](C)OP(O)(=O)OC3[C@H]([C@H](O[C@@H]3CO)N3C4=CC(C)=C(C)C=C4N=C3)O)C)C/2=C(C)\C([C@H](C/2(C)C)CCC(N)=O)=N\C\2=C\C([C@H]([C@@]/2(CC(N)=O)C)CCC(N)=O)=N\C\2=C(C)/C2=N[C@]1(C)[C@@](C)(CC(N)=O)[C@@H]2CCC(N)=O YOZNUFWCRFCGIH-BYFNXCQMSA-L 0.000 abstract 2
- 150000003839 salts Chemical class 0.000 abstract 2
- 239000003513 alkali Substances 0.000 abstract 1
- 239000012458 free base Substances 0.000 abstract 1
- 235000004867 hydroxocobalamin Nutrition 0.000 abstract 1
- 239000011704 hydroxocobalamin Substances 0.000 abstract 1
- 229960001103 hydroxocobalamin Drugs 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H23/00—Compounds containing boron, silicon or a metal, e.g. chelates or vitamin B12
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| MC751144A MC1058A1 (fr) | 1975-04-29 | 1975-04-29 | Procede de preparation d'hydroxocobalamine et de ses sels |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR2309564A1 true FR2309564A1 (fr) | 1976-11-26 |
| FR2309564B1 FR2309564B1 (enExample) | 1977-12-09 |
Family
ID=19737902
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR7514219A Granted FR2309564A1 (fr) | 1975-04-29 | 1975-05-06 | Procede de preparation d'hydroxocobalamine et de ses sels |
Country Status (2)
| Country | Link |
|---|---|
| FR (1) | FR2309564A1 (enExample) |
| MC (1) | MC1058A1 (enExample) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0533115A1 (en) * | 1991-09-17 | 1993-03-24 | Nippon Oil Co. Ltd. | Process for production of hydroxocobalamin |
| CN102351933A (zh) * | 2011-07-25 | 2012-02-15 | 河北玉星生物工程有限公司 | 一种制备羟钴胺盐的方法 |
| CN102516340A (zh) * | 2011-11-14 | 2012-06-27 | 天津理工大学 | 一种采用d150大孔树脂分离纯化羟钴胺素的方法 |
| WO2014142640A1 (es) * | 2013-03-13 | 2014-09-18 | Interquim, S.A. De C.V. | Mejoras al proceso de preparación de hidroxocobalamina y sus sales de alta pueza |
-
1975
- 1975-04-29 MC MC751144A patent/MC1058A1/fr unknown
- 1975-05-06 FR FR7514219A patent/FR2309564A1/fr active Granted
Non-Patent Citations (1)
| Title |
|---|
| NEANT * |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0533115A1 (en) * | 1991-09-17 | 1993-03-24 | Nippon Oil Co. Ltd. | Process for production of hydroxocobalamin |
| US5338418A (en) * | 1991-09-17 | 1994-08-16 | Nippon Oil Co., Ltd. | Process for production of hydroxocobalamin |
| CN102351933A (zh) * | 2011-07-25 | 2012-02-15 | 河北玉星生物工程有限公司 | 一种制备羟钴胺盐的方法 |
| CN102351933B (zh) * | 2011-07-25 | 2014-04-02 | 河北玉星生物工程有限公司 | 一种制备羟钴胺盐的方法 |
| CN102516340A (zh) * | 2011-11-14 | 2012-06-27 | 天津理工大学 | 一种采用d150大孔树脂分离纯化羟钴胺素的方法 |
| WO2014142640A1 (es) * | 2013-03-13 | 2014-09-18 | Interquim, S.A. De C.V. | Mejoras al proceso de preparación de hidroxocobalamina y sus sales de alta pueza |
Also Published As
| Publication number | Publication date |
|---|---|
| MC1058A1 (fr) | 1976-02-20 |
| FR2309564B1 (enExample) | 1977-12-09 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ST | Notification of lapse |