FR2202097A2 - Arylphosphonyl dichloride - by oxidation of aryl dichlorophosphine with nitrogen peroxide - Google Patents
Arylphosphonyl dichloride - by oxidation of aryl dichlorophosphine with nitrogen peroxideInfo
- Publication number
- FR2202097A2 FR2202097A2 FR7225406A FR7225406A FR2202097A2 FR 2202097 A2 FR2202097 A2 FR 2202097A2 FR 7225406 A FR7225406 A FR 7225406A FR 7225406 A FR7225406 A FR 7225406A FR 2202097 A2 FR2202097 A2 FR 2202097A2
- Authority
- FR
- France
- Prior art keywords
- dichlorophosphine
- dichloride
- arylphosphonyl
- oxidation
- aryl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- -1 aryl dichlorophosphine Chemical compound 0.000 title abstract 3
- OMBRFUXPXNIUCZ-UHFFFAOYSA-N dioxidonitrogen(1+) Chemical compound O=[N+]=O OMBRFUXPXNIUCZ-UHFFFAOYSA-N 0.000 title 1
- 230000003647 oxidation Effects 0.000 title 1
- 238000007254 oxidation reaction Methods 0.000 title 1
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 abstract 3
- 125000003118 aryl group Chemical group 0.000 abstract 1
- IMDXZWRLUZPMDH-UHFFFAOYSA-N dichlorophenylphosphine Chemical compound ClP(Cl)C1=CC=CC=C1 IMDXZWRLUZPMDH-UHFFFAOYSA-N 0.000 abstract 1
- IBDMRHDXAQZJAP-UHFFFAOYSA-N dichlorophosphorylbenzene Chemical compound ClP(Cl)(=O)C1=CC=CC=C1 IBDMRHDXAQZJAP-UHFFFAOYSA-N 0.000 abstract 1
- 239000012442 inert solvent Substances 0.000 abstract 1
- 230000002028 premature Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic System
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids RP(=O)(OH)2; Thiophosphonic acids, i.e. RP(=X)(XH)2 (X = S, Se)
- C07F9/42—Halides thereof
Abstract
Title cpd. is of formula ArPOCl2 (where Ar is (un)substd Aryl). Phenyl phosphonic acid dichloride is prepd. by oxidn. of phenyl dichlorophosphine and tolyl phosphonic acid dichloride from tolyl dichlorophosphine in inert solvent with b.pt. lower than prod. decompsn. temp. (methylene chloride). Reaction is rapid and proceeds at low temp. avoiding premature decompsn.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7225406A FR2202097A2 (en) | 1972-07-13 | 1972-07-13 | Arylphosphonyl dichloride - by oxidation of aryl dichlorophosphine with nitrogen peroxide |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7225406A FR2202097A2 (en) | 1972-07-13 | 1972-07-13 | Arylphosphonyl dichloride - by oxidation of aryl dichlorophosphine with nitrogen peroxide |
Publications (2)
Publication Number | Publication Date |
---|---|
FR2202097A2 true FR2202097A2 (en) | 1974-05-03 |
FR2202097B2 FR2202097B2 (en) | 1977-04-01 |
Family
ID=9101798
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7225406A Granted FR2202097A2 (en) | 1972-07-13 | 1972-07-13 | Arylphosphonyl dichloride - by oxidation of aryl dichlorophosphine with nitrogen peroxide |
Country Status (1)
Country | Link |
---|---|
FR (1) | FR2202097A2 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0010368A1 (en) * | 1978-09-29 | 1980-04-30 | Stauffer Chemical Company | Process for production of benzene phosphonic dihalide |
-
1972
- 1972-07-13 FR FR7225406A patent/FR2202097A2/en active Granted
Non-Patent Citations (1)
Title |
---|
JOURNAL OF AMERICAN CHEMICAL SOCIETY VOL 80, PAGES 5441 A 5443 1958 ) * |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0010368A1 (en) * | 1978-09-29 | 1980-04-30 | Stauffer Chemical Company | Process for production of benzene phosphonic dihalide |
Also Published As
Publication number | Publication date |
---|---|
FR2202097B2 (en) | 1977-04-01 |
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