FR2049936A5 - Carbon fibre production by polyacrylonit- - rile filament oxidation - Google Patents
Carbon fibre production by polyacrylonit- - rile filament oxidationInfo
- Publication number
- FR2049936A5 FR2049936A5 FR7020592A FR7020592A FR2049936A5 FR 2049936 A5 FR2049936 A5 FR 2049936A5 FR 7020592 A FR7020592 A FR 7020592A FR 7020592 A FR7020592 A FR 7020592A FR 2049936 A5 FR2049936 A5 FR 2049936A5
- Authority
- FR
- France
- Prior art keywords
- oxidation
- degrees
- pref
- polyacrylonit
- rile
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/20—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products
- D01F9/21—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D01F9/22—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/32—Apparatus therefor
Abstract
Carbon (graphtie) fibres of high elasticity, modulus and tenacity, suitable for C fibre strips for fibre/resin articles, are produced by subjecting PAN filaments of 1-5 den. to (a) partial oxidation in oxidising atm. pref. air, at 200-300 degrees C for less than 4 hrs; (b) further oxidation at 300-375 degrees C at rate which is at least 10 times faster than in first oxidation, where this rate is measured through dwelling-period under oxidation conditions, until complete infusibility is attained; and (c) quick pyrolysis/graphitising heat treatment in non-oxidising atm. at 1000-2500 degrees C. Pref. filamentary PAN is stretched at 100 degrees C before oxidation, and pref. the continuous filaments are led over cold guide rolls during oxidation.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US83025469A | 1969-06-04 | 1969-06-04 |
Publications (1)
Publication Number | Publication Date |
---|---|
FR2049936A5 true FR2049936A5 (en) | 1971-03-26 |
Family
ID=25256626
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7020592A Expired FR2049936A5 (en) | 1969-06-04 | 1970-06-04 | Carbon fibre production by polyacrylonit- - rile filament oxidation |
Country Status (2)
Country | Link |
---|---|
DE (1) | DE2026019A1 (en) |
FR (1) | FR2049936A5 (en) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5742925A (en) * | 1980-08-22 | 1982-03-10 | Toho Rayon Co Ltd | Production of high-performance carbon fiber strand |
KR920700318A (en) * | 1989-02-23 | 1992-02-19 | 나가이 야따로 | Flameproofing Device |
EP0626548A1 (en) * | 1993-05-28 | 1994-11-30 | Akzo Nobel N.V. | Process and apparatus for the high speed oxidation of organic fiber |
-
1970
- 1970-05-27 DE DE19702026019 patent/DE2026019A1/en active Pending
- 1970-06-04 FR FR7020592A patent/FR2049936A5/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
DE2026019A1 (en) | 1971-02-25 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ST | Notification of lapse |