FI71503B - Foerfarande foer framstaellning av smao kapslar - Google Patents
Foerfarande foer framstaellning av smao kapslar Download PDFInfo
- Publication number
- FI71503B FI71503B FI831295A FI831295A FI71503B FI 71503 B FI71503 B FI 71503B FI 831295 A FI831295 A FI 831295A FI 831295 A FI831295 A FI 831295A FI 71503 B FI71503 B FI 71503B
- Authority
- FI
- Finland
- Prior art keywords
- poly
- capsule
- salt
- maleic anhydride
- process according
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M5/00—Duplicating or marking methods; Sheet materials for use therein
- B41M5/124—Duplicating or marking methods; Sheet materials for use therein using pressure to make a masked colour visible, e.g. to make a coloured support visible, to create an opaque or transparent pattern, or to form colour by uniting colour-forming components
- B41M5/165—Duplicating or marking methods; Sheet materials for use therein using pressure to make a masked colour visible, e.g. to make a coloured support visible, to create an opaque or transparent pattern, or to form colour by uniting colour-forming components characterised by the use of microcapsules; Special solvents for incorporating the ingredients
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/06—Making microcapsules or microballoons by phase separation
- B01J13/14—Polymerisation; cross-linking
- B01J13/18—In situ polymerisation with all reactants being present in the same phase
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L61/00—Compositions of condensation polymers of aldehydes or ketones; Compositions of derivatives of such polymers
- C08L61/20—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
- C08L61/26—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with heterocyclic compounds
- C08L61/28—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with heterocyclic compounds with melamine
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
- Y10T428/2984—Microcapsule with fluid core [includes liposome]
- Y10T428/2985—Solid-walled microcapsule from synthetic polymer
Claims (10)
1. Förfarande för framställning av smä kapslar omfattan-de ett steg, i vilket man bildar en dispersion av droppar eller partiklar av en väsentligen vattenolöslig kapselkärn-material i ett surt vattenhaltigt framställningsmedium, som innehaller: a) ett kapselvägg-prekursormaterial, valt bland melamin och formaldehydi monomer metylolmelamin eller dess polymer med lag molekylvikt; monomer metylerad metylolmelamin eller dess polymer med lag molekylvikt; eller vilken som heist av deras kombinationer; och b) en negativt laddad polymer polyelektrolyt, som har en rak alifatisk kolvätestamme med i medeltal tva karbo-xylgrupper per varje 4-6 stomkolatomer; varvid det vattenlösliga kapselvägg-prekursormaterialet po-lykondenser under bildning av en kondensationspolymer, vilket resultear i i) en vätske-vätske fasavskiljning av den bildade kondensationspolymer över en molekylvikt, som är löslig i det vattenhaltiga framställningsmediumet, och ii) efter fortsatt polykondensation av den separerande polymerisätionsprodukten, en bildning av ett fast kap-selväggmaterial, som individuellt omsluter partiklar av det dispergerade kapselkärnmaterialet, kännetecknat därav, att den nämnda dispersionen även innehaller ett sait av en katjon fran den periodiska gruppen IA eller en tertiär eller kvaternär ammoniumkatjon och en anjon av en stark syra.
2. Förfarande enligt patentkravet 1, kännetecknat därav, att man bildar först en lösning av den negativt laddade polymera polyelektrolyten i det vattenhaltiga framställningsmediumet, sedan tillsätter kapselvägg-prekursormaterialet, därefter dispergerar kapselkärnmaterialet i det vattenhaltiga framställningsmediumet och sedan tillsätter saltet, varefter polykondensationen av kapselvägg-prekur-
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US37032382 | 1982-04-20 | ||
US06/370,323 US4444699A (en) | 1982-04-20 | 1982-04-20 | Capsule manufacture |
Publications (4)
Publication Number | Publication Date |
---|---|
FI831295A0 FI831295A0 (fi) | 1983-04-18 |
FI831295L FI831295L (fi) | 1983-10-21 |
FI71503B true FI71503B (fi) | 1986-10-10 |
FI71503C FI71503C (sv) | 1987-01-19 |
Family
ID=23459167
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FI831295A FI71503C (sv) | 1982-04-20 | 1983-04-18 | Förfarande för framställning av små kapslar. |
Country Status (15)
Country | Link |
---|---|
US (1) | US4444699A (sv) |
EP (1) | EP0092356B1 (sv) |
JP (1) | JPH0824841B2 (sv) |
AT (1) | ATE18512T1 (sv) |
AU (1) | AU554433B2 (sv) |
BR (1) | BR8301972A (sv) |
CA (1) | CA1188164A (sv) |
DE (1) | DE3362497D1 (sv) |
DK (1) | DK170683A (sv) |
ES (1) | ES8404199A1 (sv) |
FI (1) | FI71503C (sv) |
GR (1) | GR77458B (sv) |
NO (1) | NO831381L (sv) |
PT (1) | PT76550A (sv) |
ZA (1) | ZA832519B (sv) |
Families Citing this family (51)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4690825A (en) * | 1985-10-04 | 1987-09-01 | Advanced Polymer Systems, Inc. | Method for delivering an active ingredient by controlled time release utilizing a novel delivery vehicle which can be prepared by a process utilizing the active ingredient as a porogen |
JPS6397223A (ja) * | 1986-10-14 | 1988-04-27 | Toppan Moore Co Ltd | マイクロカプセルの製造方法 |
US4857406A (en) * | 1987-04-10 | 1989-08-15 | The Mead Corporation | Microcapsules with polysalt capsule walls and their formation |
US4978483A (en) * | 1987-09-28 | 1990-12-18 | Redding Bruce K | Apparatus and method for making microcapsules |
US5055300A (en) * | 1988-06-17 | 1991-10-08 | Basic Bio Systems, Inc. | Time release protein |
US5079005A (en) * | 1988-06-17 | 1992-01-07 | Gupta Kashmiri L | Time release protein |
US5023080A (en) * | 1988-06-17 | 1991-06-11 | Basic Bio Systems, Inc. | Time release protein |
US5154927A (en) * | 1989-01-19 | 1992-10-13 | Wm. Wrigley Jr. Company | Gum composition containing dispersed porous beads containing active chewing gum ingredients and method |
US4963369A (en) * | 1989-01-19 | 1990-10-16 | Wm. Wrigley Jr. Co. | Gum composition containing dispersed porous beads containing active chewing gum ingredients and method |
US5139787A (en) * | 1989-01-19 | 1992-08-18 | Wm. Wrigley Jr. Company | Gum composition containing dispersed porous beads containing active chewing gum ingredients and method |
US5064698A (en) * | 1989-02-16 | 1991-11-12 | Wm. Wrigley, Jr. Company | Food packaging improvements |
US5126174A (en) * | 1989-02-16 | 1992-06-30 | Wm. Wrigley Jr. Company | Food packaging improvements |
JP2502146B2 (ja) * | 1989-04-12 | 1996-05-29 | 日本製紙株式会社 | 微小カプセルの製造方法 |
US4977060A (en) * | 1989-12-07 | 1990-12-11 | The Mead Corporation | Method for producing microcapsules and photosensitive microcapsules produced thereby |
US5154938A (en) * | 1990-12-20 | 1992-10-13 | Wm. Wrigley Jr. Company | Gum composition having dispersed porous beads containing plasticizers |
US5733561A (en) * | 1991-06-12 | 1998-03-31 | Mitsui Toatsu Chemicals, Incorporated | Insecticide composition and production process thereof |
JPH06269657A (ja) * | 1993-03-17 | 1994-09-27 | Sakura Color Prod Corp | マイクロカプセルの製造方法 |
FR2723032B1 (fr) | 1994-07-26 | 1996-11-22 | Copigraph Sa | Nouveau solvant organique pour microcapsules utiles notamment pour la realisation de papier autocopiant sensible a la pression et papier sensible a lapression revetu de telles microcapsules |
US5843409A (en) * | 1994-08-08 | 1998-12-01 | Colgate Palmolive Company | Two component dentifrice for the treatment of dentinal hypersensitivity |
FR2727633A1 (fr) | 1994-12-02 | 1996-06-07 | Copigraph | Microcapsules contenant a titre de solvant un derive terpenique ou d'acide abietique et papiers sensibles a la pression revetus de ces microcapsules |
AU8852601A (en) * | 2000-09-06 | 2002-03-22 | Appleton Paper Inc | In situ microencapsulated adhesive |
US7108190B2 (en) * | 2003-02-28 | 2006-09-19 | Appleton Papers Inc. | Token array and method employing authentication tokens bearing scent formulation information |
US20060063125A1 (en) * | 2003-04-22 | 2006-03-23 | Hamilton Timothy F | Method and device for enhanced dental articulation |
US6932602B2 (en) * | 2003-04-22 | 2005-08-23 | Appleton Papers Inc. | Dental articulation kit and method |
US20040251309A1 (en) * | 2003-06-10 | 2004-12-16 | Appleton Papers Inc. | Token bearing magnetc image information in registration with visible image information |
US8267576B2 (en) | 2004-11-08 | 2012-09-18 | Freshpoint Holdings Sa | Time-temperature indicating device |
EP1861246B1 (en) | 2005-03-25 | 2017-03-29 | Encapsys, Llc | Adhesively securable stock packaging materials |
DE102006016907A1 (de) * | 2006-04-11 | 2007-10-25 | Cognis Ip Management Gmbh | Zur Insektenabwehr ausgerüstete Fasern und textile Flächengebilde |
US7935201B2 (en) * | 2006-11-29 | 2011-05-03 | Wausau Paper Mills, Llc | Non-slip masking product, and methods |
US20090274906A1 (en) * | 2008-05-01 | 2009-11-05 | Appleton Papers Inc. | Particle with low permeance wall |
US8067089B2 (en) * | 2008-05-01 | 2011-11-29 | Appleton Papers Inc. | Cationic microcapsule particles |
US8071214B2 (en) * | 2008-05-01 | 2011-12-06 | Appleton Papers Inc. | Particle with selected permeance wall |
EP2288879B1 (en) | 2008-06-04 | 2018-01-24 | G Patel | A monitoring system based on etching of metals |
EP3293493B1 (en) | 2008-06-04 | 2023-06-14 | Jp Laboratories, Inc. | Sterilization indicating device |
US7915215B2 (en) * | 2008-10-17 | 2011-03-29 | Appleton Papers Inc. | Fragrance-delivery composition comprising boron and persulfate ion-crosslinked polyvinyl alcohol microcapsules and method of use thereof |
US8455098B2 (en) * | 2009-04-07 | 2013-06-04 | Appleton Papers Inc. | Encapsulated solid hydrophilic particles |
WO2011084141A2 (en) * | 2009-12-21 | 2011-07-14 | Appleton Papers Inc. | Hydrophilic liquid encapsulates |
US9186642B2 (en) | 2010-04-28 | 2015-11-17 | The Procter & Gamble Company | Delivery particle |
US9993793B2 (en) | 2010-04-28 | 2018-06-12 | The Procter & Gamble Company | Delivery particles |
US20110269657A1 (en) | 2010-04-28 | 2011-11-03 | Jiten Odhavji Dihora | Delivery particles |
JP5869663B2 (ja) | 2011-04-07 | 2016-02-24 | ザ プロクター アンド ギャンブルカンパニー | ポリアクリレートマイクロカプセルの付着が増大したシャンプー組成物 |
WO2012138710A2 (en) | 2011-04-07 | 2012-10-11 | The Procter & Gamble Company | Personal cleansing compositions with increased deposition of polyacrylate microcapsules |
CN103458871B (zh) | 2011-04-07 | 2015-05-13 | 宝洁公司 | 具有增强的聚丙烯酸酯微胶囊的沉积的调理剂组合物 |
WO2013101889A1 (en) | 2011-12-29 | 2013-07-04 | Rohm And Haas Company | Encapsulated actives |
US10077606B2 (en) | 2013-03-27 | 2018-09-18 | Halliburton Energy Services, Inc. | Methods of mitigating bituminous material adhesion using nano-particles |
US10077636B2 (en) | 2013-03-27 | 2018-09-18 | Halliburton Energy Services, Inc. | Use of nanoparticles in cleaning well bores |
US9750243B2 (en) * | 2015-02-06 | 2017-09-05 | Lamberti Spa | Aqueous adjuvant concentrates with improved spray drift properties |
US9420781B1 (en) * | 2015-02-06 | 2016-08-23 | Lamberti Spa | Agrochemical adjuvant concentrate for herbicides |
EP3390483B1 (en) | 2015-10-27 | 2022-05-18 | The Procter & Gamble Company | Encapsulation |
CN110168042B (zh) | 2017-01-27 | 2022-05-27 | 恩盖普有限公司 | 包封物 |
EP3908246A4 (en) | 2019-01-11 | 2022-11-16 | Encapsys, LLC | INSTALLATION OF CHITOSAN IN A MICROCAPSULE WALL |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2312693A (en) * | 1941-11-01 | 1943-03-02 | Gen Electric | Reaction product of aldehydes and diazine derivatives |
US2653921A (en) * | 1949-07-25 | 1953-09-29 | Ciba Ltd | Catalysts for the hardening of artificial resins and their use in the textile industry |
CH540715A (de) * | 1970-05-26 | 1973-10-15 | Ciba Geigy Ag | Verfahren zur Einkapselung von in einer Flüssigkeit fein verteilter Substanz |
US3928272A (en) * | 1974-03-25 | 1975-12-23 | Nl Industries Inc | Process of making urea-formaldehyde solid microspheres |
BE829482R (fr) * | 1975-05-26 | 1975-09-15 | Procede pour produire des microcapsules et microcapsules ainsi obtenues | |
GB1507739A (en) * | 1975-11-26 | 1978-04-19 | Wiggins Teape Ltd | Capsules |
US4100103A (en) * | 1976-12-30 | 1978-07-11 | Ncr Corporation | Capsule manufacture |
JPS5425277A (en) * | 1977-07-27 | 1979-02-26 | Fuji Photo Film Co Ltd | Method of producing microcapsule |
JPS602100B2 (ja) * | 1977-09-28 | 1985-01-19 | 三菱製紙株式会社 | 微小カプセルの製造方法 |
JPS5592135A (en) * | 1978-12-29 | 1980-07-12 | Kanzaki Paper Mfg Co Ltd | Production of microcapsule |
JPS5951333B2 (ja) * | 1979-10-31 | 1984-12-13 | 神崎製紙株式会社 | マイクロカプセルの製造方法 |
GB2073132B (en) * | 1980-04-08 | 1983-12-14 | Wiggins Teape Group Ltd | Production of microcapsules |
NO153286C (no) * | 1980-08-20 | 1986-02-19 | Kureha Chemical Ind Co Ltd | Farvestoffholdig mikrokapsel for trykkfoelsomt registreringspapir, samt fremgangsmaate for fremstilling av en slik mikrokapsel. |
JPS57103891A (en) * | 1980-12-19 | 1982-06-28 | Fuji Photo Film Co Ltd | Microcapsule dispersing liquid |
-
1982
- 1982-04-20 US US06/370,323 patent/US4444699A/en not_active Expired - Lifetime
-
1983
- 1983-03-18 CA CA000424001A patent/CA1188164A/en not_active Expired
- 1983-04-11 DE DE8383302008T patent/DE3362497D1/de not_active Expired
- 1983-04-11 AT AT83302008T patent/ATE18512T1/de not_active IP Right Cessation
- 1983-04-11 ZA ZA832519A patent/ZA832519B/xx unknown
- 1983-04-11 EP EP83302008A patent/EP0092356B1/en not_active Expired
- 1983-04-13 AU AU13490/83A patent/AU554433B2/en not_active Ceased
- 1983-04-14 PT PT76550A patent/PT76550A/pt unknown
- 1983-04-18 BR BR8301972A patent/BR8301972A/pt unknown
- 1983-04-18 FI FI831295A patent/FI71503C/sv not_active IP Right Cessation
- 1983-04-18 GR GR71116A patent/GR77458B/el unknown
- 1983-04-19 DK DK170683A patent/DK170683A/da not_active IP Right Cessation
- 1983-04-19 ES ES521609A patent/ES8404199A1/es not_active Expired
- 1983-04-19 NO NO831381A patent/NO831381L/no unknown
- 1983-04-20 JP JP58069863A patent/JPH0824841B2/ja not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
FI831295L (fi) | 1983-10-21 |
CA1188164A (en) | 1985-06-04 |
ZA832519B (en) | 1984-02-29 |
DK170683D0 (da) | 1983-04-19 |
BR8301972A (pt) | 1983-12-20 |
JPH0824841B2 (ja) | 1996-03-13 |
JPS58216737A (ja) | 1983-12-16 |
DE3362497D1 (en) | 1986-04-17 |
NO831381L (no) | 1983-10-21 |
DK170683A (da) | 1983-10-21 |
FI831295A0 (fi) | 1983-04-18 |
AU1349083A (en) | 1983-10-27 |
ES521609A0 (es) | 1984-04-16 |
PT76550A (en) | 1983-05-01 |
EP0092356B1 (en) | 1986-03-12 |
EP0092356A2 (en) | 1983-10-26 |
EP0092356A3 (en) | 1983-12-07 |
US4444699A (en) | 1984-04-24 |
ATE18512T1 (de) | 1986-03-15 |
AU554433B2 (en) | 1986-08-21 |
GR77458B (sv) | 1984-09-24 |
ES8404199A1 (es) | 1984-04-16 |
FI71503C (sv) | 1987-01-19 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
MA | Patent expired |
Owner name: APPLETON PAPERS INC. |