FI58111C - Foerfarande foer rening av titantetraklorid - Google Patents
Foerfarande foer rening av titantetraklorid Download PDFInfo
- Publication number
- FI58111C FI58111C FI1543/74A FI154374A FI58111C FI 58111 C FI58111 C FI 58111C FI 1543/74 A FI1543/74 A FI 1543/74A FI 154374 A FI154374 A FI 154374A FI 58111 C FI58111 C FI 58111C
- Authority
- FI
- Finland
- Prior art keywords
- ticl
- vanadium
- titanium tetrachloride
- amine
- process according
- Prior art date
Links
- 229910052720 vanadium Inorganic materials 0.000 claims description 33
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims description 33
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 claims description 23
- 150000001412 amines Chemical class 0.000 claims description 22
- DMBHHRLKUKUOEG-UHFFFAOYSA-N diphenylamine Chemical compound C=1C=CC=CC=1NC1=CC=CC=C1 DMBHHRLKUKUOEG-UHFFFAOYSA-N 0.000 claims description 22
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 claims description 18
- 238000004821 distillation Methods 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 18
- 230000008569 process Effects 0.000 claims description 12
- 125000004432 carbon atom Chemical group C* 0.000 claims description 10
- UFFBMTHBGFGIHF-UHFFFAOYSA-N 2,6-dimethylaniline Chemical compound CC1=CC=CC(C)=C1N UFFBMTHBGFGIHF-UHFFFAOYSA-N 0.000 claims description 8
- NQRYJNQNLNOLGT-UHFFFAOYSA-N Piperidine Chemical compound C1CCNCC1 NQRYJNQNLNOLGT-UHFFFAOYSA-N 0.000 claims description 8
- 239000012535 impurity Substances 0.000 claims description 8
- 125000003118 aryl group Chemical group 0.000 claims description 6
- 125000000217 alkyl group Chemical group 0.000 claims description 5
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 claims description 5
- RWRDLPDLKQPQOW-UHFFFAOYSA-N tetrahydropyrrole Natural products C1CCNC1 RWRDLPDLKQPQOW-UHFFFAOYSA-N 0.000 claims description 5
- 125000000753 cycloalkyl group Chemical group 0.000 claims description 4
- PAFZNILMFXTMIY-UHFFFAOYSA-N cyclohexylamine Chemical group NC1CCCCC1 PAFZNILMFXTMIY-UHFFFAOYSA-N 0.000 claims description 4
- 239000001257 hydrogen Substances 0.000 claims description 4
- 229910052739 hydrogen Inorganic materials 0.000 claims description 4
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 4
- 125000004836 hexamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 claims description 3
- VVAKEQGKZNKUSU-UHFFFAOYSA-N 2,3-dimethylaniline Chemical compound CC1=CC=CC(N)=C1C VVAKEQGKZNKUSU-UHFFFAOYSA-N 0.000 claims description 2
- 125000003342 alkenyl group Chemical group 0.000 claims description 2
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims 2
- 125000004817 pentamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 claims 2
- 125000000719 pyrrolidinyl group Chemical group 0.000 claims 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 7
- 238000009835 boiling Methods 0.000 description 7
- 239000007787 solid Substances 0.000 description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- 239000003638 chemical reducing agent Substances 0.000 description 6
- 239000013078 crystal Substances 0.000 description 6
- 238000010438 heat treatment Methods 0.000 description 6
- 238000000746 purification Methods 0.000 description 6
- 150000001805 chlorine compounds Chemical class 0.000 description 5
- 150000001875 compounds Chemical class 0.000 description 5
- JLTDJTHDQAWBAV-UHFFFAOYSA-N N,N-dimethylaniline Chemical compound CN(C)C1=CC=CC=C1 JLTDJTHDQAWBAV-UHFFFAOYSA-N 0.000 description 4
- 230000009467 reduction Effects 0.000 description 4
- 238000010992 reflux Methods 0.000 description 4
- 150000003682 vanadium compounds Chemical class 0.000 description 4
- 229910010413 TiO 2 Inorganic materials 0.000 description 3
- 229910021550 Vanadium Chloride Inorganic materials 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000005660 chlorination reaction Methods 0.000 description 3
- 238000002845 discoloration Methods 0.000 description 3
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 3
- 229910052742 iron Inorganic materials 0.000 description 3
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- RPESBQCJGHJMTK-UHFFFAOYSA-I pentachlorovanadium Chemical compound [Cl-].[Cl-].[Cl-].[Cl-].[Cl-].[V+5] RPESBQCJGHJMTK-UHFFFAOYSA-I 0.000 description 3
- 239000000049 pigment Substances 0.000 description 3
- VOWZNBNDMFLQGM-UHFFFAOYSA-N 2,5-dimethylaniline Chemical compound CC1=CC=C(C)C(N)=C1 VOWZNBNDMFLQGM-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- ZHXZNKNQUHUIGN-UHFFFAOYSA-N chloro hypochlorite;vanadium Chemical compound [V].ClOCl ZHXZNKNQUHUIGN-UHFFFAOYSA-N 0.000 description 2
- 239000003925 fat Substances 0.000 description 2
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229920002120 photoresistant polymer Polymers 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 239000010936 titanium Substances 0.000 description 2
- 229910052719 titanium Inorganic materials 0.000 description 2
- 239000004408 titanium dioxide Substances 0.000 description 2
- OHVLMTFVQDZYHP-UHFFFAOYSA-N 1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)-2-[4-[2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidin-5-yl]piperazin-1-yl]ethanone Chemical compound N1N=NC=2CN(CCC=21)C(CN1CCN(CC1)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)=O OHVLMTFVQDZYHP-UHFFFAOYSA-N 0.000 description 1
- JQMFQLVAJGZSQS-UHFFFAOYSA-N 2-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperazin-1-yl]-N-(2-oxo-3H-1,3-benzoxazol-6-yl)acetamide Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)N1CCN(CC1)CC(=O)NC1=CC2=C(NC(O2)=O)C=C1 JQMFQLVAJGZSQS-UHFFFAOYSA-N 0.000 description 1
- 125000003341 7 membered heterocyclic group Chemical group 0.000 description 1
- 208000030507 AIDS Diseases 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- DIWPUORWECXYLU-UHFFFAOYSA-N ClN.ClN.OS(=O)(=O)C1=CC=CC=C1 Chemical compound ClN.ClN.OS(=O)(=O)C1=CC=CC=C1 DIWPUORWECXYLU-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 206010067482 No adverse event Diseases 0.000 description 1
- -1 SiCl 2 Inorganic materials 0.000 description 1
- 229910007926 ZrCl Inorganic materials 0.000 description 1
- CIUQDSCDWFSTQR-UHFFFAOYSA-N [C]1=CC=CC=C1 Chemical compound [C]1=CC=CC=C1 CIUQDSCDWFSTQR-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical class Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000010775 animal oil Substances 0.000 description 1
- 150000005840 aryl radicals Chemical class 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- LHOOSULWOYHVSL-UHFFFAOYSA-N cyclohexanamine;n-methylmethanamine Chemical compound CNC.NC1CCCCC1 LHOOSULWOYHVSL-UHFFFAOYSA-N 0.000 description 1
- 238000006298 dechlorination reaction Methods 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- RCJVRSBWZCNNQT-UHFFFAOYSA-N dichloridooxygen Chemical compound ClOCl RCJVRSBWZCNNQT-UHFFFAOYSA-N 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 125000002768 hydroxyalkyl group Chemical group 0.000 description 1
- 125000004029 hydroxymethyl group Chemical group [H]OC([H])([H])* 0.000 description 1
- YDZQQRWRVYGNER-UHFFFAOYSA-N iron;titanium;trihydrate Chemical compound O.O.O.[Ti].[Fe] YDZQQRWRVYGNER-UHFFFAOYSA-N 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 125000004433 nitrogen atom Chemical group N* 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000000546 pharmaceutical excipient Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 125000004368 propenyl group Chemical group C(=CC)* 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 125000001424 substituent group Chemical group 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/02—Halides of titanium
- C01G23/022—Titanium tetrachloride
- C01G23/024—Purification of tetrachloride
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pyrrole Compounds (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2325924 | 1973-05-22 | ||
| DE19732325924 DE2325924C3 (de) | 1973-05-22 | Verfahren zur Reinigung von Titantetrachlorid |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| FI154374A FI154374A (it) | 1974-11-23 |
| FI58111B FI58111B (fi) | 1980-08-29 |
| FI58111C true FI58111C (fi) | 1980-12-10 |
Family
ID=5881734
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FI1543/74A FI58111C (fi) | 1973-05-22 | 1974-05-20 | Foerfarande foer rening av titantetraklorid |
Country Status (18)
| Country | Link |
|---|---|
| US (1) | US3963585A (it) |
| JP (1) | JPS5128595B2 (it) |
| BE (1) | BE815265A (it) |
| BR (1) | BR7404135D0 (it) |
| CA (1) | CA1030478A (it) |
| CS (1) | CS182255B2 (it) |
| DD (1) | DD115095A5 (it) |
| ES (1) | ES426523A1 (it) |
| FI (1) | FI58111C (it) |
| FR (1) | FR2230589B1 (it) |
| GB (1) | GB1423116A (it) |
| IE (1) | IE39274B1 (it) |
| IN (1) | IN143312B (it) |
| IT (1) | IT1011465B (it) |
| NL (1) | NL7406936A (it) |
| NO (1) | NO137750C (it) |
| PL (1) | PL88794B1 (it) |
| SU (1) | SU645546A3 (it) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5590260A (en) * | 1978-12-21 | 1980-07-08 | Shigetaka Aoyanagi | Method of polishing profile |
| JPS6144777Y2 (it) * | 1980-03-22 | 1986-12-16 | ||
| US4587116A (en) * | 1984-02-06 | 1986-05-06 | The Dow Chemical Company | Process for treating chlorinated nitrogen-containing hydrocarbons |
| DE3623322A1 (de) * | 1986-07-11 | 1988-01-21 | Bayer Ag | Verfahren zur herstellung von ticl(pfeil abwaerts)4(pfeil abwaerts) |
| US5242549A (en) * | 1991-12-06 | 1993-09-07 | Shell Oil Company | Distillation separation process of titanium tetrachloride and halohydrocarbon |
| US5948212A (en) * | 1996-10-21 | 1999-09-07 | Union Carbide Chemicals & Plastics Technology Corporation | Titanium separation process |
| AT405738B (de) * | 1997-09-03 | 1999-11-25 | Chemie Linz Gmbh | Verfahren zur reinigung von phosphoroxychlorid |
| US20020179427A1 (en) * | 2001-05-21 | 2002-12-05 | Goddard John Burnham | Process for purifying titanium tetrachloride |
| WO2004063096A1 (en) * | 2003-01-09 | 2004-07-29 | E.I. Du Pont De Nemours And Company | Purification of titanium tetrachloride |
| CN101844802B (zh) * | 2010-05-04 | 2012-06-27 | 山东鲁北企业集团总公司 | 在精制四氯化钛过程中快速加热蒸馏装置 |
| CN109364765A (zh) * | 2018-11-12 | 2019-02-22 | 江苏奥净嘉环保科技有限公司 | 一种静电纺丝制备光催化过滤膜的方法 |
| CN115924965A (zh) * | 2022-12-26 | 2023-04-07 | 朝阳百盛钛业股份有限公司 | 一种新型四氯化钛除钒工艺 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH262267A (de) * | 1947-07-26 | 1949-06-30 | Schweizerhall Saeurefab | Verfahren zur Reinigung von flüssigen Metallchloriden. |
-
1974
- 1974-04-25 IN IN939/CAL/1974A patent/IN143312B/en unknown
- 1974-05-01 US US05/465,954 patent/US3963585A/en not_active Expired - Lifetime
- 1974-05-15 CS CS7400003480A patent/CS182255B2/cs unknown
- 1974-05-17 JP JP49054597A patent/JPS5128595B2/ja not_active Expired
- 1974-05-17 CA CA200,254A patent/CA1030478A/en not_active Expired
- 1974-05-20 BE BE144511A patent/BE815265A/xx unknown
- 1974-05-20 IT IT51103/74A patent/IT1011465B/it active
- 1974-05-20 FI FI1543/74A patent/FI58111C/fi active
- 1974-05-20 PL PL1974171271A patent/PL88794B1/pl unknown
- 1974-05-20 DD DD178626A patent/DD115095A5/xx unknown
- 1974-05-21 ES ES426523A patent/ES426523A1/es not_active Expired
- 1974-05-21 GB GB2260374A patent/GB1423116A/en not_active Expired
- 1974-05-21 NO NO741845A patent/NO137750C/no unknown
- 1974-05-21 IE IE1076/74A patent/IE39274B1/xx unknown
- 1974-05-21 BR BR4135/74A patent/BR7404135D0/pt unknown
- 1974-05-22 SU SU742025793A patent/SU645546A3/ru active
- 1974-05-22 FR FR7417885A patent/FR2230589B1/fr not_active Expired
- 1974-05-22 NL NL7406936A patent/NL7406936A/xx not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| BR7404135D0 (pt) | 1975-09-30 |
| JPS5019695A (it) | 1975-03-01 |
| FI58111B (fi) | 1980-08-29 |
| US3963585A (en) | 1976-06-15 |
| IE39274L (en) | 1974-11-22 |
| SU645546A3 (ru) | 1979-01-30 |
| IT1011465B (it) | 1977-01-20 |
| NO137750C (no) | 1978-04-19 |
| CS182255B2 (en) | 1978-04-28 |
| IE39274B1 (en) | 1978-09-13 |
| CA1030478A (en) | 1978-05-02 |
| IN143312B (it) | 1977-10-29 |
| PL88794B1 (it) | 1976-09-30 |
| FI154374A (it) | 1974-11-23 |
| NO741845L (no) | 1974-11-25 |
| FR2230589A1 (it) | 1974-12-20 |
| NL7406936A (it) | 1974-11-26 |
| DD115095A5 (it) | 1975-09-12 |
| FR2230589B1 (it) | 1977-10-14 |
| DE2325924B2 (de) | 1976-06-24 |
| AU6914774A (en) | 1975-11-20 |
| NO137750B (no) | 1978-01-09 |
| DE2325924A1 (de) | 1974-12-12 |
| GB1423116A (en) | 1976-01-28 |
| ES426523A1 (es) | 1976-07-01 |
| JPS5128595B2 (it) | 1976-08-20 |
| BE815265A (fr) | 1974-11-20 |
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