FI57689C - Foerfarande foer framstaellning av roekningsmedel - Google Patents
Foerfarande foer framstaellning av roekningsmedel Download PDFInfo
- Publication number
- FI57689C FI57689C FI750433A FI750433A FI57689C FI 57689 C FI57689 C FI 57689C FI 750433 A FI750433 A FI 750433A FI 750433 A FI750433 A FI 750433A FI 57689 C FI57689 C FI 57689C
- Authority
- FI
- Finland
- Prior art keywords
- distillation
- weight
- extraction
- fraction
- acid
- Prior art date
Links
- 238000004821 distillation Methods 0.000 claims description 46
- 239000000779 smoke Substances 0.000 claims description 39
- 238000000034 method Methods 0.000 claims description 29
- 239000000126 substance Substances 0.000 claims description 24
- 238000009835 boiling Methods 0.000 claims description 21
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 18
- 239000003795 chemical substances by application Substances 0.000 claims description 18
- 150000001875 compounds Chemical class 0.000 claims description 18
- 239000002253 acid Substances 0.000 claims description 17
- 238000000605 extraction Methods 0.000 claims description 17
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 16
- 230000008569 process Effects 0.000 claims description 15
- 238000011282 treatment Methods 0.000 claims description 15
- 150000005846 sugar alcohols Polymers 0.000 claims description 13
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 11
- 239000012298 atmosphere Substances 0.000 claims description 10
- 125000001477 organic nitrogen group Chemical group 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 9
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 9
- 235000011007 phosphoric acid Nutrition 0.000 claims description 9
- 239000002994 raw material Substances 0.000 claims description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- 238000001179 sorption measurement Methods 0.000 claims description 8
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 7
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 7
- 239000011707 mineral Substances 0.000 claims description 7
- 239000000243 solution Substances 0.000 claims description 7
- 239000002699 waste material Substances 0.000 claims description 7
- 229910052725 zinc Inorganic materials 0.000 claims description 7
- 239000011701 zinc Substances 0.000 claims description 7
- 229910052782 aluminium Inorganic materials 0.000 claims description 6
- 229930195733 hydrocarbon Natural products 0.000 claims description 6
- 150000002430 hydrocarbons Chemical class 0.000 claims description 6
- 150000002989 phenols Chemical class 0.000 claims description 6
- 229920005610 lignin Polymers 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 5
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 4
- 239000000194 fatty acid Substances 0.000 claims description 4
- 229930195729 fatty acid Natural products 0.000 claims description 4
- 150000004665 fatty acids Chemical class 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 239000003960 organic solvent Substances 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 4
- 235000013312 flour Nutrition 0.000 claims description 3
- 238000005194 fractionation Methods 0.000 claims description 3
- 239000011261 inert gas Substances 0.000 claims description 3
- 229910052742 iron Inorganic materials 0.000 claims description 3
- 150000007524 organic acids Chemical class 0.000 claims description 3
- 235000005985 organic acids Nutrition 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 2
- 239000007789 gas Substances 0.000 claims description 2
- 239000001301 oxygen Substances 0.000 claims description 2
- 229910052760 oxygen Inorganic materials 0.000 claims description 2
- 239000007787 solid Substances 0.000 claims description 2
- 239000001913 cellulose Substances 0.000 claims 2
- 229920002678 cellulose Polymers 0.000 claims 2
- RYXPMWYHEBGTRV-UHFFFAOYSA-N Omeprazole sodium Chemical compound [Na+].N=1C2=CC(OC)=CC=C2[N-]C=1S(=O)CC1=NC=C(C)C(OC)=C1C RYXPMWYHEBGTRV-UHFFFAOYSA-N 0.000 claims 1
- 239000000843 powder Substances 0.000 claims 1
- 238000000638 solvent extraction Methods 0.000 claims 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 27
- 239000000047 product Substances 0.000 description 18
- 235000015097 nutrients Nutrition 0.000 description 14
- 230000000391 smoking effect Effects 0.000 description 12
- 235000019441 ethanol Nutrition 0.000 description 7
- 239000003921 oil Substances 0.000 description 7
- 235000019198 oils Nutrition 0.000 description 7
- 239000002023 wood Substances 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
- 230000000711 cancerogenic effect Effects 0.000 description 6
- 231100000315 carcinogenic Toxicity 0.000 description 6
- 230000003647 oxidation Effects 0.000 description 6
- 238000007254 oxidation reaction Methods 0.000 description 6
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 5
- 239000012141 concentrate Substances 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 4
- 239000000654 additive Substances 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- 230000000844 anti-bacterial effect Effects 0.000 description 3
- 239000001569 carbon dioxide Substances 0.000 description 3
- 229910002092 carbon dioxide Inorganic materials 0.000 description 3
- 239000000428 dust Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 229910052753 mercury Inorganic materials 0.000 description 3
- 235000010755 mineral Nutrition 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 230000002335 preservative effect Effects 0.000 description 3
- 238000000746 purification Methods 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 235000002639 sodium chloride Nutrition 0.000 description 3
- 239000011780 sodium chloride Substances 0.000 description 3
- 239000002594 sorbent Substances 0.000 description 3
- AZQWKYJCGOJGHM-UHFFFAOYSA-N 1,4-benzoquinone Chemical compound O=C1C=CC(=O)C=C1 AZQWKYJCGOJGHM-UHFFFAOYSA-N 0.000 description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- FMMWHPNWAFZXNH-UHFFFAOYSA-N Benz[a]pyrene Chemical compound C1=C2C3=CC=CC=C3C=C(C=C3)C2=C2C3=CC=CC2=C1 FMMWHPNWAFZXNH-UHFFFAOYSA-N 0.000 description 2
- 101000937129 Drosophila melanogaster Cadherin-related tumor suppressor Proteins 0.000 description 2
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000003078 antioxidant effect Effects 0.000 description 2
- 150000001735 carboxylic acids Chemical class 0.000 description 2
- 239000000969 carrier Substances 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 150000001983 dialkylethers Chemical class 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 238000000895 extractive distillation Methods 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000007935 neutral effect Effects 0.000 description 2
- 238000006386 neutralization reaction Methods 0.000 description 2
- 239000012299 nitrogen atmosphere Substances 0.000 description 2
- 150000007530 organic bases Chemical class 0.000 description 2
- 238000000197 pyrolysis Methods 0.000 description 2
- 235000017557 sodium bicarbonate Nutrition 0.000 description 2
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 2
- -1 terpene compounds Chemical class 0.000 description 2
- 235000007586 terpenes Nutrition 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 239000000061 acid fraction Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 239000012223 aqueous fraction Substances 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 235000021245 dietary protein Nutrition 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 230000005686 electrostatic field Effects 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 150000008282 halocarbons Chemical class 0.000 description 1
- 239000011121 hardwood Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 235000021110 pickles Nutrition 0.000 description 1
- 238000012643 polycondensation polymerization Methods 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 235000019871 vegetable fat Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/20—Synthetic spices, flavouring agents or condiments
- A23L27/27—Smoke flavours
Landscapes
- Polymers & Plastics (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Seasonings (AREA)
- Compounds Of Unknown Constitution (AREA)
- Meat, Egg Or Seafood Products (AREA)
- Medicines Containing Plant Substances (AREA)
- General Preparation And Processing Of Foods (AREA)
- Indole Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL1974169004A PL96145B3 (pl) | 1974-02-22 | 1974-02-22 | Sposob wytwarzania srodka aromatyzujacego i/lub antyseptycznego i/lub przeciwdzialajacego utlenianiu |
| PL16900474 | 1974-02-22 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| FI750433A7 FI750433A7 (pl) | 1975-08-23 |
| FI57689B FI57689B (fi) | 1980-06-30 |
| FI57689C true FI57689C (fi) | 1980-10-10 |
Family
ID=19966186
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FI750433A FI57689C (fi) | 1974-02-22 | 1975-02-17 | Foerfarande foer framstaellning av roekningsmedel |
Country Status (15)
| Country | Link |
|---|---|
| JP (1) | JPS517159A (pl) |
| AR (1) | AR209293A1 (pl) |
| CA (1) | CA1056645A (pl) |
| CH (1) | CH614845A5 (pl) |
| DE (1) | DE2507385C3 (pl) |
| DK (1) | DK68575A (pl) |
| FI (1) | FI57689C (pl) |
| FR (1) | FR2262100B1 (pl) |
| GB (1) | GB1504406A (pl) |
| IE (1) | IE40680B1 (pl) |
| NL (1) | NL7502109A (pl) |
| NO (1) | NO140365C (pl) |
| PL (1) | PL96145B3 (pl) |
| SE (1) | SE405929B (pl) |
| SU (1) | SU575008A3 (pl) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4154866A (en) * | 1976-08-24 | 1979-05-15 | Stange Co. | Method of producing from wood tar a liquid smoke product for use in food processing, and product of said method |
| US4594251A (en) * | 1983-04-08 | 1986-06-10 | Union Carbide Corporation | Preparation of tar-depleted liquid smoke treated casings |
| PL1753308T3 (pl) * | 2004-06-04 | 2011-04-29 | Kim Plaschke | Wytwarzanie ekstraktu dymu |
| CN111165869B (zh) * | 2020-01-17 | 2021-11-05 | 湖南中烟工业有限责任公司 | 一种经低危害增烟处理的卷烟 |
-
1974
- 1974-02-22 PL PL1974169004A patent/PL96145B3/pl unknown
-
1975
- 1975-02-17 FI FI750433A patent/FI57689C/fi not_active IP Right Cessation
- 1975-02-18 NO NO750544A patent/NO140365C/no unknown
- 1975-02-20 SE SE7501926A patent/SE405929B/xx unknown
- 1975-02-20 DE DE2507385A patent/DE2507385C3/de not_active Expired
- 1975-02-21 JP JP50021789A patent/JPS517159A/ja active Pending
- 1975-02-21 NL NL7502109A patent/NL7502109A/xx not_active Application Discontinuation
- 1975-02-21 IE IE361/75A patent/IE40680B1/xx unknown
- 1975-02-21 SU SU7502110025A patent/SU575008A3/ru active
- 1975-02-21 DK DK68575*#A patent/DK68575A/da not_active Application Discontinuation
- 1975-02-21 GB GB7434/75A patent/GB1504406A/en not_active Expired
- 1975-02-21 CA CA220,598A patent/CA1056645A/en not_active Expired
- 1975-02-21 CH CH217075A patent/CH614845A5/xx not_active IP Right Cessation
- 1975-02-24 FR FR7505669A patent/FR2262100B1/fr not_active Expired
- 1975-02-24 AR AR257729A patent/AR209293A1/es active
Also Published As
| Publication number | Publication date |
|---|---|
| JPS517159A (en) | 1976-01-21 |
| PL96145B3 (pl) | 1977-12-31 |
| CA1056645A (en) | 1979-06-19 |
| NO140365B (no) | 1979-05-14 |
| SE7501926L (pl) | 1975-08-25 |
| IE40680B1 (en) | 1979-08-01 |
| SE405929B (sv) | 1979-01-15 |
| FI750433A7 (pl) | 1975-08-23 |
| GB1504406A (en) | 1978-03-22 |
| NL7502109A (nl) | 1975-08-26 |
| NO140365C (no) | 1979-08-22 |
| IE40680L (en) | 1975-08-22 |
| NO750544L (pl) | 1975-08-25 |
| AU7848275A (en) | 1976-08-26 |
| FR2262100A1 (pl) | 1975-09-19 |
| DE2507385A1 (de) | 1975-08-28 |
| CH614845A5 (en) | 1979-12-28 |
| DK68575A (pl) | 1975-10-27 |
| FI57689B (fi) | 1980-06-30 |
| DE2507385C3 (de) | 1980-07-03 |
| FR2262100B1 (pl) | 1978-10-27 |
| SU575008A3 (ru) | 1977-09-30 |
| DE2507385B2 (de) | 1979-10-25 |
| AR209293A1 (es) | 1977-04-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM | Patent lapsed |
Owner name: INSTYTUT PRZEMYSLU MIESNEGO |