ES8604036A1 - Procedimiento para la reelaboracion de catalizadores de fluoracion - Google Patents
Procedimiento para la reelaboracion de catalizadores de fluoracionInfo
- Publication number
- ES8604036A1 ES8604036A1 ES544541A ES544541A ES8604036A1 ES 8604036 A1 ES8604036 A1 ES 8604036A1 ES 544541 A ES544541 A ES 544541A ES 544541 A ES544541 A ES 544541A ES 8604036 A1 ES8604036 A1 ES 8604036A1
- Authority
- ES
- Spain
- Prior art keywords
- fluoridization
- regeneration
- catalyst
- recovery process
- paste
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/72—Copper
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PROCEDIMIENTO PARA LA REELABORACION DE CATALIZADOR DE FLUORACION. COMPRENDE: A) MEZCLAR A LOS CATALIZADORES VIEJOS CON OXIDO DE MAGNESIO O HIDROXIDO DE MAGNESIO EN PRESENCIA DE GRAN CANTIDAD DE AGUA; B) CONCENTRAR Y EVAPORAR LA MEZCLA; C) AMASAR LA MEZCLA EN UN AMASADOR DUPLEX, PARA FORMAR UNA PASTA; D) SECAR LA PASTA A UNA TEMPERATURA ENTRE 40 Y 150JC, Y BAJO VACIO; Y E) TRATAR A LA PASTA SECA CON UNA CORRIENTE DE FLUORURO DE HIDROGENO (FH) EN GAS INERTE COMO NITROGENO Y AIRE, A UNA TEMPERATURA ENTRE 100J Y 400JC, DURANTE 0,5 A 10 HORAS. LAS CANTIDADES DE REACTIVOS SON 0,01 A 1 KG MGO O 0,00145-1,45 KG DE MG(OH)2 POR 1 KG DE CATALIZADOR VIEJO Y 0,2 A 2 MOLES DE FLUORURO DE HIDROGENO POR MOL DE OXIDO O HIDROXIDO DE MAGNESIO. SE UTILIZAN COMO REACTORES DE LECHO FIJO, LECHO FLUIDO O DE CAPA TURBULENTA PARA REACCIONES DE FLUORACION Y/O DISMINUCION CON HALOGENOS/ALCANOS.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19843423625 DE3423625A1 (de) | 1984-06-27 | 1984-06-27 | Verfahren zur wiederaufbereitung von fluorierungskatalysatoren |
Publications (2)
Publication Number | Publication Date |
---|---|
ES8604036A1 true ES8604036A1 (es) | 1986-02-01 |
ES544541A0 ES544541A0 (es) | 1986-02-01 |
Family
ID=6239238
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES544541A Expired ES8604036A1 (es) | 1984-06-27 | 1985-06-25 | Procedimiento para la reelaboracion de catalizadores de fluoracion |
Country Status (10)
Country | Link |
---|---|
US (1) | US4578369A (es) |
EP (1) | EP0166336B1 (es) |
JP (1) | JPS6115738A (es) |
AR (1) | AR242129A1 (es) |
AU (1) | AU567274B2 (es) |
BR (1) | BR8503063A (es) |
CA (1) | CA1242691A (es) |
DE (2) | DE3423625A1 (es) |
ES (1) | ES8604036A1 (es) |
GR (1) | GR851545B (es) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0788326B2 (ja) * | 1987-11-26 | 1995-09-27 | 旭硝子株式会社 | 1,1−ジクロロ−1,2,2,2−テトラフルオロエタンの製造方法 |
US5227350A (en) * | 1990-09-14 | 1993-07-13 | Imperial Chemical Industries Plc | Fluorination catalyst regeneration |
GB9020084D0 (en) * | 1990-09-14 | 1990-10-24 | Ici Plc | Chemical process |
GB9105166D0 (en) * | 1991-03-12 | 1991-04-24 | Ici Plc | Chemical process |
GB9219720D0 (en) * | 1992-09-17 | 1992-10-28 | Ici Plc | Catalyst production |
JP4397687B2 (ja) * | 2001-06-28 | 2010-01-13 | ハネウェル・インターナショナル・インコーポレーテッド | 弗素化触媒を調製する方法 |
JP4327012B2 (ja) * | 2003-05-06 | 2009-09-09 | 株式会社日本触媒 | クロム系触媒の回収方法 |
FR2998815B1 (fr) * | 2012-12-03 | 2017-01-27 | Arkema France | Catalyseur prepare par broyage reactif |
CN108579726A (zh) * | 2018-04-10 | 2018-09-28 | 湖北省宏源药业科技股份有限公司 | 一种利用废弃铬酸洗液制备铬基氟化催化剂的方法 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2745886A (en) * | 1955-01-31 | 1956-05-15 | Dow Chemical Co | Process for fluorinating aliphatic halohydrocarbons with a chromium fluoride catalyst and process for preparing the catalyst |
DE1194826B (de) * | 1963-06-29 | 1965-06-16 | Hoechst Ag | Verfahren zur Stabilisierung und/oder Aktivierung von Fluorierungskatalysatoren der Chromoxyfluoridgruppe |
DE1767200B1 (de) * | 1968-04-11 | 1971-12-30 | Hoechst Ag | Verfahren zur Regenerierung von Fluorierungskatalysatoren der Chromoxyfluoridgruppe |
DE2702360A1 (de) * | 1977-01-21 | 1978-08-03 | Hoechst Ag | Verfahren zur reaktivierung von fluorierungskatalysatoren |
JPS5617146A (en) * | 1979-07-20 | 1981-02-18 | Japan Steel Works Ltd:The | Production of long sized hollow material by outer circumferential restraining |
-
1984
- 1984-06-27 DE DE19843423625 patent/DE3423625A1/de not_active Withdrawn
-
1985
- 1985-06-15 DE DE8585107422T patent/DE3572314D1/de not_active Expired
- 1985-06-15 EP EP85107422A patent/EP0166336B1/de not_active Expired
- 1985-06-24 GR GR851545A patent/GR851545B/el unknown
- 1985-06-25 ES ES544541A patent/ES8604036A1/es not_active Expired
- 1985-06-25 US US06/748,546 patent/US4578369A/en not_active Expired - Lifetime
- 1985-06-25 AR AR85300799A patent/AR242129A1/es active
- 1985-06-26 JP JP60138056A patent/JPS6115738A/ja active Granted
- 1985-06-26 CA CA000485281A patent/CA1242691A/en not_active Expired
- 1985-06-26 BR BR8503063A patent/BR8503063A/pt not_active IP Right Cessation
- 1985-06-26 AU AU44204/85A patent/AU567274B2/en not_active Ceased
Also Published As
Publication number | Publication date |
---|---|
JPH0533101B2 (es) | 1993-05-18 |
CA1242691A (en) | 1988-10-04 |
AU567274B2 (en) | 1987-11-12 |
AR242129A1 (es) | 1993-03-31 |
EP0166336A2 (de) | 1986-01-02 |
DE3572314D1 (en) | 1989-09-21 |
BR8503063A (pt) | 1986-03-11 |
AU4420485A (en) | 1986-01-02 |
GR851545B (es) | 1985-11-25 |
US4578369A (en) | 1986-03-25 |
EP0166336A3 (en) | 1987-10-28 |
DE3423625A1 (de) | 1986-01-02 |
EP0166336B1 (de) | 1989-08-16 |
JPS6115738A (ja) | 1986-01-23 |
ES544541A0 (es) | 1986-02-01 |
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Robertson | Old is new |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PC1A | Transfer granted |