ES350827A1 - Preparation of trialkylamines - Google Patents

Preparation of trialkylamines

Info

Publication number
ES350827A1
ES350827A1 ES350827A ES350827A ES350827A1 ES 350827 A1 ES350827 A1 ES 350827A1 ES 350827 A ES350827 A ES 350827A ES 350827 A ES350827 A ES 350827A ES 350827 A1 ES350827 A1 ES 350827A1
Authority
ES
Spain
Prior art keywords
alkyl
atoms
dialkanolamine
ammonia
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES350827A
Other languages
Spanish (es)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Baird Chemical Industries Inc
Original Assignee
Baird Chemical Industries Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Baird Chemical Industries Inc filed Critical Baird Chemical Industries Inc
Publication of ES350827A1 publication Critical patent/ES350827A1/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/02—Amines; Quaternary ammonium compounds
    • A01N33/12—Quaternary ammonium compounds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/46—Compounds containing quaternary nitrogen atoms
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/46—Compounds containing quaternary nitrogen atoms
    • D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic

Abstract

Tertiary amines are prepared by reacting an alkyl chloride with ammonia, a primary amine of formula R111NH 2 where R111 is an alkyl, hydroxyalkyl, alkoxyalkyl or hydroxyalkoxyalkyl group having from 1 to 4 C atoms or an aralkyl group wherein the alkyl group has from 1-4 C atoms or a dialkanolamine or an alkyl bromide with ammonia or a dialkanolamine in the presence of a soluble iodide catalyst. The alkyl halides preferably have from 4 to 22 C atoms and the process is carried out within the temperature range 80-200 C. The reaction is generally performed as a twophase system wherein the first phase is organic and comprises the alkyl halide and the second phase is aqueous and comprises water and/or a low molecular weight alcohol of 1-6 C atoms, preferably isopropanol. The catalyst is usually an alkali metal iodide such as potassium iodide. During the reaction an alkaline material such as caustic soda is added in controlled amounts.
ES350827A 1966-07-18 1968-02-23 Preparation of trialkylamines Expired ES350827A1 (en)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
US56573566A 1966-07-18 1966-07-18
US61341167A 1967-02-02 1967-02-02
US61780367A 1967-02-23 1967-02-23
US61780567A 1967-02-23 1967-02-23
US70354668A 1968-02-07 1968-02-07
US70359868A 1968-02-07 1968-02-07
US00174933A US3836669A (en) 1966-07-18 1971-08-25 Method of killing bacteria using didecyl dimethyl ammonium chloride

Publications (1)

Publication Number Publication Date
ES350827A1 true ES350827A1 (en) 1969-05-16

Family

ID=27569138

Family Applications (2)

Application Number Title Priority Date Filing Date
ES350826A Expired ES350826A1 (en) 1966-07-18 1968-02-23 Preparation of trialkylamines
ES350827A Expired ES350827A1 (en) 1966-07-18 1968-02-23 Preparation of trialkylamines

Family Applications Before (1)

Application Number Title Priority Date Filing Date
ES350826A Expired ES350826A1 (en) 1966-07-18 1968-02-23 Preparation of trialkylamines

Country Status (11)

Country Link
US (3) US3472900A (en)
BE (3) BE701166A (en)
CH (3) CH526906A (en)
DE (2) DE1643235B2 (en)
ES (2) ES350826A1 (en)
FR (2) FR1572248A (en)
GB (3) GB1130905A (en)
LU (3) LU54078A1 (en)
NL (3) NL6709647A (en)
SE (1) SE369729B (en)
SU (1) SU667112A3 (en)

Families Citing this family (45)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU5697073A (en) 1972-07-10 1974-12-19 Colgate Palmolive Co Liquid cleaner liquid cleaner
ZA733982B (en) * 1972-07-10 1975-01-29 Colgate Palmolive Co All-pupose liquid cleaner
US3920735A (en) * 1973-05-21 1975-11-18 Standard Oil Co Zirconium enhanced activity of transition metal-bromine catalysis of di- and trimethyl benzene oxidation in liquid phase
US3974214A (en) * 1974-02-27 1976-08-10 Atlantic Richfield Company Isophthalic acid manufacture
US4073888A (en) 1974-06-18 1978-02-14 Pettibone Laboratories, Inc. Chlorine dioxide and quaternary ammonium salts as sterilizing agents
US4370314A (en) * 1975-12-08 1983-01-25 Colgate-Palmolive Company Oral composition containing antibacterial agent
CA1061675A (en) * 1976-01-13 1979-09-04 Lawrence L. Schwalley Antimicrobial cleaning compositions
FR2383671A1 (en) * 1977-03-18 1978-10-13 Chemed Corp Disinfectants effective against Mycobacterium tuberculosis - contain germicidal quat. ammonium salt and an alkoxylated amine cpd.
US4272395A (en) 1978-05-30 1981-06-09 Lever Brothers Company Germicidal compositions
US4336165A (en) * 1979-06-22 1982-06-22 S. C. Johnson & Son, Inc. Defoaming powdered carpet cleaning composition for use in extraction cleaning
US4320147A (en) * 1980-05-09 1982-03-16 Lonza Inc. Disinfectant composition and the use thereof
US4464398A (en) * 1981-08-11 1984-08-07 Huntington Laboratories, Inc. Germicide and an improved method for killing bacteria, fungus and/or viruses
US4450174A (en) * 1982-05-27 1984-05-22 Millmaster Onyx Group, Inc. Decyl quaternary ammonium compounds
GB2157678B (en) * 1982-05-27 1987-12-02 Millmaster Onyx Group Inc Anti-microbial di-decyl quaternary ammonium compounds
US4444790A (en) * 1982-05-27 1984-04-24 Millmaster Onyx Group, Inc. Quaternary ammonium disinfectants
US4576729A (en) * 1983-08-10 1986-03-18 Sterling Drug Inc. Liquid disinfectant laundry detergents
DD232417C2 (en) * 1984-11-27 1987-01-21 Fahlberg List Veb AGENTS FOR THE CONTROL OF PHYTOPATHOGENIC BACTERIA AND MUSHROOMS
AR242084A1 (en) * 1986-04-02 1993-03-31 Elisai Co Ltd Y Kao Corp Bactericidal composition and use thereof
US4857209A (en) * 1986-07-23 1989-08-15 Betz Laboratories, Inc. Method for controlling macroinvertebrates
DE3628801A1 (en) * 1986-08-25 1988-03-03 Henkel Kgaa ANTIMICROBIALLY EFFECTIVE MIXTURES
CA1302659C (en) * 1986-10-24 1992-06-09 Hans-Peter K. Gribi Dental impression material
GB2218635A (en) * 1988-05-20 1989-11-22 Pitney Bowes Inc Moistening solution containing an anti microbial agent
US5008030A (en) * 1989-01-17 1991-04-16 Colgate-Palmolive Co. Acidic disinfectant all-purpose liquid cleaning composition
US5185214A (en) * 1991-06-12 1993-02-09 Levan Susan L One step process for imparting decay resistance and fire retardancy to wood products
WO1993021766A1 (en) * 1992-04-27 1993-11-11 Ethyl Corporation Quaternary ammonium composition and process
US5414124A (en) * 1993-01-19 1995-05-09 Huntington Laboratories, Inc. Method of preparing quarternary ammonium formulations with high flash points
US5389685A (en) * 1993-06-10 1995-02-14 Huntington Laboratories, Inc. Stabilizer disinfectant formulation
EP0639636B1 (en) * 1993-08-19 2001-10-31 Kao Corporation Germicidal-disinfectant detergent composition
GB9323270D0 (en) * 1993-11-12 1994-01-05 Green Bruce P Disinfectant composition
US5385604A (en) * 1993-12-20 1995-01-31 Huntington Laboratories, Inc. Germicide resistant floor finish
BR9506419A (en) * 1994-10-21 1997-09-09 Japan Clinic Co Ltd Microbicidal composition and sterilization process
US5585403A (en) * 1994-12-07 1996-12-17 Tamura Seiyaku Kabushiki Kaisha Sterilizing agent for preventing coccidiosis in animals
DE69602847T2 (en) 1995-08-15 2000-02-17 Johnson S C Comm Markets Inc TUBERKILICIDE SYNERGISTIC DISINFECTING COMPOSITION AND METHOD FOR DISINFECTING
WO1998022427A1 (en) 1996-11-18 1998-05-28 Gaba International Ag Aminohydrofluorides and their use as oral hygiene preparations
CA2303266C (en) 1997-09-03 2004-06-01 S. C. Johnson & Son, Inc. Method of disinfecting and inhibiting mold and mildew growth on non-porous hard surfaces
US20040138176A1 (en) * 2002-05-31 2004-07-15 Cjb Industries, Inc. Adjuvant for pesticides
CH703678B1 (en) * 2004-04-06 2012-03-15 Empa Testmaterialien Ag Method and apparatus for testing bactericidal effect of substances.
US20080260716A1 (en) * 2004-07-09 2008-10-23 Nanosonics Pty Limited Method and Composition for High Level Disinfection Employing Quaternary Ammonium Compounds
US7476646B1 (en) * 2004-09-27 2009-01-13 Cjb Industries, Inc. Agricultural promoters/active ingredients
US7550627B2 (en) * 2005-03-08 2009-06-23 Eastman Chemical Company Processes for producing aromatic dicarboxylic acids
US20060205974A1 (en) * 2005-03-08 2006-09-14 Lavoie Gino G Processes for producing aromatic dicarboxylic acids
GB0803026D0 (en) * 2008-02-20 2008-03-26 Enviroquest Group Ltd External surface treatment system
WO2009136561A1 (en) * 2008-05-09 2009-11-12 国立大学法人広島大学 Method of fixing antibacterial agent and article obtained by the method
WO2011097490A1 (en) * 2010-02-08 2011-08-11 Ndsu Research Foundation Method of producing polyalkylated oligoalkylenepolyamines
BR112019007795A2 (en) 2016-10-18 2019-07-09 Sterilex LLC ambient moisture activated surface treatment powder

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2040396A (en) * 1931-12-26 1936-05-12 Universal Oil Prod Co Treatment of hydrocarbon oils
US2304637A (en) * 1939-11-30 1942-12-08 Du Pont Resinous anion exchange material

Also Published As

Publication number Publication date
CH276269A4 (en) 1970-05-15
BE710970A (en) 1968-07-01
NL6802353A (en) 1968-08-26
CH501580A (en) 1971-01-15
ES350826A1 (en) 1969-05-16
US3607919A (en) 1971-09-21
CH526906A (en) 1972-08-31
GB1221224A (en) 1971-02-03
DE1668871A1 (en) 1972-02-24
BE710971A (en) 1968-07-01
LU55555A1 (en) 1968-05-06
LU54078A1 (en) 1967-09-11
SU667112A3 (en) 1979-06-05
LU55557A1 (en) 1968-05-06
NL6709647A (en) 1968-01-19
BE701166A (en) 1967-12-18
SE369729B (en) 1974-09-16
NL6802352A (en) 1968-08-26
FR1572248A (en) 1969-06-27
GB1220947A (en) 1971-01-27
FR1572247A (en) 1969-06-27
US3836669A (en) 1974-09-17
DE1643235A1 (en) 1972-03-02
CH487590A (en) 1970-05-15
US3472900A (en) 1969-10-14
CH258868A4 (en) 1972-04-14
DE1643235B2 (en) 1977-02-10
GB1130905A (en) 1968-10-16

Similar Documents

Publication Publication Date Title
ES350826A1 (en) Preparation of trialkylamines
GB1056190A (en) Method of preparing polyamines and products thereof
GB672106A (en) Improvements in or relating to preparation of azo compounds
GB1510131A (en) Preparation and purification of cellulose ethers
CN107721862B (en) Synthesis method of N, N, N-trimethyl-1-adamantyl ammonium halide
GB1523949A (en) Process for recovering organotin halides
GB632346A (en) Improvements in and relating to the preparation of 1:4-dihalobutanes
GB1100713A (en) 3-deoxyribofuranosyl derivatives
GB1427902A (en) Process for the preparation of 1,3-dichloro-butene-2
GB1438125A (en) Preparation of a-aminoalcohols
GB777544A (en) Water soluble organic copper compounds and a process for their production
KR840001967A (en) Method for preparing 2'-substituted-spiro [benzofuran-2 (3H), 1'-cycloalkane]
ES363660A1 (en) Process for producing 1-alkyl (or alkenyl)-2-aminoalkylpyrrolidines and intermediates therefor
US2735848A (en) Amese salts of penicillin g
GB999595A (en) Improvements in or relating to oximes and the manufacture thereof
US2781374A (en) Detergent sulphonic acid and sulphate salts of certain amphoteric detergents
GB1397220A (en) Microbicidal aliphatic polyamines
GB1366662A (en) 6- /3-cyanopropyl/ -tetrahydropyran derivates and a process for the preparation thereof
GB1203540A (en) A process for manufacturing 6-nitro-2-oximinohexanoic acid and derivatives thereof
GB1416434A (en) Manufacture of pyrimidines
GB1142225A (en) Isocyanate derivatives of dihydropyran
GB1104323A (en) 3-phenylpyrrole derivatives and process for preparing the same
GB846377A (en) 2-substituted-2-propargyl propanediol dicarbamates
GB1436854A (en) Process for preparing cyclopronane derivatives
GB902014A (en) A process for the preparation of tertiary acetylenic alcohols