ES350827A1 - Preparation of trialkylamines - Google Patents
Preparation of trialkylaminesInfo
- Publication number
- ES350827A1 ES350827A1 ES350827A ES350827A ES350827A1 ES 350827 A1 ES350827 A1 ES 350827A1 ES 350827 A ES350827 A ES 350827A ES 350827 A ES350827 A ES 350827A ES 350827 A1 ES350827 A1 ES 350827A1
- Authority
- ES
- Spain
- Prior art keywords
- alkyl
- atoms
- dialkanolamine
- ammonia
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/12—Quaternary ammonium compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
- D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
Landscapes
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Plant Pathology (AREA)
- Zoology (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Microbiology (AREA)
- Environmental Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Detergent Compositions (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Tertiary amines are prepared by reacting an alkyl chloride with ammonia, a primary amine of formula R111NH 2 where R111 is an alkyl, hydroxyalkyl, alkoxyalkyl or hydroxyalkoxyalkyl group having from 1 to 4 C atoms or an aralkyl group wherein the alkyl group has from 1-4 C atoms or a dialkanolamine or an alkyl bromide with ammonia or a dialkanolamine in the presence of a soluble iodide catalyst. The alkyl halides preferably have from 4 to 22 C atoms and the process is carried out within the temperature range 80-200 C. The reaction is generally performed as a twophase system wherein the first phase is organic and comprises the alkyl halide and the second phase is aqueous and comprises water and/or a low molecular weight alcohol of 1-6 C atoms, preferably isopropanol. The catalyst is usually an alkali metal iodide such as potassium iodide. During the reaction an alkaline material such as caustic soda is added in controlled amounts.
Applications Claiming Priority (7)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US56573566A | 1966-07-18 | 1966-07-18 | |
US61341167A | 1967-02-02 | 1967-02-02 | |
US61780567A | 1967-02-23 | 1967-02-23 | |
US61780367A | 1967-02-23 | 1967-02-23 | |
US70359868A | 1968-02-07 | 1968-02-07 | |
US70354668A | 1968-02-07 | 1968-02-07 | |
US00174933A US3836669A (en) | 1966-07-18 | 1971-08-25 | Method of killing bacteria using didecyl dimethyl ammonium chloride |
Publications (1)
Publication Number | Publication Date |
---|---|
ES350827A1 true ES350827A1 (en) | 1969-05-16 |
Family
ID=27569138
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES350826A Expired ES350826A1 (en) | 1966-07-18 | 1968-02-23 | Preparation of trialkylamines |
ES350827A Expired ES350827A1 (en) | 1966-07-18 | 1968-02-23 | Preparation of trialkylamines |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES350826A Expired ES350826A1 (en) | 1966-07-18 | 1968-02-23 | Preparation of trialkylamines |
Country Status (11)
Country | Link |
---|---|
US (3) | US3472900A (en) |
BE (3) | BE701166A (en) |
CH (3) | CH501580A (en) |
DE (2) | DE1643235B2 (en) |
ES (2) | ES350826A1 (en) |
FR (2) | FR1572248A (en) |
GB (3) | GB1130905A (en) |
LU (3) | LU54078A1 (en) |
NL (3) | NL6709647A (en) |
SE (1) | SE369729B (en) |
SU (1) | SU667112A3 (en) |
Families Citing this family (45)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AU5697073A (en) | 1972-07-10 | 1974-12-19 | Colgate Palmolive Co | Liquid cleaner liquid cleaner |
ZA733982B (en) * | 1972-07-10 | 1975-01-29 | Colgate Palmolive Co | All-pupose liquid cleaner |
US3920735A (en) * | 1973-05-21 | 1975-11-18 | Standard Oil Co | Zirconium enhanced activity of transition metal-bromine catalysis of di- and trimethyl benzene oxidation in liquid phase |
US3974214A (en) * | 1974-02-27 | 1976-08-10 | Atlantic Richfield Company | Isophthalic acid manufacture |
US4073888A (en) | 1974-06-18 | 1978-02-14 | Pettibone Laboratories, Inc. | Chlorine dioxide and quaternary ammonium salts as sterilizing agents |
US4370314A (en) * | 1975-12-08 | 1983-01-25 | Colgate-Palmolive Company | Oral composition containing antibacterial agent |
CA1061675A (en) * | 1976-01-13 | 1979-09-04 | Lawrence L. Schwalley | Antimicrobial cleaning compositions |
FR2383671A1 (en) * | 1977-03-18 | 1978-10-13 | Chemed Corp | Disinfectants effective against Mycobacterium tuberculosis - contain germicidal quat. ammonium salt and an alkoxylated amine cpd. |
US4272395A (en) | 1978-05-30 | 1981-06-09 | Lever Brothers Company | Germicidal compositions |
US4336165A (en) * | 1979-06-22 | 1982-06-22 | S. C. Johnson & Son, Inc. | Defoaming powdered carpet cleaning composition for use in extraction cleaning |
US4320147A (en) * | 1980-05-09 | 1982-03-16 | Lonza Inc. | Disinfectant composition and the use thereof |
US4464398A (en) * | 1981-08-11 | 1984-08-07 | Huntington Laboratories, Inc. | Germicide and an improved method for killing bacteria, fungus and/or viruses |
US4444790A (en) * | 1982-05-27 | 1984-04-24 | Millmaster Onyx Group, Inc. | Quaternary ammonium disinfectants |
FR2562888B1 (en) * | 1982-05-27 | 1989-01-20 | Millmaster Onyx Group Inc | BACTERICIDAL QUATERNARY AMMONIUM COMPOUNDS |
US4450174A (en) * | 1982-05-27 | 1984-05-22 | Millmaster Onyx Group, Inc. | Decyl quaternary ammonium compounds |
US4576729A (en) * | 1983-08-10 | 1986-03-18 | Sterling Drug Inc. | Liquid disinfectant laundry detergents |
DD232417C2 (en) * | 1984-11-27 | 1987-01-21 | Fahlberg List Veb | AGENTS FOR THE CONTROL OF PHYTOPATHOGENIC BACTERIA AND MUSHROOMS |
DK168909B1 (en) * | 1986-04-02 | 1994-07-11 | Kao Corp | Mixture comprising didecyldimethylammonium chlorideand an addition product between alkylene oxide and a least trivalent polyol, aqueous solution of such mixture, and antibacterial use of the mixture or its aqueous solution |
US4857209A (en) * | 1986-07-23 | 1989-08-15 | Betz Laboratories, Inc. | Method for controlling macroinvertebrates |
DE3628801A1 (en) * | 1986-08-25 | 1988-03-03 | Henkel Kgaa | ANTIMICROBIALLY EFFECTIVE MIXTURES |
CA1302659C (en) * | 1986-10-24 | 1992-06-09 | Hans-Peter K. Gribi | Dental impression material |
GB2218635A (en) * | 1988-05-20 | 1989-11-22 | Pitney Bowes Inc | Moistening solution containing an anti microbial agent |
US5008030A (en) * | 1989-01-17 | 1991-04-16 | Colgate-Palmolive Co. | Acidic disinfectant all-purpose liquid cleaning composition |
US5185214A (en) * | 1991-06-12 | 1993-02-09 | Levan Susan L | One step process for imparting decay resistance and fire retardancy to wood products |
WO1993021766A1 (en) * | 1992-04-27 | 1993-11-11 | Ethyl Corporation | Quaternary ammonium composition and process |
US5414124A (en) * | 1993-01-19 | 1995-05-09 | Huntington Laboratories, Inc. | Method of preparing quarternary ammonium formulations with high flash points |
US5389685A (en) * | 1993-06-10 | 1995-02-14 | Huntington Laboratories, Inc. | Stabilizer disinfectant formulation |
DE69428847T2 (en) * | 1993-08-19 | 2002-04-11 | Kao Corp., Tokio/Tokyo | Germicidal and disinfectant detergent and cleaning agent composition |
GB9323270D0 (en) * | 1993-11-12 | 1994-01-05 | Green Bruce P | Disinfectant composition |
US5385604A (en) * | 1993-12-20 | 1995-01-31 | Huntington Laboratories, Inc. | Germicide resistant floor finish |
KR100196460B1 (en) * | 1994-10-21 | 1999-06-15 | 노무라 미쯔요시 | Antimicrobial agent containing quaternary ammonium salt |
US5585403A (en) * | 1994-12-07 | 1996-12-17 | Tamura Seiyaku Kabushiki Kaisha | Sterilizing agent for preventing coccidiosis in animals |
ATE180944T1 (en) | 1995-08-15 | 1999-06-15 | Johnson S C Comm Markets Inc | TUBERCILICIDE SYNERGISTIC DISINFECTANT COMPOSITION AND METHOD FOR DISINFECTION |
DK0944579T3 (en) | 1996-11-18 | 2002-01-07 | Gaba Internat | Amine hydrofluorides and their use as oral hygiene agents |
NZ503088A (en) | 1997-09-03 | 2001-11-30 | S | Method and cleaning composition for sanitizing, disinfecting and inhibiting mold and mildew growth on non-porous hard surfaces |
US20040138176A1 (en) * | 2002-05-31 | 2004-07-15 | Cjb Industries, Inc. | Adjuvant for pesticides |
CH703678B1 (en) * | 2004-04-06 | 2012-03-15 | Empa Testmaterialien Ag | Method and apparatus for testing bactericidal effect of substances. |
US20080260716A1 (en) * | 2004-07-09 | 2008-10-23 | Nanosonics Pty Limited | Method and Composition for High Level Disinfection Employing Quaternary Ammonium Compounds |
US7476646B1 (en) * | 2004-09-27 | 2009-01-13 | Cjb Industries, Inc. | Agricultural promoters/active ingredients |
US7550627B2 (en) * | 2005-03-08 | 2009-06-23 | Eastman Chemical Company | Processes for producing aromatic dicarboxylic acids |
US20060205974A1 (en) * | 2005-03-08 | 2006-09-14 | Lavoie Gino G | Processes for producing aromatic dicarboxylic acids |
GB0803026D0 (en) * | 2008-02-20 | 2008-03-26 | Enviroquest Group Ltd | External surface treatment system |
US8859009B2 (en) * | 2008-05-09 | 2014-10-14 | Hiroshima University | Method of fixing antibacterial agent and article obtained by the method |
WO2011097490A1 (en) * | 2010-02-08 | 2011-08-11 | Ndsu Research Foundation | Method of producing polyalkylated oligoalkylenepolyamines |
CN110114450B (en) | 2016-10-18 | 2020-07-03 | 斯特里莱克斯有限责任公司 | Ambient moisture activatable surface treatment powders |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2040396A (en) * | 1931-12-26 | 1936-05-12 | Universal Oil Prod Co | Treatment of hydrocarbon oils |
US2304637A (en) * | 1939-11-30 | 1942-12-08 | Du Pont | Resinous anion exchange material |
-
1967
- 1967-02-02 US US613411A patent/US3472900A/en not_active Expired - Lifetime
- 1967-02-23 US US617803A patent/US3607919A/en not_active Expired - Lifetime
- 1967-07-10 BE BE701166D patent/BE701166A/xx unknown
- 1967-07-11 LU LU54078D patent/LU54078A1/xx unknown
- 1967-07-12 NL NL6709647A patent/NL6709647A/xx unknown
- 1967-07-18 GB GB33000/67A patent/GB1130905A/en not_active Expired
- 1967-07-18 DE DE1967B0093532 patent/DE1643235B2/en active Granted
-
1968
- 1968-02-19 BE BE710970D patent/BE710970A/xx not_active IP Right Cessation
- 1968-02-19 NL NL6802352A patent/NL6802352A/xx unknown
- 1968-02-19 FR FR1572248D patent/FR1572248A/fr not_active Expired
- 1968-02-19 NL NL6802353A patent/NL6802353A/xx unknown
- 1968-02-19 FR FR1572247D patent/FR1572247A/fr not_active Expired
- 1968-02-19 BE BE710971D patent/BE710971A/xx unknown
- 1968-02-22 CH CH258768A patent/CH501580A/en not_active IP Right Cessation
- 1968-02-22 CH CH276269A patent/CH487590A/en not_active IP Right Cessation
- 1968-02-22 CH CH258868A patent/CH526906A/en not_active IP Right Cessation
- 1968-02-22 SE SE02331/68A patent/SE369729B/xx unknown
- 1968-02-23 GB GB8833/68A patent/GB1220947A/en not_active Expired
- 1968-02-23 DE DE19681668871 patent/DE1668871A1/en not_active Withdrawn
- 1968-02-23 ES ES350826A patent/ES350826A1/en not_active Expired
- 1968-02-23 LU LU55557D patent/LU55557A1/xx unknown
- 1968-02-23 LU LU55555D patent/LU55555A1/xx unknown
- 1968-02-23 ES ES350827A patent/ES350827A1/en not_active Expired
- 1968-02-23 GB GB8832/68A patent/GB1221224A/en not_active Expired
- 1968-03-14 SU SU681226198A patent/SU667112A3/en active
-
1971
- 1971-08-25 US US00174933A patent/US3836669A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
CH501580A (en) | 1971-01-15 |
LU55555A1 (en) | 1968-05-06 |
CH276269A4 (en) | 1970-05-15 |
CH258868A4 (en) | 1972-04-14 |
BE710970A (en) | 1968-07-01 |
GB1221224A (en) | 1971-02-03 |
NL6709647A (en) | 1968-01-19 |
LU54078A1 (en) | 1967-09-11 |
GB1130905A (en) | 1968-10-16 |
BE701166A (en) | 1967-12-18 |
DE1668871A1 (en) | 1972-02-24 |
SU667112A3 (en) | 1979-06-05 |
US3472900A (en) | 1969-10-14 |
CH526906A (en) | 1972-08-31 |
FR1572248A (en) | 1969-06-27 |
NL6802353A (en) | 1968-08-26 |
ES350826A1 (en) | 1969-05-16 |
FR1572247A (en) | 1969-06-27 |
US3607919A (en) | 1971-09-21 |
SE369729B (en) | 1974-09-16 |
DE1643235A1 (en) | 1972-03-02 |
CH487590A (en) | 1970-05-15 |
BE710971A (en) | 1968-07-01 |
DE1643235B2 (en) | 1977-02-10 |
GB1220947A (en) | 1971-01-27 |
US3836669A (en) | 1974-09-17 |
LU55557A1 (en) | 1968-05-06 |
NL6802352A (en) | 1968-08-26 |
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