ES2651675T3 - Producción de grafeno a partir de alcóxido de metal - Google Patents
Producción de grafeno a partir de alcóxido de metal Download PDFInfo
- Publication number
- ES2651675T3 ES2651675T3 ES10729930.7T ES10729930T ES2651675T3 ES 2651675 T3 ES2651675 T3 ES 2651675T3 ES 10729930 T ES10729930 T ES 10729930T ES 2651675 T3 ES2651675 T3 ES 2651675T3
- Authority
- ES
- Spain
- Prior art keywords
- metal alkoxide
- solution
- graphene production
- introducing
- droplets
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 150000004703 alkoxides Chemical class 0.000 title abstract 4
- 239000002184 metal Substances 0.000 title abstract 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title abstract 3
- 229910021389 graphene Inorganic materials 0.000 title abstract 3
- 238000000354 decomposition reaction Methods 0.000 abstract 2
- 239000000443 aerosol Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000003595 mist Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 239000007921 spray Substances 0.000 abstract 1
- 238000005979 thermal decomposition reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/182—Graphene
- C01B32/184—Preparation
- C01B32/186—Preparation by chemical vapour deposition [CVD]
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/22—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
- C23C16/26—Deposition of carbon only
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J6/00—Heat treatments such as Calcining; Fusing ; Pyrolysis
- B01J6/008—Pyrolysis reactions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/182—Graphene
- C01B32/184—Preparation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/182—Graphene
- C01B32/194—After-treatment
- C01B32/196—Purification
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2204/00—Structure or properties of graphene
- C01B2204/04—Specific amount of layers or specific thickness
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2204/00—Structure or properties of graphene
- C01B2204/20—Graphene characterized by its properties
- C01B2204/22—Electronic properties
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Nanotechnology (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Crystallography & Structural Chemistry (AREA)
- General Physics & Mathematics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- General Chemical & Material Sciences (AREA)
- Composite Materials (AREA)
- Manufacturing & Machinery (AREA)
- Thermal Sciences (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
Un proceso para producir grafeno, caracterizado por la etapa de: introducir una solución (102) de un alcóxido de metal en un disolvente en un aparato de descomposición, en el que la etapa de introducir la solución incluye crear gotitas que comprenden una aspersión o bruma o aerosol (108) de la solución de alcóxido de metal, en el que el aparato de descomposición incluye una primera región (106) que tiene una temperatura suficientemente alta para causar la descomposición térmica del alcóxido de metal, para producir grafeno y en el que se crean las gotitas y se introducen en una corriente de gas (110).
Description
Claims (1)
-
imagen1 imagen2 imagen3
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GBGB0913011.3A GB0913011D0 (en) | 2009-07-27 | 2009-07-27 | Graphene |
GB0913011 | 2009-07-27 | ||
PCT/GB2010/051099 WO2011012874A1 (en) | 2009-07-27 | 2010-07-02 | Production of graphene from metal alkoxide |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2651675T3 true ES2651675T3 (es) | 2018-01-29 |
Family
ID=41066864
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES10729930.7T Active ES2651675T3 (es) | 2009-07-27 | 2010-07-02 | Producción de grafeno a partir de alcóxido de metal |
Country Status (8)
Country | Link |
---|---|
US (1) | US9932227B2 (es) |
EP (1) | EP2459484B1 (es) |
JP (2) | JP5767218B2 (es) |
KR (3) | KR20120039665A (es) |
CN (1) | CN102498061A (es) |
ES (1) | ES2651675T3 (es) |
GB (1) | GB0913011D0 (es) |
WO (1) | WO2011012874A1 (es) |
Families Citing this family (34)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2011017338A2 (en) * | 2009-08-03 | 2011-02-10 | University Of Idaho | Method for making graphene |
US20140150970A1 (en) | 2010-11-19 | 2014-06-05 | Ppg Industries Ohio, Inc. | Structural adhesive compositions |
US8796361B2 (en) | 2010-11-19 | 2014-08-05 | Ppg Industries Ohio, Inc. | Adhesive compositions containing graphenic carbon particles |
US20110086756A1 (en) * | 2010-12-20 | 2011-04-14 | Gao hong-jun | Method for preparing silicon intercalated monolayer graphene |
WO2012125854A1 (en) * | 2011-03-15 | 2012-09-20 | Peerless Worldwide, Llc | Facile synthesis of graphene, graphene derivatives and abrasive nanoparticles and their various uses, including as tribologically-beneficial lubricant additives |
KR101349912B1 (ko) | 2011-04-27 | 2014-01-13 | 한국지질자원연구원 | Pt/GR(Graphene) 나노복합체 및 그 제조방법 |
US10135059B2 (en) | 2011-06-30 | 2018-11-20 | Northwestern University | Crumpled particles, methods of synthesizing same and applications using same |
US20130266501A1 (en) * | 2011-07-05 | 2013-10-10 | Rutgers, The State University Of New Jersey | Direct Production of Large and Highly Conductive Low-Oxygen Graphene Sheets and Monodispersed Low-Oxygen Graphene Nanosheets |
US9761903B2 (en) | 2011-09-30 | 2017-09-12 | Ppg Industries Ohio, Inc. | Lithium ion battery electrodes including graphenic carbon particles |
DE102011054103A1 (de) * | 2011-09-30 | 2013-04-04 | MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. | Verfahren zum Herstellen von Graphen-Nanobändern |
US9475946B2 (en) | 2011-09-30 | 2016-10-25 | Ppg Industries Ohio, Inc. | Graphenic carbon particle co-dispersions and methods of making same |
US10294375B2 (en) | 2011-09-30 | 2019-05-21 | Ppg Industries Ohio, Inc. | Electrically conductive coatings containing graphenic carbon particles |
US9574094B2 (en) | 2013-12-09 | 2017-02-21 | Ppg Industries Ohio, Inc. | Graphenic carbon particle dispersions and methods of making same |
US9832818B2 (en) | 2011-09-30 | 2017-11-28 | Ppg Industries Ohio, Inc. | Resistive heating coatings containing graphenic carbon particles |
US9938416B2 (en) | 2011-09-30 | 2018-04-10 | Ppg Industries Ohio, Inc. | Absorptive pigments comprising graphenic carbon particles |
US10763490B2 (en) | 2011-09-30 | 2020-09-01 | Ppg Industries Ohio, Inc. | Methods of coating an electrically conductive substrate and related electrodepositable compositions including graphenic carbon particles |
US8486363B2 (en) | 2011-09-30 | 2013-07-16 | Ppg Industries Ohio, Inc. | Production of graphenic carbon particles utilizing hydrocarbon precursor materials |
US10240052B2 (en) | 2011-09-30 | 2019-03-26 | Ppg Industries Ohio, Inc. | Supercapacitor electrodes including graphenic carbon particles |
US9988551B2 (en) | 2011-09-30 | 2018-06-05 | Ppg Industries Ohio, Inc. | Black pigments comprising graphenic carbon particles |
CN102515148B (zh) * | 2011-11-25 | 2013-12-25 | 东南大学 | 一种石墨烯铸体的铸造方法 |
CN103159208A (zh) * | 2011-12-14 | 2013-06-19 | 海洋王照明科技股份有限公司 | 一种制备石墨烯的方法 |
CN102627274B (zh) * | 2012-04-23 | 2013-11-06 | 中国科学院上海微系统与信息技术研究所 | 一种制备石墨烯的方法 |
US11430979B2 (en) | 2013-03-15 | 2022-08-30 | Ppg Industries Ohio, Inc. | Lithium ion battery anodes including graphenic carbon particles |
CN103332688B (zh) * | 2013-07-16 | 2015-08-19 | 中国科学院山西煤炭化学研究所 | 一种由有机酸金属盐合成石墨烯的方法 |
CN103601177B (zh) * | 2013-11-19 | 2015-04-29 | 中国科学院山西煤炭化学研究所 | 一种碱金属盐催化固体有机酸制备石墨烯的方法 |
KR101694751B1 (ko) * | 2014-08-21 | 2017-01-10 | (주)솔라세라믹 | 박막 형성을 위한 전구체 공급 장치 및 이를 포함하는 박막 형성 장치 |
GB201416317D0 (en) * | 2014-09-16 | 2014-10-29 | Swan Thomas & Co Ltd | Two-dimensional materials |
CN105036121A (zh) * | 2015-07-07 | 2015-11-11 | 哈尔滨工业大学 | 一种增强型石墨烯表面活性剂的制备方法 |
KR101813584B1 (ko) | 2015-09-02 | 2017-12-29 | 한국과학기술연구원 | 탄소나노구조체 및 이의 제조 방법 |
US10377928B2 (en) | 2015-12-10 | 2019-08-13 | Ppg Industries Ohio, Inc. | Structural adhesive compositions |
US10351661B2 (en) | 2015-12-10 | 2019-07-16 | Ppg Industries Ohio, Inc. | Method for producing an aminimide |
ITUB20161052A1 (it) * | 2016-02-25 | 2017-08-25 | Hygraner S R L | Metodo per la sintesi di grafene o di un suo derivato funzionalizzato, grafene o suo derivato funzionalizzato ottenuto da detto metodo e loro usi |
JP7441859B2 (ja) | 2019-05-20 | 2024-03-01 | ナノグラフ コーポレイション | 低欠陥乱層炭素を含むアノード活物質 |
CN110668432B (zh) * | 2019-09-27 | 2021-05-14 | 北京碳垣新材料科技有限公司 | 以金属粉末液相为基底生长石墨烯的装置 |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS60218344A (ja) * | 1984-04-14 | 1985-11-01 | Res Dev Corp Of Japan | アルミニウムアルコキシドの合成方法及びその装置 |
AU2003292716A1 (en) * | 2002-12-27 | 2004-07-29 | Bussan Nanotech Research Institute Inc. | Process and apparatus for producing single-walled carbon nanotube |
JP4834957B2 (ja) * | 2004-02-27 | 2011-12-14 | 住友電気工業株式会社 | 触媒構造体およびこれを用いたカーボンナノチューブの製造方法 |
CN101023027B (zh) * | 2004-09-22 | 2012-07-18 | 昭和电工株式会社 | 气相法碳纳米管的制造方法 |
US20070298168A1 (en) * | 2006-06-09 | 2007-12-27 | Rensselaer Polytechnic Institute | Multifunctional carbon nanotube based brushes |
WO2009029984A1 (en) * | 2007-09-03 | 2009-03-12 | Newsouth Innovations Pty Limited | Graphene |
US20090134369A1 (en) * | 2007-11-26 | 2009-05-28 | Applied Nanoworks, Inc. | Metal alkoxides, apparatus for manufacturing metal alkoxides, related methods and uses thereof |
-
2009
- 2009-07-27 GB GBGB0913011.3A patent/GB0913011D0/en not_active Ceased
-
2010
- 2010-07-02 EP EP10729930.7A patent/EP2459484B1/en not_active Not-in-force
- 2010-07-02 KR KR1020127002126A patent/KR20120039665A/ko active Application Filing
- 2010-07-02 CN CN2010800337284A patent/CN102498061A/zh active Pending
- 2010-07-02 WO PCT/GB2010/051099 patent/WO2011012874A1/en active Application Filing
- 2010-07-02 KR KR1020157017266A patent/KR101965882B1/ko active IP Right Grant
- 2010-07-02 ES ES10729930.7T patent/ES2651675T3/es active Active
- 2010-07-02 KR KR1020177037556A patent/KR101987390B1/ko active IP Right Grant
- 2010-07-02 US US13/384,881 patent/US9932227B2/en active Active
- 2010-07-02 JP JP2012522248A patent/JP5767218B2/ja not_active Expired - Fee Related
-
2015
- 2015-03-25 JP JP2015062526A patent/JP5932090B2/ja not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
KR101987390B1 (ko) | 2019-06-10 |
JP2013500233A (ja) | 2013-01-07 |
KR20180001601A (ko) | 2018-01-04 |
JP2015143187A (ja) | 2015-08-06 |
US9932227B2 (en) | 2018-04-03 |
US20120114551A1 (en) | 2012-05-10 |
JP5932090B2 (ja) | 2016-06-08 |
EP2459484B1 (en) | 2017-09-13 |
CN102498061A (zh) | 2012-06-13 |
KR20150082683A (ko) | 2015-07-15 |
WO2011012874A1 (en) | 2011-02-03 |
KR20120039665A (ko) | 2012-04-25 |
EP2459484A1 (en) | 2012-06-06 |
GB0913011D0 (en) | 2009-09-02 |
JP5767218B2 (ja) | 2015-08-19 |
KR101965882B1 (ko) | 2019-04-04 |
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