ES2567081T3 - Producción continua de sales cuaternarias - Google Patents

Producción continua de sales cuaternarias Download PDF

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Publication number
ES2567081T3
ES2567081T3 ES11735210.4T ES11735210T ES2567081T3 ES 2567081 T3 ES2567081 T3 ES 2567081T3 ES 11735210 T ES11735210 T ES 11735210T ES 2567081 T3 ES2567081 T3 ES 2567081T3
Authority
ES
Spain
Prior art keywords
phase
cstr
continuously
water
qap
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
ES11735210.4T
Other languages
English (en)
Inventor
Barbara E. Fair
Peter E. Reed
Leonard M. Ver Vers
Jr. Larry E. Brammer
Charles J. Holada
Cheng-Sung Huang
Kailas B. Sawant
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ChampionX LLC
Original Assignee
Nalco Co LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nalco Co LLC filed Critical Nalco Co LLC
Application granted granted Critical
Publication of ES2567081T3 publication Critical patent/ES2567081T3/es
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/08—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions not involving the formation of amino groups, hydroxy groups or etherified or esterified hydroxy groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C219/00—Compounds containing amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C219/02—Compounds containing amino and esterified hydroxy groups bound to the same carbon skeleton having esterified hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C219/20—Compounds containing amino and esterified hydroxy groups bound to the same carbon skeleton having esterified hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being unsaturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Un método para producir continuamente un producto de amina cuaternaria (QAP) que comprende las etapas de: alimentar continuamente los reactivos en un reactor de tanque agitado continuamente (CSTR), los reactivos que comprenden un sustrato de amina terciaria (TAS), agua, y un agente alquilante; mantener las condiciones en el CSTR de tal manera que se forman dos fases líquidas sustancialmente distintas, una primera fase y una segunda fase, la segunda fase que es más densa que la primera fase, la segunda fase que comprende más de 80 % de QAP y menos de 20 % de agua, la primera fase presente en más de 5 % en peso de la mezcla de reacción, y comprende TAS, y agente alquilante; no permitir que el contenido de agua del CSTR exceda 16 % de los reactivos añadidos continuamente al CSTR; y eliminar continuamente, solamente la segunda fase líquida del CSTR.

Description

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Claims (1)

  1. imagen1
ES11735210.4T 2010-01-21 2011-01-21 Producción continua de sales cuaternarias Active ES2567081T3 (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US12/691,159 US8247597B2 (en) 2010-01-21 2010-01-21 Continuous production of DMAEA quaternary salts
US691159 2010-01-21
PCT/US2011/021961 WO2011091197A2 (en) 2010-01-21 2011-01-21 Continuous production of quaternary salts

Publications (1)

Publication Number Publication Date
ES2567081T3 true ES2567081T3 (es) 2016-04-19

Family

ID=44278027

Family Applications (1)

Application Number Title Priority Date Filing Date
ES11735210.4T Active ES2567081T3 (es) 2010-01-21 2011-01-21 Producción continua de sales cuaternarias

Country Status (10)

Country Link
US (1) US8247597B2 (es)
EP (1) EP2526083B1 (es)
JP (1) JP5916629B2 (es)
KR (1) KR101782186B1 (es)
CN (2) CN102712573A (es)
BR (1) BR112012017631B1 (es)
CA (1) CA2786744C (es)
ES (1) ES2567081T3 (es)
MX (1) MX2012008452A (es)
WO (1) WO2011091197A2 (es)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2607351B1 (en) 2011-12-22 2017-03-15 Cerbios-Pharma S.A. Continuous process for the alkylation of cyclic tertiary amines
US9410288B2 (en) 2013-08-08 2016-08-09 Ecolab Usa Inc. Use of nanocrystaline cellulose and polymer grafted nanocrystaline cellulose for increasing retention in papermaking process
US9303360B2 (en) 2013-08-08 2016-04-05 Ecolab Usa Inc. Use of nanocrystaline cellulose and polymer grafted nanocrystaline cellulose for increasing retention in papermaking process
US9034145B2 (en) 2013-08-08 2015-05-19 Ecolab Usa Inc. Use of nanocrystaline cellulose and polymer grafted nanocrystaline cellulose for increasing retention, wet strength, and dry strength in papermaking process
US9834730B2 (en) 2014-01-23 2017-12-05 Ecolab Usa Inc. Use of emulsion polymers to flocculate solids in organic liquids
CN104744275A (zh) * 2015-03-23 2015-07-01 浙江友联化学工业有限公司 一种季铵盐型阳离子单体水溶液的制备方法
JP6998213B2 (ja) 2015-04-17 2022-01-18 コルテバ アグリサイエンス エルエルシー 農薬の効用を有する分子ならびに関連する中間体、組成物及びプロセス
CA3001717A1 (en) 2015-10-15 2017-04-20 Ecolab Usa Inc. Nanocrystalline cellulose and polymer-grafted nanocrystalline cellulose as rheology modifying agents for magnesium oxide and lime slurries
US10822442B2 (en) 2017-07-17 2020-11-03 Ecolab Usa Inc. Rheology-modifying agents for slurries

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3244274A1 (de) * 1982-11-30 1984-05-30 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung konzentrierter waessriger loesungen von quaternisierungsprodukten von tertiaeren aminoalkylestern oder tertiaeren aminoalkylamiden der acryl- oder methacrylsaeure
US5260480A (en) * 1988-02-11 1993-11-09 Norsolor Quaternization process
JPH03206067A (ja) * 1990-01-08 1991-09-09 Dai Ichi Kogyo Seiyaku Co Ltd Ｎ，ｎ―ジアルキルアミノアルキル（メタ）アクリレート類の４級化方法
JP2837279B2 (ja) * 1990-12-20 1998-12-14 三井化学株式会社 不飽和第四級アンモニウム塩の製造法
JPH07206790A (ja) 1994-01-20 1995-08-08 Mitsui Toatsu Chem Inc 不飽和第四級アンモニウム塩の製造方法
JPH08268985A (ja) * 1995-03-29 1996-10-15 Kohjin Co Ltd 不飽和第４級アンモニウム塩の製造法
FR2788767B1 (fr) 1999-01-21 2001-03-02 Atochem Elf Sa Procede de fabrication de solutions aqueuses de sels insatures d'ammonium quaternaire
JP2000229919A (ja) * 1999-02-12 2000-08-22 Mitsubishi Rayon Co Ltd 高純度不飽和第四級アンモニウム塩水溶液の製造方法
US6423871B1 (en) * 1999-02-26 2002-07-23 University Of South Florida Efficient synthesis of secondary amines by selective alkylation of primary amines
CN1276367A (zh) 1999-06-05 2000-12-13 中国石化集团齐鲁石油化工公司 一种不饱和季铵盐的制备方法
CN1126731C (zh) 1999-11-17 2003-11-05 中国石化集团齐鲁石油化工公司 一种不饱和季铵盐的制备方法
FR2824062B1 (fr) * 2001-04-27 2004-10-15 Atofina Procede de fabrication de solutions aqueuses de sels insatures d'ammonium quaternaire
JP4178837B2 (ja) 2002-05-29 2008-11-12 東亞合成株式会社 ジアルキルアミノアルキル（メタ）アクリレート４級塩の製造方法
JP2004010508A (ja) 2002-06-04 2004-01-15 Toagosei Co Ltd ジアルキルアミノアルキル（メタ）アクリレート４級塩の製造方法
JP4062055B2 (ja) 2002-11-01 2008-03-19 東亞合成株式会社 ジアルキルアミノアルキル（メタ）アクリレート４級塩の製造方法
JP2008081443A (ja) 2006-09-27 2008-04-10 Toagosei Co Ltd ジアルキルアミノアルキル（メタ）アクリレート４級塩の製造方法及びその製造装置
WO2009090791A1 (ja) * 2008-01-17 2009-07-23 Toagosei Co., Ltd. ジアルキルアミノアルキル（メタ）アクリレート４級塩の製造方法
CN201424446Y (zh) 2009-04-29 2010-03-17 北京恒聚化工集团有限责任公司 阳离子单体二甲胺基乙基丙烯酸脂氯甲烷季铵盐生产系统
US7973195B2 (en) * 2009-07-22 2011-07-05 Kemira Oyj Process for unsaturated quaternary ammonium salt

Also Published As

Publication number Publication date
CN105646241A (zh) 2016-06-08
WO2011091197A3 (en) 2011-12-29
US8247597B2 (en) 2012-08-21
CA2786744C (en) 2017-10-17
KR20120116440A (ko) 2012-10-22
CA2786744A1 (en) 2011-07-28
KR101782186B1 (ko) 2017-09-26
BR112012017631B1 (pt) 2018-10-09
MX2012008452A (es) 2012-08-15
CN102712573A (zh) 2012-10-03
JP2013518047A (ja) 2013-05-20
US20110178327A1 (en) 2011-07-21
EP2526083B1 (en) 2016-03-23
WO2011091197A2 (en) 2011-07-28
JP5916629B2 (ja) 2016-05-11
BR112012017631A2 (pt) 2016-03-29
EP2526083A2 (en) 2012-11-28
EP2526083A4 (en) 2013-12-25

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