ES2184211T3 - Procedimiento de fabricacion de esteres de cuerpos grasos. - Google Patents

Procedimiento de fabricacion de esteres de cuerpos grasos.

Info

Publication number
ES2184211T3
ES2184211T3 ES98403164T ES98403164T ES2184211T3 ES 2184211 T3 ES2184211 T3 ES 2184211T3 ES 98403164 T ES98403164 T ES 98403164T ES 98403164 T ES98403164 T ES 98403164T ES 2184211 T3 ES2184211 T3 ES 2184211T3
Authority
ES
Spain
Prior art keywords
stage
esteres
oil
monoalcohol
glycerine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES98403164T
Other languages
English (en)
Inventor
Robert Stern
Gerard Hillion
Jean-Jacques Rouxel
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IFP Energies Nouvelles IFPEN
Original Assignee
IFP Energies Nouvelles IFPEN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Application granted granted Critical
Publication of ES2184211T3 publication Critical patent/ES2184211T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Fats And Perfumes (AREA)

Abstract

PARA PRODUCIR SIMULTANEAMENTE UNA COMPOSICION DE ESTERES DE ACIDOS MONOCARBOXILICOS LINEALES DE ENTRE 6 Y 26 ATOMOS DE CARBONO Y GLICERINA CON ALTOS GRADOS DE PUREZA, SE REALIZA: UNA ETAPA (A), EN LA QUE SE HACE REACCIONAR UN ACEITE VEGETAL O ANIMAL, ACIDO O NO, CON UN EXCESO DE AL MENOS UN MONOALCOHOL ALIFATICO DE ENTRE 1 Y 4 ATOMOS DE CARBONO, EN PRESENCIA DE UN CATALIZADOR HETEROGENEO, CON ELIMINACION DEL MONOALCOHOL SOBRANTE Y SEPARACION DE LA GLICERINA, PRODUCIENDO ESTA ETAPA UN ESTER BRUTO QUE CONTIENE MONOGLICERIDOS RESIDUALES; - UNA ETAPA (B), EN LA QUE SE SOMETE EL ESTER BRUTO ASI OBTENIDO A UNA REACCION DE, TRANSESTERIFICACION O DE ESTERIFICACION DE LOS MONOGLICERIDOS RESIDUALES EN DI- Y TRIGLICERIDOS, EN PRESENCIA DE UN CATALIZADOR HETEROGENO Y - UNA ETAPA (C) EN LA QUE SE PROCEDE A UNA EVAPORACION A PRESION REDUCIDA DE LA COMPOSICION DE ESTERES, CON RECICLADO DEL RESIDUO DE EVAPORACION HACIA EL ACEITE DE SALIDA DE LA ETAPA (A). LAS COMPOSICIONES DE ESTERES OBTENIDAS, QUE PRESENTAN UNA PUREZA ELEVADA, PUEDEN UTILIZARSE PARTICULARMENTE COMO SUSTITUTOS DEL GASOLEO.
ES98403164T 1997-12-18 1998-12-15 Procedimiento de fabricacion de esteres de cuerpos grasos. Expired - Lifetime ES2184211T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9716293A FR2772756B1 (fr) 1997-12-18 1997-12-18 Procede de fabrication d'esters de corps gras et les esters de haute purete obtenus

Publications (1)

Publication Number Publication Date
ES2184211T3 true ES2184211T3 (es) 2003-04-01

Family

ID=9514951

Family Applications (1)

Application Number Title Priority Date Filing Date
ES98403164T Expired - Lifetime ES2184211T3 (es) 1997-12-18 1998-12-15 Procedimiento de fabricacion de esteres de cuerpos grasos.

Country Status (7)

Country Link
US (1) US6147196A (es)
EP (1) EP0924185B1 (es)
AR (1) AR017876A1 (es)
AT (1) ATE224352T1 (es)
DE (1) DE69808029T2 (es)
ES (1) ES2184211T3 (es)
FR (1) FR2772756B1 (es)

Families Citing this family (43)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2838433B1 (fr) * 2002-04-11 2005-08-19 Inst Francais Du Petrole Procede de production d'esters alkyliques a partir d'une huile vegetale ou animale et d'un monoalcool aliphatique
US7157401B2 (en) * 2002-10-17 2007-01-02 Carnegie Mellon University Catalyst for the treatment of organic compounds
US20040074760A1 (en) * 2002-10-17 2004-04-22 Carnegie Mellon University Production of biofuels
US7387712B2 (en) * 2002-10-17 2008-06-17 Carnegie Mellon University Catalytic process for the treatment of organic compounds
FR2852602B1 (fr) 2003-03-17 2007-08-10 Inst Francais Du Petrole Procede d'alcoolyse d'huiles acides d'origine vegetale ou animale
FR2855517B1 (fr) * 2003-05-26 2007-04-20 Inst Francais Du Petrole Procede de transesterification d'huiles vegetales ou animales au moyen de catalyseurs heterogenes a base de titane et d'aluminium
KR20060069424A (ko) * 2003-07-10 2006-06-21 아크조 노벨 엔.브이. 정제된 지방산을 제조하는 방법
FR2869612B1 (fr) * 2004-05-03 2008-02-01 Inst Francais Du Petrole Procede de transesterification d'huiles vegetales ou animales au moyen de catalyseurs heterogenes a base de zinc, de titane et d'aluminium
FR2869613B1 (fr) * 2004-05-03 2008-08-29 Inst Francais Du Petrole Procede de transesterification d'huiles vegetales ou animales au moyen de catalyseurs heterogenes a base de bismuth, de titane et d'aluminium
EP1593732A1 (fr) * 2004-05-03 2005-11-09 Institut Français du Pétrole Procede de transesterification d'huiles vegezales ou animales au moyen de catalyseurs heterogenes a base de zinc ou de bismuth de titane et d'aluminium
US20050274065A1 (en) * 2004-06-15 2005-12-15 Carnegie Mellon University Methods for producing biodiesel
GB0416256D0 (en) * 2004-07-20 2004-08-25 Avecia Ltd Manufacturing process
CA2596105A1 (en) * 2005-02-21 2006-08-24 Nippon Shokubai Co., Ltd. Method for producing fatty acid alkyl esters and/or glycerin
AT502218B1 (de) 2005-07-25 2010-09-15 Bdi Biodiesel Internat Ag Verfahren zur herstellung von carbonsäurealkylestern
FR2890656B1 (fr) * 2005-09-14 2010-12-24 Inst Francais Du Petrole Procede de fabrication d'esters a partir de triglycerides et d'alcools
US7795460B2 (en) * 2006-05-05 2010-09-14 Tda Research, Inc. Method of making alkyl esters
US20070260078A1 (en) * 2006-05-05 2007-11-08 Bhat Ramanath N Integrated process for the manufacture of biodiesel
KR100725335B1 (ko) 2006-07-20 2007-06-07 (주)퓨렉스에너지 고순도 메틸에스테르의 정제방법
US7767837B2 (en) * 2007-05-04 2010-08-03 Tda Research, Inc. Methods of making alkyl esters
BRPI0702373A2 (pt) * 2007-05-30 2009-01-20 Petroleo Brasileiro Sa processo para produÇço de biodiesel a partir de àleos vegetais e gorduras utilizando catalisadores heterogÊneos
US8070836B2 (en) * 2007-10-16 2011-12-06 Wayne State University Combined homogeneous and heterogeneous catalytic transesterification process for biodiesel production
US8110698B2 (en) * 2008-02-11 2012-02-07 Shell Oil Company Process for producing diphenyl carbonate
US7851645B2 (en) 2008-02-11 2010-12-14 Catalytic Distillation Technologies Process for continuous production of organic carbonates or organic carbamates and solid catalysts therefore
US8975426B2 (en) 2008-05-19 2015-03-10 Wayne State University ZnO nanoparticle catalysts for use in transesterification and esterification reactions and method of making
WO2009143159A1 (en) * 2008-05-19 2009-11-26 Wayne State University Methods and catalysts for making biodiesel from the transesterification and esterification of unrefined oils
US8895764B2 (en) * 2008-05-19 2014-11-25 Wayne State University ZnO nanoparticle catalysts for use in biodiesel production and method of making
CA2729116C (en) * 2008-06-25 2017-01-24 Benefuel Inc. Process of manufacturing of fatty acid alkyl esters
EP3572395A1 (en) 2008-06-25 2019-11-27 Benefuel Inc. Process of manufacturing of fatty acid alkyl esters
EP2154226A1 (en) 2008-07-22 2010-02-17 Yellow Diesel B.V. Process for manufacturing acid esters through reactive distillation
EP2153893A1 (en) 2008-07-22 2010-02-17 Yellow Diesel B.V. Sulfated zirconia catalyst; its production by melting the precursors and its use for esterification of fatty acids with alcohols.
CA2770524A1 (en) 2008-08-21 2010-02-25 Sbi Fine Chemicals Inc. Solid, heterogeneous catalysts and methods of use
DE102008060902A1 (de) 2008-12-09 2010-06-10 Grace Gmbh & Co. Kg Verfahren zur Herstellung von Biodiesel
DE102009006777A1 (de) 2009-01-30 2010-08-05 Wolfgang F. Prof. Dr. Hölderich Verfahren zur Herstellung von Fettsäureestern und Glycerin durch Umesterung von pflanzlichen und tierischen Fetten und Ölen
FR2953831B1 (fr) * 2009-12-16 2012-03-09 Inst Francais Du Petrole Procede de production d'esters alkyliques a partir d'huile vegetale ou animale et d'un monoalcool aliphatique avec purification a chaud en lit fixe.
US8962873B2 (en) 2011-03-09 2015-02-24 Benefuel, Inc. Systems and methods for making bioproducts
WO2012135728A1 (en) 2011-03-30 2012-10-04 University Of Louisville Research Foundation, Inc. Catalytic isomerisation of linear olefinic hydrocarbons
GB201119871D0 (en) 2011-11-17 2011-12-28 Davy Process Techn Ltd Process
GB201218078D0 (en) 2012-10-09 2012-11-21 Davy Process Techn Ltd Process
US9328054B1 (en) 2013-09-27 2016-05-03 Travis Danner Method of alcoholisis of fatty acids and fatty acid gyicerides
FR3053335B1 (fr) 2016-07-01 2019-07-05 Easyl Procede de production d'esters d'acides gras et de glycerol a basse temperature
EP3837050A4 (en) 2018-08-17 2022-05-18 SBI Fine Chemicals Inc. PROCESS FOR THE PRODUCTION OF CARBONATE ESTER
BR102021012721A2 (pt) 2021-06-25 2022-12-27 Petróleo Brasileiro S.A. - Petrobras Processo de obtenção de catalisador, catalisador e processo de pré-tratamento de cargas ácidas
BR102021016123A2 (pt) 2021-08-16 2023-02-23 Petróleo Brasileiro S.A. - Petrobras Processo para produção de biodiesel a partir de cargas ácidas

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB795573A (en) * 1955-05-10 1958-05-28 Belge Produits Chimiques Sa An improved process for the preparation of higher aliphatic alcohols
DK0391485T3 (da) * 1989-04-05 1994-04-11 Unilever Plc Fremgangsmåde til fremstilling af lavere alkyl-fedtsyremonoestere
FR2752242B1 (fr) * 1996-08-08 1998-10-16 Inst Francais Du Petrole Procede de fabrication d'esters a partir d'huiles vegetales ou animales et d'alcools

Also Published As

Publication number Publication date
EP0924185A1 (fr) 1999-06-23
EP0924185B1 (fr) 2002-09-18
FR2772756A1 (fr) 1999-06-25
DE69808029D1 (de) 2002-10-24
FR2772756B1 (fr) 2000-02-11
ATE224352T1 (de) 2002-10-15
US6147196A (en) 2000-11-14
AR017876A1 (es) 2001-10-24
DE69808029T2 (de) 2003-02-06

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