ES2131356T3 - Procedimiento para la obtencion de 3-aminometil-3,5,5-trimetilciclohexilamina. - Google Patents

Procedimiento para la obtencion de 3-aminometil-3,5,5-trimetilciclohexilamina.

Info

Publication number
ES2131356T3
ES2131356T3 ES96102839T ES96102839T ES2131356T3 ES 2131356 T3 ES2131356 T3 ES 2131356T3 ES 96102839 T ES96102839 T ES 96102839T ES 96102839 T ES96102839 T ES 96102839T ES 2131356 T3 ES2131356 T3 ES 2131356T3
Authority
ES
Spain
Prior art keywords
place
aminometil
procedure
obtaining
trimetilciclohexilamina
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES96102839T
Other languages
English (en)
Inventor
Guido Dr Voit
Tom Dr Witzel
Boris Dr Breitscheidel
Wolfgang Dr Harder
Hermann Luyken
Axel Dr Paul
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Application granted granted Critical
Publication of ES2131356T3 publication Critical patent/ES2131356T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
    • C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

PROCEDIMIENTO PARA LA OBTENCION DE 3-AMINOMETIL-3,5,5TRIMETILCICLOHEXILAMINA A PARTIR DE 3-CIANO-3,5,5-TRIMETILCICLOHEXANONA, REALIZANDOSE EN TRES LUGARES SEPARADOS A) EN UN PRIMER LUGAR SE HACE REACCIONAR LA 3-CIANO-3,5,5TRIMETIL-CICLOHEXANONA CON MUCHO AMONIACO CON CATALIZADORES ACIDOS DE OXIDOS METALICOS, A TEMPERATURAS DE 20 A 150 S, B) LOS PRODUCTOS OBTENIDOS SE HIDROGENAN CON HIDROGENO EN UN SEGUNDO LUGAR, TAMBIEN EN PRESENCIA DE MUCHO AMONIACO CON CATALIZADORES DE HIDROGENACION, OPCIONALMENTE CON COMPONENTES BASICOS SOBRE PORTADORES NEUTROS O BASICOS, A TEMPERATURAS DE 50 A 100 ENIDOS SE LLEVAN A UN TERCER LUGAR, DONDE SE HIDROGENAN CON HIDROGENO, CON CATALIZADORES DE HIDROGENACION, OPCIONALMENTE CON COMPONENTES BASICOS O SOBRE PORTADORES NEUTROS O BASICOS A TEMPERATURAS DE 110 A 160
ES96102839T 1995-03-03 1996-02-26 Procedimiento para la obtencion de 3-aminometil-3,5,5-trimetilciclohexilamina. Expired - Lifetime ES2131356T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19507398A DE19507398C1 (de) 1995-03-03 1995-03-03 Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin

Publications (1)

Publication Number Publication Date
ES2131356T3 true ES2131356T3 (es) 1999-07-16

Family

ID=7755507

Family Applications (1)

Application Number Title Priority Date Filing Date
ES96102839T Expired - Lifetime ES2131356T3 (es) 1995-03-03 1996-02-26 Procedimiento para la obtencion de 3-aminometil-3,5,5-trimetilciclohexilamina.

Country Status (6)

Country Link
US (1) US5756845A (es)
EP (1) EP0729937B1 (es)
JP (1) JP4170403B2 (es)
CA (1) CA2170555C (es)
DE (2) DE19507398C1 (es)
ES (1) ES2131356T3 (es)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19747913C1 (de) * 1997-10-30 1999-02-11 Degussa Verfahren zur Herstellung primärer und/oder sekundärer Amine aus Iminen oder Nitrilen, insbesondere zur Herstellung von 3-Aminomethyl-3,5,5-trimethyl-cyclohexylamin (Isophorondiamin) aus 3-Cyano-3,5,5-trimethylcyclohexanimin (Isophoronnitril-imin) durch Hydrierung in Gegenwart eines quaternären Ammoniumhydroxids
DE19756400A1 (de) * 1997-12-18 1999-06-24 Basf Ag Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethyl-cyclohexylamin mit einem cic/trans-Isomerenverhältnis von mindestens 70/30
DE10142635A1 (de) * 2001-08-31 2003-03-20 Basf Ag Verfahren zur Herstellung von Isophorondiamin (IPDA, 3-Aminomethyl-3,5,5,-trimethylcyclohexylamin)
DE10236675A1 (de) * 2002-08-09 2004-02-19 Basf Ag Verfahren zur Herstellung von Isophorondiamin(IPDA, 3-Aminomethyl-3,5,5-trimethylcyclohexylamin) mit einem hohen cis/trans-Isomerenverhältnis
DE10236674A1 (de) 2002-08-09 2004-02-19 Basf Ag Destillative Verfahren zur Herstellung von IPDA mit einem hohen cis/trans-Isomerenverhältnis
WO2008077852A1 (de) * 2006-12-22 2008-07-03 Basf Se Kontinuierliches verfahren zur hydrierung von 3-cyano-3,5,5-trimethyl-cyclohexylimin
US9024072B2 (en) 2009-07-31 2015-05-05 Dow Global Technologies Llc Process for reductive amination of aliphatic cyanoaldehydes to aliphatic diamines
CN102471231B (zh) 2009-07-31 2015-01-07 陶氏环球技术有限责任公司 脂环族二胺及其制备方法
DE102010062603A1 (de) 2010-12-08 2012-06-14 Evonik Degussa Gmbh Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin
DE102010062594B4 (de) 2010-12-08 2022-02-17 Evonik Operations Gmbh Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin
CN102924291B (zh) * 2011-08-08 2014-08-06 万华化学集团股份有限公司 3-氨甲基-3,5,5-三甲基环己胺的制备方法
RU2616616C2 (ru) 2012-12-07 2017-04-18 Ваньхуа Кемикал Груп Ко., Лтд. Способ получения 3-аминометил-3,5,5-триметилциклогексиламина
CN104230721B (zh) * 2013-06-05 2016-05-18 万华化学集团股份有限公司 3-氨甲基-3,5,5-三甲基环己胺的制备方法
EP3186221B1 (de) * 2014-08-28 2022-02-23 Basf Se Verfahren zur herstellung von primären aminen unter verwendung eines kobalt-vollkontaktkatalysators
CN108017547B (zh) * 2017-12-22 2019-07-02 浙江新和成股份有限公司 一种异佛尔酮腈亚胺加氢还原制备异佛尔酮二胺的方法
EP4294787A1 (en) 2021-02-16 2023-12-27 Basf Se Method for manufacture of isophoronediamine
CN117425640A (zh) 2021-06-02 2024-01-19 巴斯夫欧洲公司 制造异佛尔酮二胺的方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4010227A1 (de) * 1990-03-30 1991-10-02 Basf Ag Verfahren zur herstellung von 3-aminomethyl-3,5,5-trimethyl-cyclohexylamin
DE4106882C2 (de) * 1991-03-05 1994-02-03 Degussa Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethyl-cyclohexylamin durch reduktive Aminierung von 1,3,3-Trimethyl-5-oxocyclohexan-carbonitril
US5286906A (en) * 1991-09-25 1994-02-15 Mitsubishi Kasei Corporation Process for the preparation of 3-aminomethyl-3,5,5-trialkylcyclohexylamine
DE4325847A1 (de) * 1993-07-31 1995-02-02 Basf Ag Kobaltkatalysatoren
DE4343891A1 (de) * 1993-12-22 1995-06-29 Degussa Verfahren zur Beeinflussung des cis-/trans-Isomerenverhältnisses von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin bei dessen Herstellung aus 3-Cyano-3,5,5-trimethylcyclohexanon

Also Published As

Publication number Publication date
JPH08253444A (ja) 1996-10-01
DE19507398C1 (de) 1996-09-12
US5756845A (en) 1998-05-26
EP0729937A1 (de) 1996-09-04
CA2170555A1 (en) 1996-09-04
JP4170403B2 (ja) 2008-10-22
CA2170555C (en) 2006-06-27
EP0729937B1 (de) 1999-04-28
DE59601745D1 (de) 1999-06-02

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