ES2099711T3 - Procedimiento y aparato para realizar a temperaturas variables una espectroscopia de resonancia magnetica en estado solido. - Google Patents

Procedimiento y aparato para realizar a temperaturas variables una espectroscopia de resonancia magnetica en estado solido.

Info

Publication number
ES2099711T3
ES2099711T3 ES90906620T ES90906620T ES2099711T3 ES 2099711 T3 ES2099711 T3 ES 2099711T3 ES 90906620 T ES90906620 T ES 90906620T ES 90906620 T ES90906620 T ES 90906620T ES 2099711 T3 ES2099711 T3 ES 2099711T3
Authority
ES
Spain
Prior art keywords
sample
temperature
magnetic resonance
spectroscopy
procedure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES90906620T
Other languages
English (en)
Inventor
Victor J Bartuska
David H Lewis
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Otsuka Electronics USA Inc
Original Assignee
Otsuka Electronics USA Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Otsuka Electronics USA Inc filed Critical Otsuka Electronics USA Inc
Application granted granted Critical
Publication of ES2099711T3 publication Critical patent/ES2099711T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00—Arrangements or instruments for measuring magnetic variables
    • G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
    • G01R33/28—Details of apparatus provided for in groups G01R33/44 - G01R33/64
    • G01R33/30—Sample handling arrangements, e.g. sample cells, spinning mechanisms
    • G01R33/31—Temperature control thereof

Landscapes

  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Magnetic Resonance Imaging Apparatus (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)

Abstract

TECNICA Y DISEÑO PARA UN ESPECTROSCOPIO DE RESONANCIA MAGNETICA Y TEMPERATURA VARIABLE. LOS DISEÑOS QUE UTILIZAN UN GAS SEPARADO PARA EL CONTROL DE LA TEMPERATURA DE MUESTRA CONFINAN LOS GRADIENTES DE TEMPERATURA FUERA DE LA MUESTRA. LOS CIERRES ANULARES AISLAN UNA CAMARA DE GAS DE MUESTRA A LO LARGO DE UN ROTOR Y EVITA LA MEZCLA DE GAS Y OTROS EFECTOS DE TEMPERATURA EN LA MUESTRA. SE CONSIGUE UNA RESOLUCION MEJORADA EVITANDO LOS GRADIENTES DE TEMPERATURA Y LA INDEPENDENCIA DE LA VELOCIDAD DE ROTACION DESDE LA TEMPERATURA DE MUESTRA.
ES90906620T 1989-04-14 1990-04-12 Procedimiento y aparato para realizar a temperaturas variables una espectroscopia de resonancia magnetica en estado solido. Expired - Lifetime ES2099711T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US07/339,053 US4940942A (en) 1989-04-14 1989-04-14 Method and apparatus for conducting variable-temperature solid state magnetic resonance spectroscopy

Publications (1)

Publication Number Publication Date
ES2099711T3 true ES2099711T3 (es) 1997-06-01

Family

ID=23327284

Family Applications (1)

Application Number Title Priority Date Filing Date
ES90906620T Expired - Lifetime ES2099711T3 (es) 1989-04-14 1990-04-12 Procedimiento y aparato para realizar a temperaturas variables una espectroscopia de resonancia magnetica en estado solido.

Country Status (9)

Country Link
US (1) US4940942A (es)
EP (1) EP0467963B1 (es)
JP (1) JPH087168B2 (es)
AT (1) ATE148235T1 (es)
AU (1) AU5439090A (es)
DE (1) DE69029800T2 (es)
DK (1) DK0467963T3 (es)
ES (1) ES2099711T3 (es)
WO (1) WO1990013046A1 (es)

Families Citing this family (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2662253B1 (fr) * 1990-05-15 1994-04-29 Sadis Bruker Spectrospin Ensemble de conditionnement de l'echantillon pour mesures de resonance magnetique nucleaire a hautes temperatures.
DE4018734A1 (de) * 1990-06-12 1991-12-19 Spectrospin Ag Probentemperiervorrichtung
US5122746A (en) * 1990-06-12 1992-06-16 Gas Research Institute Hydrocarbon gas measurements using nuclear magnetic resonance
US5202633A (en) * 1990-11-01 1993-04-13 Doty Scientific, Inc. High temperature nmr sample spinner
US5260657A (en) * 1992-03-26 1993-11-09 Otsuka Electronics (U.S.A.) Inc. Magnetic resonance spectroscopy sample spinning apparatus with mechanical bearing
US5289130A (en) * 1992-07-31 1994-02-22 Doty Scientific Inc. NMR sample rotor cooling technique
US5408181A (en) * 1993-08-30 1995-04-18 Auburn International, Inc. NMR system for measuring polymer properties
US6064398A (en) * 1993-09-10 2000-05-16 Geovector Corporation Electro-optic vision systems
AU7722194A (en) * 1993-09-23 1995-04-10 Auburn International, Inc. Nmr on-line viscometer for liquids or polymer melts
US6804726B1 (en) * 1996-05-22 2004-10-12 Geovector Corporation Method and apparatus for controlling electrical devices in response to sensed conditions
WO1998030917A1 (en) 1996-12-23 1998-07-16 Doty Scientific, Inc. Thermal buffering of cross-coils in high-power nmr decoupling
US6054857A (en) * 1997-03-18 2000-04-25 Doty Scientific, Inc. NMR MAS sealing sample cells and methods
US7075303B2 (en) * 2003-07-30 2006-07-11 Syracuse University Polymeric NMR sample tubes and method for using
US7170292B2 (en) * 2004-10-20 2007-01-30 Doty Scientific, Inc. NMR MAS inflow bernoulli bearing
US7151374B2 (en) * 2005-01-12 2006-12-19 Doty Scientific, Inc. NMR MAS probe with cryogenically cooled critical circuit components
US7282919B2 (en) * 2005-02-10 2007-10-16 Doty Scientific, Inc. NMR CryoMAS probe for high-field wide-bore magnets
WO2007003218A1 (en) * 2005-07-05 2007-01-11 Commissariat A L'energie Atomique Apparatus for high-resolution nmr spectroscopy and/or imaging with an improved filling factor and rf field amplitude
CA2672798A1 (en) * 2006-12-08 2008-06-12 Doty Scientific, Inc. Improved nmr cryomas probe for high-field wide-bore magnets
US7541807B2 (en) * 2007-07-19 2009-06-02 Varian, Inc. Rotor drive apparatus and methods utilizing center-fed radial-outflow gas
CA2851252C (en) * 2011-10-04 2021-02-23 Pressure Biosciences, Inc. High pressure sample containment system for electromagnetic measurements
JP6019515B2 (ja) * 2012-05-15 2016-11-02 日本電子株式会社 Ｎｍｒ用試料管およびｎｍｒ装置
JP5953633B2 (ja) * 2012-10-09 2016-07-20 日本電子株式会社 Ｎｍｒ測定用スピナ
US9062904B2 (en) 2012-10-23 2015-06-23 Doty Scientific, Inc. Stabilizing control of a saturated cold gas stream
FR3000553B1 (fr) * 2012-12-27 2016-02-19 Commissariat Energie Atomique Sonde, dispositif et procede d'analyse par resonnance magnetique nucleaire
FR3000554B1 (fr) 2012-12-27 2015-03-13 Commissariat Energie Atomique Dispositif d'analyse par resonance magnetique
JP6622081B2 (ja) * 2015-12-21 2019-12-18 日本電子株式会社 核磁気共鳴測定装置及び排ガス処理方法
JP6549980B2 (ja) * 2015-12-22 2019-07-24 日本電子株式会社 Ｎｍｒ測定用スピナ装置
DE102016218772A1 (de) 2016-09-28 2018-03-29 Bruker Biospin Gmbh Verbesserte Temperierung eines NMR-MAS-Rotors
DE102017220707B4 (de) 2017-11-20 2019-05-29 Bruker Biospin Ag MAS-NMR-Probenkopfanordnung mit auswechselbarem Stator
DE102017220709B4 (de) 2017-11-20 2019-05-29 Bruker Biospin Ag MAS-NMR-Rotorsystem mit verbesserter Raumnutzung
DE102019202001B3 (de) * 2019-02-14 2020-06-25 Bruker Biospin Gmbh MAS-Probenkopf mit thermisch isolierter Probenkammer
JP2024068324A (ja) * 2022-11-08 2024-05-20 日本電子株式会社 Ｍａｓ装置

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS52116285A (en) * 1976-03-26 1977-09-29 Hitachi Ltd Nuclear magnetic resonator probe
US4088944A (en) * 1976-10-04 1978-05-09 Varian Associates, Inc. NMR Spectrometer employing self centering turbine
SU765724A1 (ru) * 1977-06-03 1980-09-23 Институт Кибернетики Ан Эстонской Сср Датчик сигналов дерного магнитного резонанса
US4266194A (en) * 1979-07-23 1981-05-05 Varian Associates, Inc. Sensor for VT probes
US4301410A (en) * 1979-09-28 1981-11-17 International Business Machines Corporation Spin imaging in solids using synchronously rotating field gradients and samples
JPS5712463A (en) * 1980-06-25 1982-01-22 Nippon Gakki Seizo Kk Tape reproducing device
US4306878A (en) * 1980-08-29 1981-12-22 Brown Charles E Method of selecting flame retardants for polymers
US4456882A (en) * 1982-01-04 1984-06-26 University Of South Carolina High speed cylindrical nuclear magnetic resonance (NMR) sample spinner
US4511841A (en) * 1982-06-17 1985-04-16 Chemagnetics, Inc. Method and apparatus for high speed magic angle spinning
US4510450A (en) * 1982-09-28 1985-04-09 The Medical College Of Wisconsin, Inc. Apparatus and assay method for the quantitative determination of mineral content in bone
US4587492A (en) * 1984-03-02 1986-05-06 Varian Associates, Inc. Thermal barrier for variable temperature NMR

Also Published As

Publication number Publication date
US4940942A (en) 1990-07-10
WO1990013046A1 (en) 1990-11-01
EP0467963B1 (en) 1997-01-22
DE69029800D1 (de) 1997-03-06
DE69029800T2 (de) 1997-06-05
AU5439090A (en) 1990-11-16
ATE148235T1 (de) 1997-02-15
JPH087168B2 (ja) 1996-01-29
DK0467963T3 (da) 1997-02-10
EP0467963A1 (en) 1992-01-29
JPH04504308A (ja) 1992-07-30

Similar Documents

Publication Publication Date Title
ES2099711T3 (es) Procedimiento y aparato para realizar a temperaturas variables una espectroscopia de resonancia magnetica en estado solido.
ES535550A0 (es) Aparato para deposicion quimica de vapor
ES8204498A1 (es) Procedimiento y aparato para rellenar con grava por los me- nos una zona perforada por un pozo de sondeo
ES8306519A1 (es) Procedimiento y aparato para rellenar con grava una zona traspasada por un pozo de sondeo
SE407264B (sv) Forfarande och apparat for reducering av de skadliga bestandsdelarna i avgaserna fran forbrenningsmotorer
IE781959L (en) Temperature sensing apparatus
GB1509693A (en) Immersion sampler for molten metal
EP0305863A3 (en) Temperature testing device provided with sample-receiving chamber from which a specimen is easily detachable and in which temperature is controllable
AU7952382A (en) Probe for taking gas samples and thermal measurements in a shaft furnace
JPS5697734A (en) Combustion chamber for gas turbine and its operation method
NO165987C (no) Fremgangsmaate for maling av faste partikler i en sentrifugalmoelle, og sentrifugalmoelle for utfoerelse av fremgangsmaaten.
FR2614322B1 (fr) Four a gradient destine a la solidification orientee, notamment par la methode de bridgmann.
ES2079993B1 (es) Procedimiento y aparato de desorcion termica programada.
KR900010004A (ko) 샤프트 노용 장입 로크의 플로우-오프 오리피스를 시일링하기 위한 장치
JPS6410209A (en) Polygon mirror
NO905578D0 (no) Fremgangsmaate og innretning til fremstilling av enbasiskedrivladningskrutt med alkohol og eter som opploesningsmiddel.
SU649877A1 (ru) Тепловой двигатель шпади
JPS54133404A (en) Method and apparatus for sealing rotary furnace bodies
DK164186D0 (da) Apparat til farvning af tekstilmateriale ved hoej temperatur
Crowe et al. Fluorescence and absorption spectroscopy applied in studies of certain laboratory products, isolated and purified by chromatographic and electrophoretic analyses
RU94042117A (ru) Способ определения неоднородности температурного поля газового потока за соплом при сверхкритическом истечении
Petzow Advanced Materials by Tuned Microstructures--Chances and Limits
JPS52116285A (en) Nuclear magnetic resonator probe
Gurbanyazov Magnetic and Optical Investigations of Ferromagnetic Films
DK205486D0 (da) Apparat til styring af taendingstidspunktet ved en fremmedtaendt stempelmotor

Legal Events

Date Code Title Description
FG2A Definitive protection

Ref document number: 467963

Country of ref document: ES