ES2019431B3 - Procedimiento para aislar acidos sulfonicos aromaticos de soluciones o suspensiones acuosas. - Google Patents
Procedimiento para aislar acidos sulfonicos aromaticos de soluciones o suspensiones acuosas.Info
- Publication number
- ES2019431B3 ES2019431B3 ES88108361T ES88108361T ES2019431B3 ES 2019431 B3 ES2019431 B3 ES 2019431B3 ES 88108361 T ES88108361 T ES 88108361T ES 88108361 T ES88108361 T ES 88108361T ES 2019431 B3 ES2019431 B3 ES 2019431B3
- Authority
- ES
- Spain
- Prior art keywords
- sulphonic acids
- aromatic sulphonic
- suspensions
- procedure
- aqueous solutions
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/42—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D213/84—Nitriles
- C07D213/85—Nitriles in position 3
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pyridine Compounds (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
PROCESO PARA EL AISLAMIENTO DE ACIDOS SULFONICOS AROMATICOS EN FORMA DE ACIDO LIBRE O DE SAL ALCALINA, DE UNA SOLUCION O DISPERSION ACUOSA EXTRAYENDO DICHA SOLUCION O SUSPENSION CON UN DISOLVENTE ORGANICO, NO MISCIBLE O POCO MISCIBLE, CON AGUA, PERTENECIENTE AL GRUPO DE LOS ALCOHOLES, CETONAS O ESTERES CARBOXILICOS. A CONTINUACION SE SEPARA LA FASE ORGANICA, O EN SU CASO, SE CONVIERTEN LOS ACIDOS SULFONICOS AROMATICOS EN SUS SALES ALCALINAS Y SE SEPARA EL DISOLVENTE ORGANICO.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19873718314 DE3718314A1 (de) | 1987-06-01 | 1987-06-01 | Verfahren zur isolierung von aromatischen sulfonsaeuren aus waessriger loesung oder suspension |
Publications (2)
Publication Number | Publication Date |
---|---|
ES2019431B3 true ES2019431B3 (es) | 1991-06-16 |
ES2019431T5 ES2019431T5 (es) | 1996-05-16 |
Family
ID=6328801
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES88108361T Expired - Lifetime ES2019431T5 (es) | 1987-06-01 | 1988-05-26 | Procedimiento para el aislamiento de acidos sulfonicos aromaticos a partir de soluciones o suspensiones acuosas. |
Country Status (4)
Country | Link |
---|---|
EP (1) | EP0293744B2 (es) |
JP (1) | JP2515375B2 (es) |
DE (2) | DE3718314A1 (es) |
ES (1) | ES2019431T5 (es) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4006225A1 (de) * | 1990-02-28 | 1991-08-29 | Basf Ag | Verfahren zur herstellung von na-salz der diethylmetanilsaeure |
DE4006226A1 (de) * | 1990-02-28 | 1991-08-29 | Basf Ag | Verfahren zur herstellung von na-salz der diethylmetanilsaeure |
FR2727410B1 (fr) * | 1994-11-25 | 1996-12-20 | Synthelabo | Chlorures de sulfonyles, leur preparation et leur utilisation comme intermediaires de synthese |
JP2007521328A (ja) * | 2003-11-20 | 2007-08-02 | ワーナー−ランバート カンパニー リミテッド ライアビリティー カンパニー | アンドロゲン受容体モジュレーター |
CN102617411A (zh) * | 2012-03-14 | 2012-08-01 | 宜兴市中正化工有限公司 | N-乙基-n(3'-磺酸基)苄基苯胺的合成方法 |
CN105348150B (zh) * | 2015-09-25 | 2017-07-11 | 恒升化工有限公司 | N‑乙基‑n‑(3ˊ‑磺酸)苄基苯胺的清洁生产工艺 |
CN111170896A (zh) * | 2019-12-31 | 2020-05-19 | 恒升化工有限公司 | 一种n-乙基-n-(3ˊ-磺酸)苄基苯胺的制备方法 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1668048A1 (de) * | 1967-12-01 | 1971-04-22 | Hoechst Ag | Verfahren zur Reinigung von Olefinsulfonaten |
IT941650B (it) * | 1970-08-07 | 1973-03-10 | Aquitaine Petrole | Procedimento per la preparazione di acidi solfonici e di solfonati |
CH549625A (de) * | 1971-03-18 | 1974-05-31 | Sandoz Ag | Verfahren zum reinigen von 1-amino-1-bromanthrachinon-2-sulfonsaeure. |
US4175092A (en) * | 1976-11-30 | 1979-11-20 | Shell Oil Company | Extraction process |
DE3013808C2 (de) * | 1980-04-10 | 1982-12-23 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur Abtennung von Schwefelsäure aus dem bei der Umsetzung von Paraffinen mit Schwefeldioxid, Sauerstoff und Wasser in Gegenwart von UV-Licht anfallenden Sulfoxidationsaustrag |
-
1987
- 1987-06-01 DE DE19873718314 patent/DE3718314A1/de not_active Withdrawn
-
1988
- 1988-05-26 EP EP88108361A patent/EP0293744B2/de not_active Expired - Lifetime
- 1988-05-26 DE DE8888108361T patent/DE3861061D1/de not_active Expired - Lifetime
- 1988-05-26 ES ES88108361T patent/ES2019431T5/es not_active Expired - Lifetime
- 1988-05-27 JP JP63128552A patent/JP2515375B2/ja not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
EP0293744B1 (de) | 1990-11-14 |
DE3861061D1 (de) | 1990-12-20 |
ES2019431T5 (es) | 1996-05-16 |
JPH01156931A (ja) | 1989-06-20 |
EP0293744B2 (de) | 1996-03-27 |
DE3718314A1 (de) | 1988-12-22 |
JP2515375B2 (ja) | 1996-07-10 |
EP0293744A1 (de) | 1988-12-07 |
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