EP4268630A1 - Tabakprodukt zur erwärmung ohne verbrennung und elektrisch erhitztes tabakprodukt - Google Patents

Tabakprodukt zur erwärmung ohne verbrennung und elektrisch erhitztes tabakprodukt Download PDF

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Publication number
EP4268630A1
EP4268630A1 EP21910165.6A EP21910165A EP4268630A1 EP 4268630 A1 EP4268630 A1 EP 4268630A1 EP 21910165 A EP21910165 A EP 21910165A EP 4268630 A1 EP4268630 A1 EP 4268630A1
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EP
European Patent Office
Prior art keywords
tobacco
flavoring agent
heating
less
combustion
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
EP21910165.6A
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English (en)
French (fr)
Inventor
Hiroki NAKAAE
Tetsuya Yoshimura
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Japan Tobacco Inc
Original Assignee
Japan Tobacco Inc
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Filing date
Publication date
Application filed by Japan Tobacco Inc filed Critical Japan Tobacco Inc
Publication of EP4268630A1 publication Critical patent/EP4268630A1/de
Pending legal-status Critical Current

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Classifications

    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00—Cigars; Cigarettes
    • A24D1/20—Cigarettes specially adapted for simulated smoking devices
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/281—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed
    • A24B15/283—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed by encapsulation of the chemical substances
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00—Cigars; Cigarettes
    • A24D1/02—Cigars; Cigarettes with special covers
    • A24D1/027—Cigars; Cigarettes with special covers with ventilating means, e.g. perforations
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/40—Constructional details, e.g. connection of cartridges and battery parts
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/20—Devices using solid inhalable precursors

Definitions

  • the present disclosure relates to a non-combustion-heating-type tobacco and an electric heating tobacco product.
  • Non-combustion-heating-type tobaccos that are inserted into an electric heating device when used have been developed as an alternative to cigarettes (paper-wrapped tobaccos)(Pantet Document 1).
  • the non-combustion-heating-type tobacco commonly includes a tobacco rod formed by a shredded tobacco, a material that generates a flavor component, and the like being wrapped with a wrapping paper, a mouthpiece used for inhaling components generated from the tobacco rod by heating, and a tipping paper with which the above members are wrapped.
  • the non-combustion-heating-type tobacco is inserted into an electric heating device and, subsequently, a heater member is caused to produce heat.
  • a heater member is caused to produce heat.
  • the tobacco rod is heated from a portion of the tobacco rod which is in contact with the heater member, and the generated components are delivered to the user.
  • a flavoring agent may be added to a tobacco rod of a non-combustion-heating-type tobacco in order to impart a flavor note to mainstream smoke.
  • a solution of a flavoring agent is added to dry tobacco leaves. This method is advantageous in that a flavoring agent can be added to dry tobacco leaves in an easy and simple manner by spraying a solution of the flavoring agent to the dry tobacco leaves.
  • Pantet Document 1 Japanese Unexamined Patent Application Publication (Translation of PCT Application) No. 2015-508676
  • an object of the present invention is to provide a non-combustion-heating-type tobacco in which variations in the amount of flavoring agent delivered per puff are small from the early to late stages of smoking and an electric heating tobacco product that includes the non-combustion-heating-type tobacco.
  • the inventors of the present invention conducted extensive studies and consequently found that the above-described issues may be addressed by adding dry tobacco leaves and a flavoring agent-containing material, which includes a polysaccharide gel and a flavoring agent included in the polysaccharide gel, to a tobacco rod portion.
  • a flavoring agent-containing material which includes a polysaccharide gel and a flavoring agent included in the polysaccharide gel
  • a non-combustion-heating-type tobacco in which variations in the amount of flavoring agent delivered per puff are small from the early to late stages of smoking and an electric heating tobacco product that includes the non-combustion-heating-type tobacco can be provided.
  • a non-combustion-heating-type tobacco is a rod-shaped non-combustion-heating-type tobacco including a tobacco rod portion and a mouthpiece portion.
  • the mouthpiece portion includes a cooling segment and a filter segment including a filter element.
  • the cooling segment and the filter segment are arranged adj acent to each other.
  • the tobacco rod portion includes dry tobacco leaves (tobacco leaves that have been dried) and a flavoring agent-containing material including a polysaccharide gel and a flavoring agent included in the polysaccharide gel.
  • the non-combustion-heating-type tobacco 10 illustrated in Fig. 1 is a rod-shaped non-combustion-heating-type tobacco that includes a tobacco rod portion 11, a mouthpiece portion 14, and a tipping paper 15 wrapped around the above members.
  • the mouthpiece portion 14 includes a cooling segment 12 and a filter segment 13 including a filter element.
  • the cooling segment 12 is arranged adjacent to the tobacco rod portion 11 and the filter segment 13 and sandwiched therebetween in the axial direction (also referred to as "longitudinal direction") of the non-combustion-heating-type tobacco 10.
  • perforations V may be formed concentrically in the cooling segment 12 in the circumferential direction.
  • the perforations V formed in the cooling segment 12 of the non-combustion-heating-type tobacco 10 illustrated in Fig. 1 are usually perforations that facilitate the entry of outside air by the inhalation of the user.
  • the entry of air reduces the temperature of the components and air taken in from the tobacco rod portion 11.
  • the perforations V which may be formed in this embodiment, are present at, for example, a position 4 mm from the boundary between the cooling segment 12 and the filter segment 13 toward the cooling segment.
  • the cooling capacity with which the temperature of the components generated by heating and the air is reduced can be enhanced.
  • the retention of the above components and the air in the cooling segment can be reduced and, consequently, the amount of the components delivered can be increased.
  • Examples of the components generated by heating include a flavor component derived from a flavoring agent, nicotine and tar derived from tobacco leaves, and an aerosol component derived from an aerosol-source material.
  • aerosol-source material refers to a substrate that generates an aerosol.
  • the rod-shaped non-combustion-heating-type tobacco 10 preferably has a pillar-like shape that is a shape having an aspect ratio of 1 or more, the aspect ratio being defined as described below.
  • Aspect ratio h / w
  • w represents the width of the bottom of the pillar-shaped body (in the present specification, the width of the tobacco rod portion-side bottom)
  • h represents the height of the pillar-shaped body.
  • h ⁇ w In the present specification, the longitudinal direction is defined as the direction represented by h. Thus, even if w ⁇ h, the direction represented by h is referred to as "longitudinal direction" for the sake of simplicity.
  • the shape of the bottom may be, but not limited to, a polygonal shape, a polygonal shape having rounded corners, a circular shape, an oval shape, or the like.
  • the width w is the diameter of the circle.
  • the width w is the major-axis length of the oval.
  • the width w is the diameter of the circle circumscribing the polygon or the major-axis length of the oval circumscribing the polygon.
  • the length h of the non-combustion-heating-type tobacco 10 in the longitudinal direction is not limited.
  • the length h is, for example, usually 40 mm or more, is preferably 45 mm or more, and is more preferably 50 mm or more.
  • the length h is usually 100 mm or less, is preferably 90 mm or less, and is more preferably 80 mm or less.
  • the width w of the bottom of the pillar-shaped body of the non-combustion-heating-type tobacco 10 is not limited.
  • the width w is, for example, usually 5 mm or more and is preferably 5.5 mm or more.
  • the width w is usually 10 mm or less, is preferably 9 mm or less, and is more preferably 8 mm or less.
  • the proportions of the lengths of the cooling segment and the filter segment to the length of the non-combustion-heating-type tobacco 10 in the longitudinal direction is usually, but not limited to, 0.60 to 1.40:0.60 to 1.40, are preferably 0.80 to 1.20:0.80 to 1.20, are more preferably 0.85 to 1.15:0.85 to 1.15, are further preferably 0.90 to 1.10:0.90 to 1.10, and are particularly preferably 0.95 to 1.05:0.95 to 1.05 in consideration of the amount of the flavoring agent delivered and an adequate aerosol temperature.
  • the cooling effect, the effect of reducing loss caused due to the adhesion of the generated vapor and aerosol on the inner wall of the cooling segment, and the function of the filter to adjust the amounts of air and flavor can be all achieved in a balanced manner and a suitable flavor and a suitable intensity of the flavor can be achieved.
  • the length of the cooling segment is increased, the formation of aerosol particles and the like is increased and, consequently, a suitable flavor can be achieved.
  • the length of the cooling segment is excessively increased, the substance that passes therethrough may adhere on the inner wall.
  • the airflow resistance of the non-combustion-heating-type tobacco 10 in the longitudinal direction is not limited.
  • the above airflow resistance is usually 8 mmH 2 O or more, is preferably 10 mmH 2 O or more, and is more preferably 12 mmH 2 O or more, and is usually 100 mmH 2 O or less, is preferably 80 mmHzO or less, and is more preferably 60 mmH 2 O or less.
  • the above airflow resistance is measured in conformity with an ISO standard method (ISO6565:2015) using, for example, a filter airflow resistance gage produced by Cerulean.
  • the airflow resistance is the difference in the air pressure between one of the edge surfaces (first edge surface) of the non-combustion-heating-type tobacco 10 and the other edge surface (second edge surface) which occurs when air is passed through the non-combustion-heating-type tobacco 10 in the direction from the first to second edge surface at a predetermined air flow rate (17.5 cc/min) while the permeation of air through the side surfaces of the non-combustion-heating-type tobacco 10 is blocked.
  • the airflow resistance is commonly expressed in units of mmH 2 O.
  • the airflow resistance is proportional to the length of the non-combustion-heating-type tobacco when the length of the non-combustion-heating-type tobacco falls within a usual range (length: 5 to 200 mm); if the length of the non-combustion-heating-type tobacco doubles, the airflow resistance of the non-combustion-heating-type tobacco doubles.
  • the mouthpiece portion 14 may have any structure that includes the cooling segment 12 and the filter segment 13 including a filter element such that the cooling segment 12 is arranged adj acent to the tobacco rod portion 11 and the filter segment 13 and sandwiched therebetween in the axial direction of the non-combustion-heating-type tobacco 10. Details of the filter segment and the cooling segment are described below.
  • the filter segment 13 is not limited and may be any filter segment that includes a filter element and has common filter functions
  • a tow formed of synthetic fibers also referred to simply as "tow”
  • a material such as paper which is formed in a cylindrical shape
  • the common filter functions include a function of adjusting the amount of air that enters upon the inhalation of an aerosol or the like, a function of reducing a flavor, and a function of reducing nicotine and tar.
  • the filter segment does not necessarily have all of the above functions.
  • a function of suppressing the filtration function and preventing detachment of the tobacco filler is one of the important functions.
  • the shape of the filter segment 13 is not limited; publicly known shapes may be used.
  • the filter segment 13 usually has a cylindrical shape.
  • the filter segment 13 may have the following structure.
  • the filter segment 13 may have a section in which a cavity (e.g., center hole) is formed such that a cross section of the filter segment 13 which is taken in the circumferential direction is hollow or in which a recess or the like is formed.
  • a cavity e.g., center hole
  • the shape of cross section of the filter segment 13 which is taken in the circumferential direction is substantially circular.
  • the diameter of the circle can be changed appropriately in accordance with the size of the product.
  • the diameter of the circle is usually 4.0 mm or more and 9.0 mm or less, is preferably 4.5 mm or more and 8.5 mm or less, and is more preferably 5.0 mm or more and 8.0 mm or less.
  • the above diameter is the diameter of a virtual circle having the same area as the cross section.
  • the perimeter of the shape of a cross section of the filter segment 13 which is taken in the circumferential direction can be changed appropriately in accordance with the size of the product.
  • the above perimeter is usually 14.0 mm or more and 27.0 mm or less, is preferably 15.0 mm or more and 26.0 mm or less, and is more preferably 16.0 mm or more and 25.0 mm or less.
  • the length of the filter segment 13 in the axial direction can be changed appropriately in accordance with the size of the product.
  • the above length is usually 15 mm or more and 35 mm or less, is preferably 17.5 mm or more and 32.5 mm or less, and is more preferably 20.0 mm or more and 30.0 mm or less.
  • the shape and dimensions of the filter element can be adjusted as needed such that the shape and dimensions of the filter segment 13 fall within the respective ranges.
  • the airflow resistance of the filter segment 13 in the axial direction per length of 120 mm is not limited.
  • the above airflow resistance is usually 40 mmH 2 O or more and 300 mmH 2 O or less, is preferably 70 mmH 2 O or more and 280 mmH 2 O or less, and is more preferably 90 mmHzO or more and 260 mini IiO or less.
  • the above airflow resistance is measured in conformity with an ISO standard method (ISO6565) using, for example, a filter airflow resistance gage produced by Cerulean.
  • the airflow resistance of the filter segment 13 is the difference in the air pressure between one of the edge surfaces (first edge surface) of the filter segment 13 and the other edge surface (second edge surface) which occurs when air is passed through the filter segment 13 in the direction from the first to second edge surface at a predetermined air flow rate (17.5 cc/min) while the permeation of air through the side surfaces of the filter segment 13 is blocked.
  • the airflow resistance is commonly expressed in units of mmH 2 O.
  • the airflow resistance of the filter segment 13 is proportional to the length of the filter segment 13 when the length of the filter segment 13 falls within a usual range (length: 5 to 200 mm); if the length of the filter segment 13 doubles, the airflow resistance of the filter segment 13 doubles.
  • the filter element which constitutes the filter segment 13, may be, for example, a filter element produced by the production method described below or a commercial filter element.
  • the type of the filter segment 13 is not limited.
  • Examples of the filter segment 13 include a plain filter including a single filter element and a multi-segment filter including a plurality of filter elements, such as a dual filter or a triple filter.
  • the filter segment 13 can be produced by a publicly known method.
  • a synthetic fiber such as cellulose acetate tow
  • the filter segment 13 can be produced by spinning a polymer solution including a polymer and a solvent into thread and crimping the thread. Examples of the above method include the method described in International Publication No. 2013/067511 .
  • the adjustment of air-flow resistance and the addition of additives (publicly known adsorbent, flavoring agent (e.g., menthol), granular active carbon, and flavoring agent-holding material) to the filter element can be done appropriately.
  • additives publicly known adsorbent, flavoring agent (e.g., menthol), granular active carbon, and flavoring agent-holding material
  • the filter element constituting the filter segment 13 is not limited; publicly known filter elements may be used. Examples thereof include a filter element produced by forming cellulose acetate tow into a cylindrical shape.
  • the filament denier and total denier of the cellulose acetate tow are not limited. In the case where the mouthpiece portion has a perimeter of 22 mm, it is preferable that the filament denier be 5 g/9000 m or more and 12 g/9000 m or less and the total denier be 12000 g/9000 m or more and 35000 g/9000 m or less.
  • Examples of the cross-sectional shape of fibers of the cellulose acetate tow include circular, oval, Y-shaped, I-shaped, and R-shaped.
  • triacetin may be added to the filter in an amount that is 5% by weight or more and 10% by weight or less of the weight of the cellulose acetate tow, in order to increase the hardness of the filter.
  • a paper filter filled with sheet-like pulp paper may also be used.
  • the density of the filter element is usually, but not limited to, 0.10 g/cm 3 or more and 0.25 g/cm 3 or less, is preferably 0.11 g/cm 3 or more and 0.24 g/cm 3 or less, and is more preferably 0.12 g/cm 3 or more and 0.23 g/cm 3 or less.
  • the filter element may include, in addition to synthetic fibers such as cellulose acetate tow, a crushable additive release container (e.g., a capsule) that includes a crushable shell composed of gelatin or the like.
  • a crushable additive release container e.g., a capsule
  • the capsule also referred to as "additive release container” in the technical field
  • the capsule may be a crushable additive release container that includes a crushable shell composed of gelatin or the like.
  • the capsule when the capsule is broken before, while, or after the user uses the tobacco product, the capsule releases a liquid or substance (usually, a flavor agent) included in the capsule.
  • the liquid or substance is transferred to tobacco smoke during the use of the tobacco product and then transferred to the ambient environment after the use.
  • the form of the capsule is not limited.
  • the capsule may be, for example, an easy-to-crush capsule.
  • the shape of the capsule is preferably spherical.
  • the capsule may include the optional additives described above and particularly preferably include a flavor agent and active carbon.
  • One or more materials that assist the filtration of smoke may be used as an additive.
  • the form of the additive is usually, but not limited to, liquid or solid. Note that the use of a capsule including an additive is known in the technical field. An easy-to-crush capsule and the method for producing such a capsule are known in the technical field.
  • the filter segment 13 may further include a center hole segment having one or a plurality of hollow portions.
  • the center hole segment is usually arranged closer to the cooling segment than the filter element and is preferably arranged adjacent to the cooling segment.
  • the center hole segment is constituted by a packed layer having one or a plurality of hollow portions and an inner plug wrapper (inner filter wrapper) wrapped around the packed layer.
  • the center hole segment is constituted by a packed layer having a hollow portion and an inner plug wrapper wrapped around the packed layer.
  • the center hole segment increases the strength of the mouthpiece portion.
  • the packed layer is, for example, a rod having an inside diameter ⁇ of 1.0 mm or more and 5.0 mm or less which is filled with cellulose acetate fibers at a high density and cured with a plasticizer including triacetin, the plasticizer being added in an amount that is 6% by mass or more and 20% by mass or less of the mass of the cellulose acetate.
  • the center hole segment does not necessarily include the inner plug wrapper. In such a case, the shape of the product may be maintained by thermoforming.
  • the center hole segment and the filter element may be connected to each other with an outer plug wrapper (outer filter wrapper) or the like.
  • the outer plug wrapper can be, for example, a cylindrical paper.
  • the tobacco rod portion 11, the cooling segment 12, and the center hole segment and the filter element connected to each other may be connected to one another with, for example, a mouthpiece lining paper
  • the above connection can be achieved by, for example, applying a vinyl acetate-based paste or the like onto the inner surface of the mouthpiece lining paper, placing the tobacco rod portion 11, the cooling segment 12, and the center hole segment and the filter element connected to each other on the mouthpiece lining paper, and rolling the mouthpiece lining paper
  • the above members may be connected to one another using a plurality of lining papers in a plurality of stages.
  • the filter segment 13 may include a filter wrapper (filter plug wrapper) with which the filter element etc. described below are wrapped.
  • the filter wrapper is not limited and may include one or more seams including an adhesive.
  • the adhesive may include a hot-melt adhesive.
  • the hot-melt adhesive may include polyvinyl alcohol. In the case where the filter segment 13 is constituted by two or more segments, it is preferable that the two or more segments be collectively wrapped with the filter wrapper.
  • the material constituting the filter wrapper is not limited; publicly known materials may be used.
  • the filter wrapper may include a filler, such as calcium carbonate.
  • the thickness of the filter wrapper is usually, but not limited to, 20 ⁇ m or more and 140 ⁇ m or less, is preferably 30 ⁇ m or more and 130 ⁇ m or less, and is more preferably 30 ⁇ m or more and 120 ⁇ m or less.
  • the basis weight of the filter wrapper is usually, but not limited to, 20 gsm or more and 100 gsm or less, is preferably 22 gsm or more and 95 gsm or less, and is more preferably 23 gsm or more and 90 gsm or less.
  • the filter wrapper may be coated and is not necessarily coated. In order to impart functions other than strength or structural stiffness, it is preferable to coat the filter wrapper with an intended material.
  • the cooling segment 12 is arranged adjacent to the tobacco rod portion 11 and the filter segment 13 and sandwiched therebetween.
  • the cooling segment 12 is usually a rod-shaped member having a cavity formed therein such that a cross section taken in the circumferential direction is hollow, such as a cylinder.
  • the cooling segment 12 may have perforations V (in the technical field, also referred to as "ventilation filter (Vf)”) formed concentrically therein in the circumferential direction as illustrated in Fig. 2 . Although eight perforations V are arranged concentrically in Fig. 2 , the number of the perforations V is not limited to this.
  • the perforations V may be present at a position 2 mm or more from the boundary between the cooling segment 12 and the filter segment 13 toward the cooling segment.
  • the presence of the perforations V allows outside air to enter the inside of the cooling portion during use and thereby reduces the temperature of components and air that enter from the tobacco rod portion 11. Furthermore, arranging the cooling segment 12 at a position 4 mm or more from the boundary between the cooling segment 12 and the filter segment 13 toward the cooling segment enhances the cooling capacity and also reduces the likelihood of the components generated by heating being retained inside the cooling segment. This increases the amount of the components delivered.
  • the tobacco rod portion 11 includes an aerosol-source material
  • a vapor containing an aerosol-source material and a tobacco flavor component which are generated upon heating of the tobacco rod portion 11 comes into contact with outside air and the temperature of the vapor is reduced.
  • the vapor becomes liquefied and the generation of aerosol can be facilitated.
  • the number of the perforation groups may be one or two or more. In the case where two or more perforation groups are present, it is preferable that the perforation groups be not arranged at a position less than 4 mm from the boundary between the cooling segment 12 and the filter segment 13 toward the cooling segment in order to increase the amount of the delivered components generated by heating.
  • the non-combustion-heating-type tobacco 10 includes the tobacco rod portion 11, the cooling segment 12, the filter segment 13, and the tipping paper 15 wrapped around the above members, it is preferable that the tipping paper 15 have perforations formed therein at positions directly above the perforations V formed in the cooling segment 12.
  • wrapping may be performed using a tipping paper 15 having perforations arranged to overlap the perforations V
  • the perforations V are preferably formed such that the proportion of the air taken in through the perforations when inhalation is performed at 17.5 ml/sec with an automated smoking machine (the proportion of the volume of the air taken in though the perforations, with the amount of the air inhaled through the mouth end being 100% by volume) is 10% to 90% by volume, is preferably 50% to 80% by volume, and is more preferably 55% to 75% by volume.
  • the above condition can be satisfied by, for example, selecting the number of the perforations V per perforation group from 5 to 50, selecting the diameter of the perforations V from 0.1 to 0.5 mm, and changing the combination thereof.
  • the above air inflow proportion can be determined using an automated smoking machine (e.g., single-port automated smoking machine produced by Borgwaldt) in conformity with ISO9512.
  • an automated smoking machine e.g., single-port automated smoking machine produced by Borgwaldt
  • the position at which the perforations V are present is not limited. In order to enhance the delivery of the components generated by heating, the perforations V are preferably formed at a position 2 mm or more from the boundary between the cooling segment 12 and the filter segment 13 toward the cooling segment.
  • the above position is more preferably 3 mm or more, is further preferably 4 mm or more, is particularly preferably 5 mm or more, and is most preferably 5.5 mm or more from the above boundary.
  • the above position is preferably 15 mm or less, is more preferably 10 mm or less, and is further preferably 6 mm or less from the boundary.
  • the perforations V are preferably present at a position 22 mm or more from the mouth end of the non-combustion-heating-type tobacco toward the cooling segment.
  • the above distance is preferably 23 mm or more, is preferably 24 mm or more, is more preferably 25 mm or more, and is further preferably 25.5 mm or more.
  • the above distance is preferably 35 mm or less, is more preferably 30 mm or less, and is further preferably 26 mm or less.
  • the perforations V are preferably present at a position 2 mm or more from the boundary between the cooling segment 12 and the tobacco rod portion 11 toward the cooling segment.
  • the above distance is more preferably 5 mm or more, is further preferably 10 mm or more, and is particularly preferably 14.5 mm or more.
  • the above distance is preferably 18 mm or less, is more preferably 16 mm or less, and is further preferably 14.5 mm or less.
  • the diameter of the perforations V is preferably, but not limited to, 100 ⁇ m or more and 1000 ⁇ m or less, is more preferably 100 ⁇ m or more and 500 ⁇ m or less, and is further preferably 300 ⁇ m or more and 800 ⁇ m or less.
  • the perforations V are preferably substantially circular or substantially oval. In the case where the perforations are substantially oval, the major-axis length of the perforations is considered as diameter of the perforations.
  • the length of the cooling segment 12 in the longitudinal direction may be changed appropriately in accordance with the size of the product.
  • the above length is usually 15 mm or more, is preferably 20 mm or more, and is more preferably 25 mm or more.
  • the above length is usually 40 mm or less, is preferably 35 mm or less, and is more preferably 30 mm or less. Setting the length of the cooling segment 12 in the longitudinal direction to be equal to or more than the above lower limit enables a sufficiently high cooling effect to be maintained and allows a suitable flavor to be produced. Setting the above length to be equal to or less than the above upper limit reduces the loss of the generated vapor and aerosol which may be caused as a result of the vapor and aerosol adhering on the inner wall of the cooling segment.
  • the total surface area of the cooling segment 12 may be, for example, but not limited to, 300 mm 2 /mm or more and 1000 mm 2 /mm or less.
  • the above surface area is the surface area of the cooling segment 12 per length (mm) of the cooling segment 12 in the airflow direction.
  • the total surface area of the cooling segment 12 is preferably 400 mm 2 /mm or more and is more preferably 450 mm 2 /mm or more.
  • the above total surface area is preferably 600 mm 2 /mm or less and is more preferably 550 mm 2 /mm or less.
  • the inside structure of the cooling segment 12 may be formed of a thin sheet material that has been wrinkled in order to form channels and then pleated, gathered, or folded. The larger the number of folds or pleats per unit volume of the component, the larger the total surface area of the cooling segment.
  • the thickness of the material constituting the cooling segment 12 is, for example, 5 ⁇ m or more and 500 ⁇ m or less and may be, for example, 10 ⁇ m or more and 250 ⁇ m or less.
  • the tobacco rod portion 11 is not limited and may be any tobacco rod portion that includes dry tobacco leaves and a flavoring agent-containing material that includes a polysaccharide gel and a flavoring agent included in the polysaccharide gel.
  • the tobacco rod portion 11 usually includes a tobacco filler including dry tobacco leaves and a wrapping paper with which the tobacco filler is wrapped.
  • the tobacco filler is not limited; the first, second, and third tobacco fillers described below can be used.
  • products formed of dry tobaccos such as the shredded tobacco, tobacco sheet, tobacco granules, and the like described below, may be referred to simply as "dry tobacco leaves".
  • the tobacco rod portion 11 may have a fitting portion to which, for example, a heater member used for heating the tobacco product can be fit.
  • the tobacco rod portion 11, which includes a tobacco filler and a wrapping paper with which the tobacco filler is wrapped, preferably has a pillar-like shape.
  • the aspect ratio that is the ratio of the height of the tobacco rod portion 11 in the longitudinal direction to the width of the bottom of the tobacco rod portion 11 is preferably 1 or more.
  • the shape of the bottom may be, but not limited to, a polygonal shape, a polygonal shape having rounded corners, a circular shape, or an oval shape.
  • the above width is the diameter of the circle.
  • the width is the major-axis length of the oval.
  • the width is the diameter of the circle circumscribing the polygon or the major-axis length of the oval circumscribing the polygon.
  • the height of the tobacco filler constituting the tobacco rod portion 11 is preferably about 10 to 70 mm.
  • the width of the tobacco filler is preferably about 4 to 9 mm.
  • the length of the tobacco rod portion 11 in the longitudinal direction may be changed appropriately in accordance with the size of the product.
  • the above length is usually 10 mm or more, is preferably 12 mm or more, is more preferably 15 mm or more, and is further preferably 18 mm or more.
  • the above length is usually 70 mm or less, is preferably 50 mm or less, is more preferably 30 mm or less, and is further preferably 25 mm or less.
  • the ratio of the length of the tobacco rod portion 11 to the length h of the non-combustion-heating-type tobacco 10 in the longitudinal direction is not limited. In consideration of the balance between the amount of delivery and aerosol temperature, the above ratio is usually 10% or more, is preferably 20% or more, is more preferably 25% or more, and is further preferably 30% or more. The above ratio is usually 80% or less, is preferably 70% or less, is more preferably 60% or less, is further preferably 50% or less, is particularly preferably 45% or less, and is most preferably 40% or less.
  • the content of the dry tobacco leaves in the tobacco rod portion 11 is, for example, but not limited to, 200 mg/rod portion or more and 800 mg/rod portion or less and is preferably 250 mg/rod portion or more and 600 mg/rod portion or less.
  • the above range is particularly suitable in the case where the tobacco rod portion has a perimeter of 22 mm and a length of 20 mm.
  • the flavoring agent-containing material is a material including a polysaccharide gel and a flavoring agent included in the polysaccharide gel. Adding the flavoring agent-containing material to the tobacco rod portion 11 reduces variations in the amount of flavoring agent delivered per puff from the early to late stages of smoking and enables a suitable flavor to be produced continuously.
  • the inventors of the present invention consider the reasons as follows. The smoking of a non-combustion-heating-type tobacco is started after it has been inserted into an electric heating device and preheated for a predetermined amount of time. In the case where a flavoring agent is added directly to the tobacco rod portion 11, the flavoring agent becomes volatilized during the preheating and the most part of the flavoring agent is delivered in the early stages of smoking.
  • the type of the flavoring agent is not limited.
  • the following flavoring agents may be used: acetanisole, acetophenone, acetylpyrazine, 2-acetylthiazole, an alfalfa extract, amyl alcohol, amyl butyrate, trans-anethole, a star anise oil, an apple juice, a Peru balsam oil, a beeswax absolute, benzaldehyde, benzoin resinoid, benzyl alcohol, benzyl benzoate, benzyl phenylacetate, benzyl propionate, 2,3-butanedione, 2-butanol, butyl butyrate, butyric acid, caramel, a cardamom oil, a carob absolute, ⁇ -carotene, a carrot juice, L-carvone, ⁇ -caryophyllene, a cassia bark oil, a cedarwood oil,
  • the content of the flavoring agent in the flavoring agent-containing material is usually, but not limited since it varies depending on the types of the flavoring agent and polysaccharide and the like, 18% by mass or more, is preferably 50% by mass or more, and is more preferably 60% by mass or more; and is usually 90% by mass or less and is preferably 80% by mass or less.
  • the type of the polysaccharide is not limited.
  • the polysaccharide is preferably a monocomponent polysaccharide, such as carrageenan, agar, gellan gum, tamarind gum, psyllium seed gum, or konjac glucomannan; or a complex polysaccharide that is a combination of two or more components selected from the group consisting of carrageenan, locust bean gum, guar gum, agar, gellan gum, tamarind gum, xanthan gum, tara gum, konjac glucomannan, starch, cassia gum, and psyllium seed gum.
  • a monocomponent polysaccharide such as carrageenan, agar, gellan gum, tamarind gum, psyllium seed gum, or konjac glucomannan
  • a complex polysaccharide that is a combination of two or more components selected from the group consisting of carrageenan, locust bean gum, guar gum,
  • the above polysaccharides which become gelated when heated to 30°C to 90°C in an aqueous solution, are preferable in that they eliminate the need to use a gelation reaction agent, such as a metal chloride, in the preparation of the flavoring agent-containing material and they do not generate components unfavorable during smoking, such as decomposition products of a chloride, in the mainstream smoke.
  • a gelation reaction agent such as a metal chloride
  • the flavoring agent-containing material may include an emulsifier used for emulsifying raw materials in the preparation of the flavoring agent-containing material.
  • emulsifier used for emulsifying raw materials in the preparation of the flavoring agent-containing material.
  • the types of the emulsifier include, but are not limited to, lecithin, glycerine fatty acid ester, polyglycerine fatty acid ester, sorbitan fatty acid ester, polyoxyethylene sorbitan fatty acid ester, propylene glycol fatty acid ester, and cane sugar fatty acid ester, and lecithin is preferable.
  • the above emulsifiers may be used alone or in combination of two or more.
  • the method for preparing the flavoring agent-containing material is not limited; the flavoring agent-containing material can be prepared in conformity with a publicly known method.
  • the publicly known method include the methods described in International Publication No. 2011/118040 , Japanese Unexamined Patent Application Publication No. 2013-099349 , and International Publication No. 2012/118034 .
  • the flavoring agent-containing material can be prepared using, for example, a method including the steps (i) and (ii) below.
  • the content of the flavoring agent-containing material in the tobacco rod portion 11 is usually, but not limited since it varies depending on the content of the flavoring agent in the flavoring agent-containing material, 1% by mass or more and is preferably 5% by mass or more of the amount of the dry tobacco leaves and is usually 20% by mass or less and is preferably 10% by mass or less of the amount of the dry tobacco leaves.
  • the tobacco rod portion 11 includes the flavoring agent-containing material such that the content of the flavoring agent included in the flavoring agent-containing material in the tobacco rod portion 11 is usually 1 mg or more, is preferably 5 mg or more, and is more preferably 10 mg or more; and is usually 30 mg or more and is preferably 20 mg or less.
  • the content of the flavoring agent-containing material in the tobacco rod portion 11 falls within the above range, a suitable flavor note can be imparted. Furthermore, variations in the amount of flavoring agent delivered per puff can be reduced from the early to late stages of smoking. Moreover, a sufficient amount of delivery can be maintained in all of the early, middle, and late stages of smoking.
  • the mode in which the flavoring agent-containing material is added to the tobacco rod portion 11 is not limited.
  • the flavoring agent-containing material may be disposed on the inner and/or outer surface of the wrapping paper with which the tobacco filler is wrapped.
  • the wrapping paper may be impregnated with the flavoring agent-containing material.
  • the flavoring agent-containing material may be added to the tobacco filler.
  • the above emulsion slurry is applied to the wrapping paper or the emulsion slurry is cast on a substrate and then dried to form a flavoring agent-containing sheet, which is wrapped around the tobacco filler together with the wrapping paper.
  • a wrapping paper impregnated with the flavoring agent-containing material can be prepared by immersing the wrapping paper in the emulsion slurry and then performing drying.
  • the emulsion slurry may be applied to dry tobacco leaves or dry tobacco leaves may be impregnated with the emulsion slurry.
  • the above-described flavoring agent-containing sheet or a material formed by shredding or pulverizing the flavoring agent-containing sheet may be mixed with dry tobacco.
  • the first tobacco filler is composed of shredded tobacco.
  • the material constituting the shredded tobacco included in the first filler is not limited; publicly known materials, such as lamina and midrib, can be used.
  • the first filler may be produced by pulverizing dry tobacco leaves into ground tobacco having an average particle size of 20 ⁇ m or more and 200 ⁇ m or less, homogenizing the pulverized tobacco particles, forming the homogenized tobacco particles into a sheet-like shape (hereinafter, such a sheet is also referred to simply as "homogenized sheet”), and shredding the sheet.
  • a homogenized sheet having a length substantially equal to the length of the tobacco rod in the longitudinal direction is shredded in a direction substantially parallel to the longitudinal direction of the tobacco rod and the shredded sheet is charged into the tobacco rod. That is, a "strand-type" tobacco filler may be used.
  • the width of the shredded tobacco is preferably 0.5 mm or more and 2.0 mm or less and the length of the shredded tobacco is preferably 3.0 mm or more and 10.0 mm or less.
  • a first example is a method in which a sheet is prepared using a papermaking process.
  • a second example is a method in which an appropriate solvent, such as water, is mixed with pulverized tobacco leaves, the resulting mixture is homogenized, the homogenized material is cast on a metal plate or a metal plate belt to form a thin layer, and the thin layer is dried to form a cast sheet.
  • a third example is a method in which an appropriate solvent, such as water, is mixed with pulverized tobacco leaves, the resulting mixture is homogenized, and the homogenized material is extrusion-molded into a sheet-like shape to form a rolled sheet. Details of types of the homogenized sheets are disclosed in "Encyclopedia of Tobacco, Tobacco Academic Studies Center, 2009.3.31".
  • the first tobacco filler preferably includes the flavoring agent-containing material.
  • the flavoring agent-containing material in order to make it easy to produce the advantageous effects of the present invention, it is preferable to add the flavoring agent-containing material to the first tobacco filler by mixing the flavoring agent-containing material with the shredded tobacco homogeneously.
  • Examples of the method for adding the flavoring agent-containing material to the first tobacco filler include, but are not limited to, a method in which the emulsion slurry is applied to the homogenized sheet or shredded tobacco or the homogenized sheet or shredded tobacco is impregnated with the emulsion slurry; and a method in which a material formed by shredding the flavoring agent-containing sheet is mixed with the shredded tobacco.
  • the method in which the material formed by shredding the flavoring agent-containing sheet is mixed with the shredded tobacco is preferable because of an easy and simple production process. In the above case, it is suitable to use a material formed by shredding the flavoring agent-containing sheet to a size substantially equal to the size of the shredded tobacco in order to make it easy to mix the shredded material with the shredded tobacco homogeneously.
  • the first tobacco filler may include a flavoring agent other than the flavoring agent-containing material in an amount with which the advantageous effects of the present invention are not impaired (hereinafter, the flavoring agent included in the flavoring agent-containing material may be referred to as "flavoring agent A", while the flavoring agent that is not included in the flavoring agent-containing material may be referred to as “flavoring agent B" for distinction).
  • the flavoring agent B are the same as those of the flavoring agent A included in the flavoring agent-containing material. The same applies to the preferable aspect.
  • the content of the flavoring agent B in the first tobacco filler is not limited as long as the advantageous effects of the present invention are not impaired.
  • the content of the flavoring agent B in the first tobacco filler is set such that the total content of the flavoring agents A and B in the first tobacco filler is usually 10000 ppm or more, is preferably 20000 ppm or more, and is more preferably 25000 ppm or more; and is usually 70000 ppm or less, is preferably 50000 ppm or less, is more preferably 40000 ppm or less, and is further preferably 33000 ppm or less.
  • the moisture content in the first tobacco filler is, for example, 10% by weight or more and 15% by weight or less and is preferably 11% by weight or more and 13% by weight or less of the total amount of the first tobacco filler.
  • the size of the shredded tobacco included in the first tobacco filler and a method for preparing the shredded tobacco are not limited.
  • a material prepared by shredding dry tobacco leaves to a width of 0.5 mm or more and 2.0 mm or less may be used.
  • a material prepared by pulverizing a homogenized sheet In the case where a material prepared by pulverizing a homogenized sheet is used, a material prepared by pulverizing dry tobacco leaves into particles having an average particle size of about 20 to 200 ⁇ m, homogenizing the particles, forming the homogenized material into a sheet-like shape, and shredding the resulting sheet to a width of 0.5 mm or more and 2.0 mm or less may be used.
  • the first tobacco filler may include an aerosol-source material that generates smoke aerosol.
  • the type of the aerosol-source material is not limited; substances extracted from various natural products and/or components thereof can be selected in accordance with the intended application.
  • Examples of the aerosol-source material include glycerine, propylene glycol, triacetin, 1,3-butanediol, and mixtures thereof.
  • the content of the aerosol-source material in the first tobacco filler is not limited. In order to generate aerosol in a sufficient manner and impart a good flavor, the above content is usually 5% by weight or more and is preferably 10% by weight or more; and is usually 50% by weight or less and is preferably 15% by weight or more and 25% by weight or less of the total amount of the first tobacco filler.
  • the pack density of the first tobacco filler is not limited. In order to maintain the performance of the non-combustion-heating-type tobacco at a certain level and impart a good flavor, the above pack density is usually 250 mg/cm 3 or more and is preferably 300 mg/cm 3 or more. The above pack density is usually 400 mg/cm 3 or less and is preferably 350 mg/cm 3 or less.
  • the tobacco rod portion 11 is prepared by wrapping the above-described first tobacco filler with a wrapping paper with the filler facing inward.
  • a second tobacco filler is constituted by tobacco sheets charged in a filling material that is to be filled.
  • the number of the tobacco sheets may be one or two or more.
  • the tobacco sheet may be, for example, a tobacco sheet having a length that is substantially the same as the length of the filling material in the longitudinal direction and filled in the filling material while being folded a plurality of times in a direction horizontal to the longitudinal direction of the filling material, that is, a "gathered sheet".
  • the above tobacco sheet may also be, for example, a tobacco sheet having a length that is substantially the same as the length of the filling material in the longitudinal direction and filled in the filling material while being wound in a direction orthogonal to the longitudinal direction of the filling material.
  • the tobacco sheets may be, for example, a plurality of tobacco sheets having a length that is substantially the same as the length of the filling material in the longitudinal direction and filled in the filling material while being wound in a direction orthogonal to the longitudinal direction of the filling material so as to be arranged concentrically.
  • the expression "arranged concentrically” means that the tobacco sheets are arranged such that all of the centers of the tobacco sheets are substantially at the same position.
  • the number of the tobacco sheets may be, for example, but not limited to, 2, 3, 4, 5, 6, or 7.
  • All of the two or more tobacco sheets may have the same composition or physical properties. Some or all of the tobacco sheets may have different compositions or physical properties. The thicknesses of the tobacco sheets may be equal to or different from one another
  • the second tobacco filler can be produced by preparing a plurality of tobacco sheets having different widths, laminating the tobacco sheets on top of one another such that the widths of the tobacco sheets decreases in the direction from bottom to top to prepare a multilayer body, and passing the multilayer body through a winding tube to perform winding forming.
  • This production method enables the tobacco sheets to extend in the longitudinal direction and be arranged concentrically with the longitudinal direction axis being the center.
  • a fitting portion extending in the longitudinal direction may be formed between the longitudinal direction axis and the innermost tobacco sheet.
  • the multilayer body be prepared such that a noncontact portion is formed between each pair of the adjacent tobacco sheets subsequent to the winding forming.
  • a noncontact portion at which the tobacco sheets do no come into contact with one another is present between the tobacco sheets, the flow path through which a flavor passes can be maintained and the efficiency with which a flavor component is delivered can be increased.
  • a high heat transfer efficiency can be achieved because the heat produced by a heater can be transferred to outer tobacco sheets through contact portions between the tobacco sheets.
  • the multilayer body may be prepared by, for example, the following methods: a method in which embossed tobacco sheets are used, a method in which the tobacco sheets are laminated on top of one another without bonding the entire surfaces of each pair of the adjacent tobacco sheets to each other; a method in which the tobacco sheets are laminated on top of one another with parts of each pair of the adjacent tobacco sheets being bonded to each other, and a method in which the tobacco sheets are laminated on top of one another while the entirety or parts of the surfaces of each pair of the adj acent tobacco sheets being bonded to each other slightly such that they become detached subsequent to the winding forming.
  • the wrapping paper may be arranged at the bottommost portion of the multilayer body.
  • the fitting portion can also be formed by placing a tubular dummy, such as a mandrel, at the topmost portion of the multilayer body and removing the dummy after the second tobacco filler has been formed.
  • a tubular dummy such as a mandrel
  • the pack density of the second tobacco filler is not limited. In order to maintain the performance of the tobacco product and impart a suitable flavor, the above pack density is usually 250 mg/cm 3 or more and is preferably 300 mg/cm 3 or more. The above pack density is usually 400 mg/cm 3 or less and is preferably 350 mg/cm 3 or less.
  • the second tobacco filler preferably includes the flavoring agent-containing material. Specifically, it is preferable to add the flavoring agent-containing material to the second tobacco filler by using a tobacco sheet coated or impregnated with the above-described emulsion slurry or winding the tobacco sheet together with the flavoring agent-containing sheet or a material formed by shredding or pulverizing the flavoring agent-containing sheet.
  • the second tobacco filler may include the flavoring agent B in an amount with which the advantageous effects of the present invention are not impaired.
  • Examples of the flavoring agent B are the same as those of the flavoring agent A. The same applies to the preferable aspect.
  • the content of the flavoring agent B in the second tobacco filler is not limited as long as the advantageous effects of the present invention are not impaired.
  • the content of the flavoring agent B in the second tobacco filler is set such that the total content of the flavoring agents A and B in the second tobacco filler is usually 10000 ppm or more, is preferably 20000 ppm or more, and is more preferably 25000 ppm or more; and is usually 70000 ppm or less, is preferably 50000 ppm or less, is more preferably 40000 ppm or less, and is further preferably 33000 ppm or less.
  • the tobacco sheets may include an aerosol-source material that generates smoke aerosol upon being heated.
  • An aerosol source such as a polyol, such as glycerine, propylene glycol, or 1,3-butanediol, is added as an aerosol-source material.
  • the amount of the aerosol-source material added is preferably 5% by weight or more and 50% by weight or less and is more preferably 15% by weight or more and 25% by weight or less of the dry weight of the tobacco sheet.
  • the tobacco sheets can be produced using a publicly known method, such as a papermaking method, a slurry method, or a rolling method, as needed.
  • a publicly known method such as a papermaking method, a slurry method, or a rolling method, as needed.
  • the homogenized sheet described in "First Tobacco Filler" above can also be used.
  • the tobacco sheets can be produced by a method including the following steps: 1) grinding dry tobacco leaves and subsequently performing extraction using water to separate a water extract and a residue from each other, and 2) drying the water extract under reduced pressures to perform concentration, 3) adding pulp to the residue, then performing fibrillation with a refiner, and subsequently perform papermaking, and 4) adding the condensate of the water extract to the resulting paper sheet, which is then dried to form a tobacco sheet.
  • a step of removing some of the components, such as nitrosamine may be further conducted (see Japanese Unexamined Patent Application Publication (Translation of PCT Application) No. 2004-510422 ).
  • the tobacco sheets can be produced by a method including the following steps: 1) mixing water, pulp, a binder, and ground tobacco leaves with one another, 2) stretching (casting) the resulting mixture into a thin film and drying the film.
  • a step of irradiating the slurry including water, pulp, a binder, and ground tobacco leaves with ultraviolet radiation or an X-ray to remove some of the components, such as nitrosamine, may be further conducted.
  • a nonwoven fabric-like tobacco sheet produced by a method including the following steps can also be used: 1) mixing powder-like tobacco leaves with a binding agent, 2) sandwiching the resulting mixture between nonwoven fabric sheets, and 3) forming the resulting multilayer body into a predetermined shape by thermal welding to produce a nonwoven fabric-like tobacco sheet.
  • the types of the tobacco leaves used as a raw material in the above methods may be the same as those described in the description of the first filler above.
  • the composition of the tobacco sheets is not limited.
  • the content of the tobacco raw material (tobacco leaves) is preferably 50% by weight or more and 95% by weight or less of the total weight of the tobacco sheet.
  • the tobacco sheets may include a binder.
  • the binder include a guar gum, a xanthan gum, CMC (carboxymethyl cellulose), and CMC-Na (sodium salt of carboxymethyl cellulose).
  • the amount of the binder is preferably 1% by weight or more and 10% by weight or less of the total weight of the tobacco sheet.
  • the tobacco sheets may further include another additive. Examples of the additive include a filler, such as pulp. In this embodiment, a plurality of tobacco sheets are used. All the tobacco sheets may have the same composition or the same physical properties. Some or all of the tobacco sheets may have different compositions or different physical properties.
  • each of the tobacco sheets are not limited. In consideration of the balance between heat transfer efficiency and strength, the above thickness is preferably 150 ⁇ m or more and 1000 ⁇ m or less and is more preferably 200 ⁇ m or more and 600 ⁇ m or less. The thicknesses of the tobacco sheets may be the same as or different from one another.
  • a third tobacco filler is composed of tobacco granules.
  • raw materials constituting the third tobacco filler include, but are not limited to, (a) a pulverized tobacco material, (b) moisture, (c) at least one pH-controlling agent selected from the group consisting of potassium carbonate and sodium hydrogen carbonate, and (d) at least one binder selected from the group consisting of pullulan and hydroxypropyl cellulose.
  • Examples of the pulverized tobacco material (component (a)) included in the third tobacco filler include pulverized tobacco leaves and a pulverized tobacco sheet.
  • the type of tobacco may be a Burley species, a yellow species, or an orient species.
  • the tobacco material is preferably pulverized to a size of 200 ⁇ m or more and 300 ⁇ m or less.
  • the content of the pulverized tobacco material in a mixture of the raw materials of the third tobacco filler is usually 20% by weight or more and 80% by weight or less.
  • the third tobacco filler preferably includes the flavoring agent-containing material.
  • Examples of the method for adding the flavoring agent-containing material to the third tobacco filler include, but are not limited to, a method in which the emulsion slurry or a material formed by pulverizing the flavoring agent-containing sheet is added to raw materials that constitute the tobacco granules; and a method in which a material formed by pulverizing the flavoring agent-containing sheet is mixed with the tobacco granules.
  • the method in which the material formed by pulverizing the flavoring agent-containing sheet is mixed with the tobacco granules is preferable because of an easy and simple production process.
  • the third tobacco filler may include the flavoring agent B in an amount with which the advantageous effects of the present invention are not impaired.
  • Examples of the flavoring agent B are the same as those of the flavoring agent A. The same applies to the preferable aspect.
  • the content of the flavoring agent B in the third tobacco filler is not limited as long as the advantageous effects of the present invention are not impaired.
  • the content of the flavoring agent B in the third tobacco filler is set such that the total content of the flavoring agents A and B in the third tobacco filler is usually 10000 ppm or more, is preferably 20000 ppm or more, and is more preferably 25000 ppm or more; and is usually 70000 ppm or less, is preferably 50000 ppm or less, is more preferably 40000 ppm or less, and is further preferably 33000 ppm or less.
  • the moisture (component (b)) included in the third tobacco filler maintains the unity of the tobacco granules.
  • the content of the moisture in a mixture of the raw materials of the third tobacco filler is usually 3% by weight or more and 13% by weight or less.
  • the third tobacco filler may include moisture such that the weight loss on drying is usually 5% by weight or more and 17% by weight or less.
  • weight loss on drying refers to the change in the weight of a part of the sample taken for the measurement which occurs while the sample is completely dried by causing all the moisture included in the sample to evaporate (e.g., drying for 15 minutes at a constant temperature (105°C)).
  • the pH-controlling agent (component (c)) included in the third tobacco filler is composed of potassium carbonate, sodium hydrogen carbonate, or a mixture thereof.
  • the pH-controlling agent adjusts the pH of the third tobacco filler to shift to alkaline, thereby accelerates the release of the flavor component included in the third tobacco filler from the tobacco granules, and produces a flavor that may satisfy the user.
  • the content of the pH-controlling agent in the mixture of the raw materials of the third tobacco filler may be usually 5% by weight or more and 20% by weight or less.
  • the binder (component (d)) included in the third tobacco filler causes the tobacco granule components to bind to one another and thereby maintains the unity of the tobacco granules.
  • the binder is composed of pullulan, hydroxypropyl cellulose (HPC), or a mixture thereof.
  • the content of the binder in the mixture of the raw materials of the third tobacco filler may be, usually, 0.5% by weight or more and 15% by weight or less.
  • the third tobacco filler which may be composed of the components (a), (b), (c), and (d) above, may further include an additional component.
  • the additional component examples include an aerosol-source material (component (e)).
  • the aerosol-source material is a material that generates smoke aerosol.
  • the aerosol-source material is composed of a polyhydric alcohol.
  • the polyhydric alcohol include glycerine, propylene glycol, sorbitol, xylitol, and erythritol. The above polyhydric alcohols can be used alone or in combination of two or more.
  • the content of the aerosol-source material may be 5% to 15% by weight.
  • Examples of the additional component further include (f) a flavor material (solid or liquid) other than the flavor component.
  • a flavor material include sugar (e.g., sucrose or fructose), a cocoa powder, a carob powder, a coriander powder, a licorice powder, an orange peel powder, a rose hip powder, a chamomile flower (flower) powder, a lemon verbena powder, a peppermint powder, a leaf powder, a spearmint powder, a black tea powder, and menthol.
  • sugar e.g., sucrose or fructose
  • a cocoa powder e.g., a cocoa powder, a carob powder, a coriander powder, a licorice powder, an orange peel powder, a rose hip powder, a chamomile flower (flower) powder, a lemon verbena powder, a peppermint powder, a leaf powder, a spearmint powder, a black tea powder, and menthol.
  • the content of the flavor material in the mixture of the raw materials of the third tobacco filler may be, usually, 0.5% by weight or more and 30% by weight or less.
  • the flavor material may be added to the components (a), (b), (c), (d), and (e) by being directly kneaded with these components.
  • the flavor material may also be added to the above components by supporting the flavor material on a publicly known inclusion host compound, such as cyclodextrin, to form an inclusion compound and kneading the inclusion compound with the above components.
  • the content of the component (a) in the mixture of the raw materials of the third tobacco filler may be, usually, about 33% by weight or more (and about 90% by weight or less).
  • the third tobacco filler can be produced by mixing the components (a), (c), and (d) and, as needed, the components (e) and (f) with one another, adding the component (b) to the resulting mixture, then kneading the mixture, granulating the kneaded material into particles (long pillar-shaped) with a wet extrusion granulation machine, and subsequently forming the particles into a short pillar-like or spherical shape.
  • the average particle size (D50) of the resulting tobacco granules is usually 0.2 mm or more and 1.2 mm or less, is preferably 0.2 mm or more and 1.0 mm or less, and is more preferably 0.2 mm or more and 0.8 mm or less.
  • the kneaded material be extruded at a pressure of 2 kN or more and ambient temperature.
  • the temperature of the kneaded material instantaneously and rapidly increases from ambient temperature to, for example, 90°C to 100°C at the outlet of the extrusion granulation machine and the amount of moisture and volatile component reduces by 2% by weight or more and 4% by weight or less as a result of evaporation. Therefore, the water used for preparing the kneaded material is set to be larger than the amount of moisture that is intended to be included in the tobacco granules, which is the final product, by an amount equal to the amount of the evaporation.
  • the tobacco granules prepared by the extrusion granulation may be further dried as needed for moisture control.
  • the tobacco granules prepared by the extrusion granulation may be further dried in order to achieve the intended weight loss on drying.
  • the drying conditions (temperature and time) necessary for achieving the intended weight loss on drying can be set on the basis of predetermined drying conditions (temperature and time) necessary for reducing the weight loss on drying by a predetermined value.
  • the third tobacco filler may be composed only of the tobacco granules described above.
  • the third tobacco filler may further include an additional tobacco material other than the tobacco granules.
  • the additional tobacco material is usually shredded tobacco leaves or a fine powder of tobacco leaves.
  • the additional tobacco material can be used in combination with tobacco granules in the form of a mixture.
  • the wrapping paper is not limited, and a common wrapping paper may be employed.
  • Examples of the wrapping paper include a wrapping paper that includes pulp as a principal component.
  • the wrapping paper may be a wrapping paper made of a wood pulp, such as a conifer wood pulp or a broadleaf wood pulp, or a wrapping paper made of pulp mixture further including a nonwood pulp commonly used for producing wrapping paper for tobacco products, such as a flax pulp, a cannabis pulp, a sisal hemp pulp, or an esparto pulp.
  • Examples of the pulp that can be used include a chemical pulp, a ground pulp, a chemiground pulp, or a thermomechanical pulp, which are produced by kraft cooking, acidic, neutral, or alkaline sulfite cooking, sodium salt cooking, or the like.
  • a wrapping paper is produced with a fourdrinier paper machine, a cylinder paper machine, a cylinder-tanmo hybrid paper machine, or the like using the pulp.
  • the formation is arranged and homogenization is performed.
  • a wet strength agent may be added to impart water resistance to the wrapping paper
  • a sizing agent may be added to adjust the manner in which printing is performed on the wrapping paper.
  • aluminum sulfate various anionic, cationic, nonionic, and zwitterionic internal agents for papermaking, such as a yield improver, a freeness improver, and a strength agent
  • papermaking additives such as a dye, a pH-controlling agent, an antifoaming agent, a pitch-controlling agent, and a slime-controlling agent, can also be added.
  • the basis weight of the base paper for the wrapping paper is, for example, usually 20 gsm or more and is preferably 25 gsm or more.
  • the above basis weight is usually 65 gsm or less, is preferably 50 gsm or less, and is further preferably 45 gsm or less.
  • the thickness of the wrapping paper having the above properties is not limited. In consideration of stiffness, air permeability, and ease of control during papermaking, the above thickness is usually 10 ⁇ m or more, is preferably 20 ⁇ m or more, and is more preferably 30 ⁇ m or more. The above thickness is usually 100 ⁇ m or less, is preferably 75 ⁇ m or less, and is more preferably 50 ⁇ m or less.
  • Examples of the shape of the wrapping paper included in the non-combustion-heating-type tobacco include square and rectangular.
  • the length of a side of the wrapping paper is, for example, about 12 to 70 mm.
  • the length of the other side is, for example, 15 to 28 mm, is preferably 22 to 24 mm, and is further preferably about 23 mm.
  • the length of a side of the wrapping paper is, for example, 20 to 60 mm.
  • the length of the other side is, for example, 15 to 28 mm.
  • the wrapping paper may include a filler in addition to the above pulp.
  • the content of the filler is, for example, 10% by weight or more and less than 60% by weight and is preferably 15% by weight or more and 45% by weight or less of the total weight of the wrapping paper.
  • the content of the filler in the wrapping paper is preferably 15% by weight or more and 45% by weight or less when the basis weight falls within the preferable range (25 gsm or more and 45 gsm or less).
  • the above filler content is preferably 15% by weight or more and 45% by weight or less.
  • the above filler content is preferably 25% by weight or more and 45% by weight or less.
  • the filler examples include calcium carbonate, titanium dioxide, and kaolin.
  • calcium carbonate is preferably used.
  • a water resistance improver may be added in order to enhance water resistance.
  • the water resistance improver include a wet strength agent (WS agent) and a sizing agent.
  • the wet strength agent include a urea formaldehyde resin, a melamine formaldehyde resin, and polyamide epichlorohydrin (PAE).
  • PAE polyamide epichlorohydrin
  • the sizing agent include a rosin soap, alkyl ketene dimer (AKD), alkenylsuccinic anhydride (ASA), and highly saponified polyvinyl alcohol having a degree of saponification of 90% or more.
  • a strength agent may be added as an agent.
  • the strength agent include polyacrylamide, a cationic starch, an oxidized starch, CMC, a polyamide epichlorohydrin resin, and polyvinyl alcohol.
  • the use of a trace amount of oxidized starch enhances air permeability ( Japanese Unexamined Patent Application Publication No. 2017-218699 ).
  • the wrapping paper may be coated as needed.
  • a coating agent may be applied onto at least one of the two surfaces, that is, the front and rear surfaces, of the wrapping paper.
  • the coating agent is not limited. It is preferable to use a coating agent capable of forming a film on the surface of the paper and thereby reducing the permeability of the paper to liquids.
  • alginic acid and salts thereof e.g., sodium salt
  • polysaccharides such as pectin
  • cellulose derivatives such as ethyl cellulose, methyl cellulose, carboxymethyl cellulose, and nitro cellulose
  • starch and derivatives thereof e.g., ether derivatives, such as a carboxymethyl starch, a hydroxyalkyl starch, and a cationic starch
  • ester derivatives such as starch acetate, starch phosphate, and starch octenylsuccinate.
  • the tipping paper 15 is not limited and may be a common one, such as paper including pulp as a principal component.
  • the paper may be paper made of a wood pulp, such as a conifer wood pulp or a broadleaf wood pulp, or paper made of pulp mixture further including nonwood pulp commonly used for producing wrapping paper for tobacco items, such as a flax pulp, a cannabis pulp, a sisal hemp pulp, or an esparto pulp.
  • the above pulp materials may be used alone. Alternatively, a plurality of types of pulp materials may be used in combination at any ratio.
  • the tipping paper 15 may be constituted by one sheet or a plurality of sheets.
  • pulp materials examples include a chemical pulp, a ground pulp, a chemiground pulp, and a thermomechanical pulp, which are produced by kraft cooking, acidic, neutral, or alkaline sulfite cooking, sodium salt cooking, or the like.
  • the tipping paper 15 may be either a tipping paper produced by the production method described below or a commercial tipping paper.
  • the shape of the tipping paper 15 is not limited.
  • the tipping paper 15 may be, for example, square or rectangle.
  • the basis weight of the tipping paper 15 is usually, but not limited to, 32 gsm or more and 40 gsm or less, is preferably 33 gsm or more and 39 gsm or less, and is more preferably 34 gsm or more and 38 gsm or less.
  • the air permeability of the tipping paper 15 is usually, but not limited to, 0 CORESTA unit or more and 30000 CORESTA unit or less and is preferably more than 0 CORESTA unit and 10000 CORESTA unit or less.
  • air permeability refers to a value measured in conformity with ISO 2965:2009. Air permeability is expressed as an amount (cm 3 ) of gas that passes through an area of 1 cm 2 per minute when a pressure difference between the surfaces of the paper is 1 kPa. Note that 1 CORESTA unit (1 C.U.) is cm 3 /(min ⁇ cm 2 ) at 1 kPa.
  • the tipping paper 15 may contain a filler in addition to the above pulp.
  • a filler in addition to the above pulp.
  • examples thereof include metal carbonates, such as calcium carbonate and magnesium carbonate, metal oxides, such as titanium oxide, titanium dioxide, and aluminum oxide, metal sulfates, such as barium sulfate and calcium sulfate, metal sulfides, such as zinc sulfide, quartz, kaolin, talc, diatomaceous earth, and gypsum.
  • metal carbonates such as calcium carbonate and magnesium carbonate
  • metal oxides such as titanium oxide, titanium dioxide, and aluminum oxide
  • metal sulfates such as barium sulfate and calcium sulfate
  • metal sulfides such as zinc sulfide, quartz, kaolin, talc, diatomaceous earth, and gypsum.
  • tipping paper 15 include calcium carbonate.
  • the above fillers may be used alone or in combination of two or more.
  • the tipping paper 15 may include a water resistance improver in order to enhance.
  • the water resistance improver include a wet strength agent (WS agent) and a sizing agent.
  • the wet strength agent include a urea formaldehyde resin, a melamine formaldehyde resin, and polyamide epichlorohydrin (PAE).
  • PAE polyamide epichlorohydrin
  • the sizing agent include a rosin soap, an alkyl ketene dimer (AKD), alkenylsuccinic anhydride (ASA), and highly saponified polyvinyl alcohol having a degree of saponification of 90% or more.
  • a coating agent may be added onto at least one of the front and rear surfaces of the tipping paper 15.
  • the coating agent is not limited and is preferably a coating agent with which a film can be formed on the surface of the paper and which thereby reduces liquid permeability.
  • non-combustion-heating-type tobacco can be applied to the electric heating tobacco product described below, it can also be applied to cigarettes (paper-wrapped tobaccos), which involve combustion.
  • the method for producing the above-described non-combustion-heating-type tobacco is not limited; publicly known methods may be used.
  • the non-combustion-heating-type tobacco can be produced by wrapping the tipping paper around the tobacco rod portion and the mouthpiece portion.
  • An electric heating tobacco product according to another embodiment of the present invention is an electric heating tobacco product constituted by an electric heating device including a heater member, a battery unit that serves as a power source for the heater member, and a control unit that controls the heater member and the above-described non-combustion-heating-type tobacco inserted in the electric heating device so as to come into contact with the heater member.
  • the electric heating tobacco product may be an electric heating tobacco product that heats the outer circumferential surface of the non-combustion-heating-type tobacco 10 as illustrated in Fig. 3 or an electric heating tobacco product that heats the inside of the tobacco rod portion 11 of the non-combustion-heating-type tobacco 10 as illustrated in Fig. 4 .
  • An electric heating tobacco product 30 is described below with reference to Fig. 4 .
  • reference numerals that denote the components illustrated in Figs. 1 and 2 are partially omitted.
  • the above-described non-combustion-heating-type tobacco 10 is inserted into an electric heating device 20 so as to come into contact with a heater member 21 disposed in the electric heating device 20.
  • the electric heating device 20 includes a body 24 formed of a resin or the like and a battery unit 22 and a control unit 23 that are disposed inside the body 24.
  • the outer circumferential surface of the tobacco rod portion 11 is brought into contact with the heater member 21 of the electric heating device 20 and, subsequently, the entirety of the outer circumferential surface of the tobacco rod portion 11 and a part of the outer circumferential surface of the tipping paper are brought into contact with the heater member 21.
  • the heater member 21 of the electric heating device 20 produces heat due to the control performed by the control unit 23.
  • the control unit 23 As a result of the heat transferring to the tobacco rod portion 11 of the non-combustion-heating-type tobacco 10, the aerosol-source material, flavor component, and the like included in the tobacco filler of the tobacco rod portion 11 become volatilized.
  • the heater member 21 may be, for example, a sheet-like heater, a tabular heater, or a tubular heater.
  • the sheet-like heater is a flexible, sheet-shaped heater. Examples thereof include a heater including a film (thickness: about 20 to 225 ⁇ m) formed of a heat-resistant polymer, such as polyimide.
  • the tabular heater is a stiff, flat sheet-shaped heater (thickness: about 200 to 500 ⁇ m). Examples thereof include a heater that includes, for example, a flat-sheet substrate and a resistance circuit disposed on the substrate, the resistance circuit serving as a heat-producing portion.
  • the tubular heater is a hollow or solid tube-shaped heater (thickness: about 200 to 500 ⁇ m).
  • Examples thereof include a heater that includes, for example, a cylinder made of a metal or the like and a resistance circuit formed on the outer periphery of the cylinder, the resistance circuit serving as a heat-producing portion.
  • Examples of the tubular heater further include rod-shaped and cone-shaped heaters made of a metal or the like which include an internal resistance circuit that serves as a heat-producing portion.
  • the cross-sectional shape of the tubular heater may be, for example, a circular shape, an oval shape, a polygonal shape, or the shape of a polygon with rounded corners.
  • the sheet-like heater, the tabular heater, and the tubular heater can be used.
  • the electric heating tobacco product is an electric heating tobacco product that heats the inside of the tobacco rod portion 11 included in the non-combustion-heating-type tobacco 10 as illustrated in Fig. 4 .
  • the length of the heater member 21 in the longitudinal direction may fall within the range of L ⁇ 5.0 mm, where L [mm] represents the length of the tobacco rod portion 11 in the longitudinal direction.
  • L [mm] represents the length of the tobacco rod portion 11 in the longitudinal direction.
  • the length of the heater member 21 in the longitudinal direction is preferably L mm or more.
  • the above length is preferably L + 0.5 mm or less, L + 1.0 mm or less, L + 1.5 mm or less, L + 2.0 mm or less, L + 2.5 mm or less, L + 3.0 mm or less, L + 3.5 mm or less, L + 4.0 mm or less, L + 4.5 mm or less, or L + 5.0 mm or less.
  • the heating intensity such as the amount of heating time during which the heater member 21 heats the non-combustion-heating-type tobacco 10 and the heating temperature at which the heater member 21 heats the non-combustion-heating-type tobacco 10, can be predetermined for each electric heating tobacco product 30.
  • the heating intensity can be predetermined such that, after the non-combustion-heating-type tobacco 10 has been inserted into the electric heating device 20, preheating is performed for a predetermined period of time to increase the temperature of the outer circumferential surface of the portion of the non-combustion-heating-type tobacco 10 which is inserted in the electric heating device 20 to X(°C) and the temperature is subsequently maintained to be a certain temperature equal to or less than X(°C).
  • the temperature X(°C) is preferably 80°C or more and 400°C or less in consideration of the amount of the delivered components generated by heating or the like.
  • the temperature X(°C) can be 80°C, 90°C, 100°C, 110°C, 120°C, 130°C, 140°C, 150°C, 160°C, 170°C, 180°C, 190°C, 200°C, 210°C, 220°C, 230°C, 240°C, 250°C, 260°C, 270°C, 280°C, 290°C, 300°C, 310°C, 320°C, 330°C, 340°C, 350°C, 360°C, 370°C, 380°C, 390°C, or400°C.
  • a vapor including components derived from the aerosol-source material, components derived from the flavor component, etc. which are generated from the tobacco rod portion 11 as a result of heating performed by the heater member 21 is delivered into the oral cavity of the user through the mouthpiece portion 14, which is constituted by the cooling segment 12, the filter segment 13, etc.
  • the perforations V formed in the cooling segment 12 are preferably present at a position closer to the mouth end than the mouth end-side end (the position denoted by the arrow X in the drawing) of a region of the cooling segment 12 which comes into contact with the electric heating device 20, as illustrated in Fig. 5 .
  • the insertion opening of the electric heating device 20 through which the non-combustion-heating-type tobacco 10 is inserted into the electric heating device 20 may be tapered as illustrated in Fig. 6 in order to make it easy to insert the non-combustion-heating-type tobacco 10 into the electric heating device 20.
  • the mouth end-side end of a region of the cooling segment 12 which comes into contact with the electric heating device 20 is the position denoted by the arrow Y in the drawing.
  • reference numerals that denote the components illustrated in Figs. 1 to 4 are partially omitted.
  • a liquid mixture of 1.0 g of gellan gum ("KELCOGEL " produced by CP Kelco), 1.0 g of tamarind gum ("BISTOP D-2032" produced by San-Ei Gen F.F.I., Inc.), and 100 mL of water was heated in a thermostat water tank kept at 80°C in order to dissolve gellan gum and tamarind gum in water to a sufficient degree.
  • the resulting emulsion slurry was cast on an appropriate support in a sheet-like form. Then, drying was performed for 1 week with a forced air circulation dryer at 40°C. Hereby, a flavoring agent-containing sheet having a thickness of 100 ⁇ m was prepared.
  • the sheet-like flavoring agent-containing material was cut into pieces having a width of about 1 mm and a length of about 10 mm with scissors. Then, about 0.1 g of pieces of the flavoring agent-containing material was precisely weighed and charged into a serum bottle.
  • 10 mL of methanol for HPLC, produced by Wako
  • the serum bottle was closed with a rubber stopper and hermetically sealed with a PARAFILM (registered trademark).
  • the serum bottle was then shaken at 200 rpm for 40 minutes with a shaker. After the serum bottle had been left to stand for 12 hours or more temporarily, it was again shaken for another 40 minutes with the shaker.
  • the serum bottle was left to stand for 5 minutes.
  • the supernatant was taken with a Pasteur pipette and used as a sample for the measurement of the content of the flavoring agent. Note that, since the extract had a high concentration, it was diluted 10-fold prior to the analysis.
  • the above sample was analyzed with GC-FID (produced by Agilent) under the measurement conditions below.
  • the content of the flavoring agent in the flavoring agent-containing material was determined on the basis of the peak area value.
  • the content of the flavoring agent (menthol) in the flavoring agent-containing material was 70% by mass.
  • the flavoring agent-containing sheet was shredded into strip-shaped pieces having a width of 1 mm and a length of 3 mm.
  • a material formed by shredding the flavoring agent-containing sheet was prepared.
  • a tobacco filler was prepared. Using a high-speed wrapping machine, the tobacco filler was wrapped with a wrapping paper (produced by Nippon Paper Papylia Co., Ltd., basis weight: 35 g/m 2 , thickness: 52 ⁇ m).
  • the weight of shreds per stick was 0.8 g.
  • the perimeter of the stick was 22 mm.
  • the length of the stick was 68 mm.
  • the stored tobacco rod portions were cut to a length of 20 mm. Subsequently, the tobacco rod portion, a paper tube having a length of 20 mm (cooling segment), and a filter segment having a length of 20 mm which was constituted by a center hole filter (5.8Y35000) having a through-hole (diameter: 4.5 mm) and a filter having a length of 20 mm and filled with cellulose acetate fibers were wrapped with the tipping paper prepared above. Hereby, a non-combustion-heating-type tobacco having no perforations was prepared.
  • the diameter of the perforations was adjusted such that the proportion of the air taken in through the perforations when inhalation was performed at 17.5 ml/sec with a single-port automated smoking machine produced by Borgwaldt was 72% by volume.
  • the above air inflow proportion was measured in conformity with ISO9512. In all of Example and Comparative Example described below, the diameter of the perforations was adjusted such that the above air inflow proportion was 72% by volume.
  • Example 1 The non-combustion-heating-type tobacco prepared in Example 1 was subjected to a smoking test in order to evaluate the amount of the delivered components generated by heating.
  • the smoking test was conducted under the following conditions in accordance with Canadian Intense Smoking (CIR).
  • CIR Canadian Intense Smoking
  • the heater temperature was increased to 295°C within 21 seconds and then reduced to 260°C within 5 seconds. Subsequently, the temperature was maintained at 260°C until the evaluation was completed (for about 330 seconds). Then, in the smoking test, automated smoking was performed using a single-port automated smoking machine produced by Borgwaldt at a flow rate of 55 cc/2 sec and smoking intervals of 30 sec. In this test, the positions of the perforations formed in the cooling segment were adjusted to be 25.5 mm from the mouth end-side end of the region of the non-combustion-heating-type tobacco which came into contact with the electric heating device.
  • the mainstream smoke generated in the smoking test was collected with a Cambridge pad. After a puff action had been performed 12 times, the Cambridge pad was removed and extraction was performed with 10 mL of ethanol. The amount of menthol included in the mainstream smoke which was taken by the puff actions was measured by GC-MS.
  • Table 1 lists and Fig. 7 illustrates the amount of menthol delivered from the non-combustion-heating-type tobacco prepared in Example 1 in each puff, with the total amount of menthol delivered being 1.
  • a non-combustion-heating-type tobacco of Comparative Example 1 was prepared using the same method as in Example 1, except that a tobacco filler prepared by adding menthol to a mixture of sheet-like shredded tobacco (width: 0.8 mm), 15 g/100 g of glycerine, and 4 g/100 g of propylene glycol such that the content of menthol in a final non-combustion-heating-type tobacco was 7 mg was used.
  • the amount of flavoring agent delivered from the non-combustion-heating-type tobacco was evaluated as in Example 1. Table 1 lists and Fig. 7 illustrates the results.
  • Example 1 Comparative example 1 Puff (number of times) 1 0.072 0.078 2 0.095 0.152 3 0.114 0.180 4 0.117 0.135 5 0.112 0.104 6 0.114 0.080 7 0.094 0.067 8 0.078 0.056 9 0.064 0.048 10 0.053 0.041 11 0.047 0.032 12 0.039 0.027

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  • General Chemical & Material Sciences (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)
EP21910165.6A 2020-12-24 2021-11-30 Tabakprodukt zur erwärmung ohne verbrennung und elektrisch erhitztes tabakprodukt Pending EP4268630A1 (de)

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BR0114448A (pt) 2000-10-05 2003-09-02 Nicolas Baskevitch Redução de nitrosaminas em tabaco e em produtos de tabaco
RU2010151986A (ru) * 2008-05-19 2012-06-27 Джапан Тобакко Инк. (Jp) Содержащий ароматизатор материал для сигареты, способ его получения и сигарета
WO2011118040A1 (ja) 2010-03-26 2011-09-29 日本たばこ産業株式会社 揮発性香料デリバリー量を高めたシガレット
JP2012118034A (ja) 2010-12-03 2012-06-21 Azbil Corp 差圧センサの故障判定方法及び故障判定装置
US8967155B2 (en) 2011-11-03 2015-03-03 Celanese Acetate Llc Products of high denier per filament and low total denier tow bands
EP2625975A1 (de) 2012-02-13 2013-08-14 Philip Morris Products S.A. Aerosolerzeugender Artikel mit Aerosolkühlelement
JP6014684B2 (ja) 2012-12-28 2016-10-25 日本たばこ産業株式会社 非燃焼吸引型たばこ製品用香味源及び非燃焼吸引型たばこ製品
JP5395285B2 (ja) 2013-01-23 2014-01-22 八鹿鉄工株式会社 施肥装置
JP2017218699A (ja) 2016-06-09 2017-12-14 日本製紙パピリア株式会社 喫煙物品用巻紙
CN113163856B (zh) * 2018-12-07 2023-08-18 日本烟草产业株式会社 非燃烧加热型吸烟物品以及电加热型吸烟系统

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