EP4265059A1 - Élément porte-échantillon pour un appareil de laboratoire - Google Patents
Élément porte-échantillon pour un appareil de laboratoireInfo
- Publication number
- EP4265059A1 EP4265059A1 EP21844297.8A EP21844297A EP4265059A1 EP 4265059 A1 EP4265059 A1 EP 4265059A1 EP 21844297 A EP21844297 A EP 21844297A EP 4265059 A1 EP4265059 A1 EP 4265059A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- receiving element
- sample receiving
- sample
- layer
- separating layer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000010410 layer Substances 0.000 claims description 182
- 239000000463 material Substances 0.000 claims description 58
- 238000003760 magnetic stirring Methods 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 13
- 238000013316 zoning Methods 0.000 claims description 11
- 238000009434 installation Methods 0.000 claims description 10
- 229910000838 Al alloy Inorganic materials 0.000 claims description 9
- 230000033001 locomotion Effects 0.000 claims description 8
- 239000011241 protective layer Substances 0.000 claims description 8
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 239000004020 conductor Substances 0.000 claims description 6
- 230000003647 oxidation Effects 0.000 claims description 6
- 238000007254 oxidation reaction Methods 0.000 claims description 6
- 230000000149 penetrating effect Effects 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 229910000676 Si alloy Inorganic materials 0.000 claims description 4
- -1 aluminum-magnesium-silicon Chemical compound 0.000 claims description 4
- 230000000694 effects Effects 0.000 claims description 4
- 239000000615 nonconductor Substances 0.000 claims description 4
- 238000002161 passivation Methods 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 description 14
- 229910052782 aluminium Inorganic materials 0.000 description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000000919 ceramic Substances 0.000 description 3
- 239000012212 insulator Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 229910017916 MgMn Inorganic materials 0.000 description 2
- 238000007743 anodising Methods 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000001652 electrophoretic deposition Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 238000005304 joining Methods 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 230000013011 mating Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000006748 scratching Methods 0.000 description 1
- 230000002393 scratching effect Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000003313 weakening effect Effects 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B3/00—Ohmic-resistance heating
- H05B3/68—Heating arrangements specially adapted for cooking plates or analogous hot-plates
- H05B3/74—Non-metallic plates, e.g. vitroceramic, ceramic or glassceramic hobs, also including power or control circuits
- H05B3/746—Protection, e.g. overheat cutoff, hot plate indicator
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/45—Magnetic mixers; Mixers with magnetically driven stirrers
- B01F33/452—Magnetic mixers; Mixers with magnetically driven stirrers using independent floating stirring elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F35/92—Heating or cooling systems for heating the outside of the receptacle, e.g. heated jackets or burners
Definitions
- the present invention relates to a sample receiving element for a laboratory device and a laboratory device with such a sample receiving element.
- a magnetic stirrer This comprises a sample receiving element designed as a heating plate, on the upper side of which a sample receiving vessel is provided.
- a magnetic drive is arranged below the heating plate, which generates a changing magnetic field during operation, which in turn sets a magnetic stirring rod provided in the sample receiving vessel into a stirring movement.
- the heating plate can be made of aluminum or an aluminum alloy, for example, in order in particular to allow good heat transfer to the sample receptacle.
- the heating plate comprises a metal-ceramic layered composite with a base layer made of an aluminum alloy and a ceramic layer facing the vessel.
- the magnetic stirrer T shows a magnetic stirrer T according to the prior art with a heating plate or mounting plate 3' which has a round shape and is formed as a continuous layer of a base material at least in a plane parallel to the surface of the mounting plate 3'. Furthermore, the magnetic stirrer T has a magnetic drive 6 and a drive magnet (not shown) in order to generate a changing magnetic field during operation, which a magnetic stirring bar arranged in a sample 4 set in motion. As shown schematically in FIG. 4, the changing magnetic field (represented by the magnetic field lines 20') penetrates the mounting plate 3' during operation of the magnetic stirrer and, in particular in conjunction with the magnetic field of the magnetic stirring bar 4, can generate electrical eddy currents 21' in the mounting plate 3'.
- these eddy currents 21' in turn generate a magnetic field which counteracts the magnetic field generating them and thus weakens the changing magnetic field of the drive magnet and/or causes the drive to be braked.
- a sample receiving element serves for use in or with a laboratory device and is designed to receive a sample to be treated by means of the laboratory device and penetrated by a magnetic field during operation of the laboratory device.
- the sample receiving element is designed to effect an interruption, at least in sections, of an electric current induced by changes in the magnetic field penetrating the sample receiving element.
- the sample receiving element can be part of the laboratory device, for example designed as a mounting plate for a magnetic stirrer, or be a sample receiving element provided separately from the laboratory device, such as a container or a pot for receiving a sample.
- the temperature of the sample receiving element can preferably be controlled by means of a temperature control device in order to allow heat to be transferred from or to a sample received by the sample receiving element.
- a temperature control device is understood to mean, in particular, a device which is designed to heat and/or cool the sample receiving element and/or a sample arranged thereon.
- the temperature control device can be a temperature control device formed integrally with the sample receiving element, or a temperature control device which is provided separately or externally from the sample receiving element and is thermally conductively connected to the sample receiving element.
- the temperature control device can, for example, enable heating and/or cooling of the sample to be treated.
- the sample receiving element preferably has a first side facing the sample and a second side facing away from the sample, in particular opposite the first side, and the sample receiving element comprises a base layer made of at least one base material and a separating layer, the separating layer being in a region of the sample receiving element from extends from the first side to the second side of the sample receiving element and forms a zoning of the base layer, and the separating layer is formed from a separating layer material which has a greater electrical resistivity than the at least one base material of the base layer.
- the separating layer can extend continuously from the first side to the second side of the sample receiving element, but it can also be formed only in sections between the first and the second side.
- the first side of the sample-receiving element facing the sample can be, for example, an upper side on which the sample, in particular a sample-receiving vessel, is arranged, for example when the sample-receiving element is designed as an installation plate.
- the first side of the sample receiving element can be, for example, an inside of a container in which the sample is provided.
- the second side facing away from the sample can be, for example, an underside opposite the top, or alternatively an outside of a container.
- the separating layer is formed from a separating layer material that has a higher specific electrical resistance (i.e. is less electrically conductive or has lower electrical conductivity) than a base material of the base layer, the separating layer has an electrically insulating effect at least up to a certain current intensity.
- induced electrical currents essentially cannot flow through the separating layer, which can lead to an overall reduction in electrical currents occurring in the sample receiving element.
- the separating layer is preferably formed at least partially by converting the base material of the base layer, in particular by producing an oxidic layer by anodic oxidation of the base layer and/or by passivating the base layer.
- the production of an oxidic layer by anodic oxidation of the base layer can be carried out, for example, in a process which is also referred to as “anodising process” or “anodising” (from eloxal, abbreviation for electrolytic oxidation of aluminum).
- the layer is formed by converting the surface of the base layer in a galvanic bath, the base layer forming the anode.
- the separating layer can be implemented, for example, by electrophoretic deposition, in particular cathodic dip painting (KTL coating).
- KTL coating cathodic dip painting
- the formation of the separating layer by conversion from the base material of the base layer has the advantage, for example, that the separating layer as an electrically essentially non-conductive layer in a simple way and way can be made from the base material.
- a layer can be provided in a simple manner, which can interrupt an electrical current flow in the sample receiving element.
- the separating layer formed in this way can have a particularly smooth surface, for example.
- the separating layer can be a layer formed separately from the base layer, in particular a plastic layer. Different types of a separating layer are thus provided, for example, which can also be combined with one another.
- the base material is an electrical conductor and the release liner material is an electrical non-conductor.
- a subdivision into electrical non-conductors (insulators) and electrical conductors can be made, for example, based on the specific electrical resistance p of the respective material, whereby, for example, materials with p ⁇ 100 ⁇ -mm 2 /m are referred to as conductors and materials with p > 10 12 ⁇ -mm 2 /m as an insulator.
- a separating layer is thus provided, for example, which can interrupt an electrical current flow in the sample receiving element.
- the separating layer preferably has an extension of 50 pm to 130 pm, more preferably 60 pm to 120 pm and even more preferably 90 pm to 110 pm in a direction parallel to the first side and/or the second side of the sample receiving element.
- a relatively thin separating layer is thus provided, for example, which essentially does not impede the transfer of thermal energy through the sample receiving element to or from the sample.
- the base material is preferably an aluminum alloy, more preferably an aluminum-magnesium-silicon alloy, such as material no. 3.2315, according to European standard EN AW 6082; AISil MgMn or similar material. Since an aluminum alloy has good thermal conductivity, a good thermal energy transfer can be achieved by using the same as a base material or to the sample-receiving element, as well as good control of the temperature of the sample-receiving element by means of a temperature control device.
- the sample receiving element is a plate having a defined geometric shape, preferably a circular, oval, rectangular, or square plate, and the separating layer is provided in a centered area of the plate such that the separating layer divides the base layer into a first zone and one provided around it second zone divided. More preferably, a largest diameter of the first zone essentially corresponds to a maximum extension of a magnetic stirring bar, which can be set in motion by the magnetic field penetrating the sample receiving element.
- the separating layer is thus provided, for example, in an area in which the magnetic field penetrates the sample receiving element during operation of the laboratory device, as a result of which the greatest possible reduction in electrical currents that occur can be brought about.
- the sample receiving element is a circular plate and the separating layer is provided in a centered annular region of the plate, such that the separating layer divides the base layer into a first circular zone and a second annular zone provided therearound. More preferably, the diameter of the first zone essentially corresponds to a maximum extent of a magnetic stirring bar.
- the sample receiving element preferably has a first side facing the sample and a second side facing away from the sample, in particular opposite the first side, and a recess extending from the first side to the second side is provided in a region of the sample receiving element.
- the recess can be provided as an alternative or in addition to the separating layer described above.
- the recess is continuous from the first to the second side of the sample receiving element.
- a protective layer is preferably provided on the first side of the sample receiving element, wherein the protective layer is more preferably made of the same material as the separating layer and/or the protective layer is more preferably formed at least partially by conversion from the base material of the base layer.
- a layer is thus provided on the first side of the sample receiving element, for example, which protects the sample receiving element, in particular from mechanical influences such as scratching and/or chemical influences such as corrosion.
- a laboratory device comprises a sample receiving element as described above, with the laboratory device preferably being designed as a magnetic stirrer and more preferably the sample receiving element being designed as an installation plate, in particular a temperature control plate, of the magnetic stirrer.
- the effects described above in relation to the sample receiving element can also be achieved with a laboratory device.
- a method according to the invention is used to produce a sample receiving element for a laboratory device, wherein the sample receiving element is designed to receive a sample to be treated by the laboratory device and is penetrated by a magnetic field during operation of the laboratory device and the sample receiving element has a first side facing the sample and one of the sample second side facing away, in particular opposite the first side.
- the method comprises the steps of: providing a base layer of the sample receiving element and forming a separating layer in a region of the sample receiving element such that the separating layer extends from the first side to the second side of the sample receiving element and forms a zoning of the base layer, the separating layer being formed from a separating layer material , which has a larger electrical resistivity than a base material of the base layer.
- the step of forming a separating layer may include a step of forming a recess, the recess being provided in a portion of the sample receiving member and extending from the first side to the second side.
- a mating insert manufactured separately is placed in the recess.
- the insert forms the first zone of the base layer and can be made of the same Material like the first zone of the base layer. However, the insert can also be made from a different material, preferably also from an aluminum alloy.
- at least a first zone of the base layer is removed when forming a recess, so that the first zone and a second zone of the base layer formed by removing the first zone are present.
- the first zone has a first, outer edge and the second zone has a second, inner edge.
- the separating layer is then formed on the first edge and/or the second edge, and the sample receiving element is formed by subsequently joining the first and second zones, in particular inserting the first zone into the second zone of the base layer, so that the separating layer is between the first and the second zone is formed. More preferably, the assembly is done by thermal press fitting.
- the method according to the invention can also be further developed by the features of the sample receiving element and/or the laboratory device described above.
- the sample receiving element according to the invention and the laboratory device can be further developed by the features of the method according to the invention described above, and the features of the sample receiving element and the laboratory device can be used together for further development.
- FIG. 1 shows a schematic perspective view of an embodiment of a laboratory device according to the present invention in the form of a magnetic stirrer
- FIG. 2 shows a schematic, perspective view of the magnetic stirrer shown in FIG. 1, the magnetic stirrer being shown without a housing and with magnetic field lines shown purely schematically during operation of the magnetic stirrer;
- 3 shows a schematic plan view of a mounting plate of the magnetic stirrer shown in FIGS. 1 and 2;
- FIG. 4 shows a schematic, perspective view of a magnetic stirrer according to the prior art, the magnetic stirrer being shown without a housing and with magnetic field lines shown purely schematically during operation of the magnetic stirrer;
- Fig. 5 is a schematic representation of steps for manufacturing the magnetic stirrer shown in Figs. 1 to 3.
- FIGS. 1 to 3 A first exemplary embodiment of a laboratory device according to the present invention is described below with reference to FIGS.
- the laboratory device shown in FIGS. 1 to 3 is designed as a magnetic stirrer 1 .
- the magnetic stirrer 1 has a housing 2 (not shown in FIG. 2), on the top of which is a mounting plate
- a heat reflector 5 is optionally arranged between the mounting plate 3 and the housing 2 .
- a magnetic drive 6 (see FIG. 2) and a drive magnet (not shown in the figures) are provided in the housing 2 and are designed such that the magnetic drive 6 sets the drive magnet in motion, in particular a rotary motion, during operation.
- a changing, preferably rotating, magnetic field is thus generated.
- the magnetic drive 6 is mounted on a base plate 7 which is fixed to the housing 2 (not shown in FIG. 2).
- Fastening elements 8 are also provided, by means of which the mounting plate 3 and optionally the optional heat reflector 5 are attached to the housing 2 (not shown in FIG. 2).
- the changing magnetic field can also be generated in other ways, for example by electronically controlling coils.
- the mounting plate 3 is optionally designed as a temperature control plate, in particular as a heating plate.
- the mounting plate has a temperature control device, in particular a heating device (not shown in the figures) for supplying and/or discharging heat energy to and from the mounting plate 3 .
- the temperature control device (not shown in the figures) can be formed integrally with the mounting plate, for example in the form of temperature control elements integrated into the mounting plate. Alternatively, the temperature control device can be provided separately from the mounting plate and connected to it in a thermally conductive manner.
- Operating elements 9 for controlling the operation of the magnetic stirrer 1 for example a heating temperature of the mounting plate and/or properties of the changing magnetic field that can be predetermined by the magnetic drive 6 , are provided on the housing 2 .
- an operating unit provided separately from or integrally on the magnetic stirrer can be provided for controlling the individual components of the magnetic stirrer (not shown in the figures).
- the mounting plate 3 has a first side facing away from the housing 2 (i.e. facing a sample) designed as an upper side 11 and a second side facing the housing 2 (i.e. facing away from a sample) designed as a lower side 12 .
- the top 11 and the bottom 12 are opposite sides of the mounting plate 3.
- a peripheral edge 13 of the mounting plate 3 extends between the top 11 and the bottom 12.
- the set-up plate 3 is circular, i.e. the upper side 11 and the lower side 12 are each circular.
- a protective layer 14 is optionally provided on the upper side 11 of the mounting plate 3 .
- the mounting plate 3 is essentially divided into a first zone 15, a second zone 16 and a separating layer 17.
- the separating layer 17 is in an area of the installation plate 3 between the first zone
- the separating layer 17 extends continuously from the top 11 to the underside 12 of the installation plate 3.
- the first zone 15 and the second zone 16 are formed from a base material and the separating layer 17 is formed from a different separating layer material from the base material.
- the first zone 15 of the base layer is a central circular zone of the installation plate 3 with a first diameter D1.
- the separating layer 17 radially directly adjoins the first zone 15 and is formed in the shape of a circular ring around the first zone 15 .
- the separating layer 17 thus extends in an area between the first diameter D1 and a second diameter D2 of the mounting plate 3.
- the second zone 16 of the base layer radially directly adjoins the separating layer 17 and is formed around the separating layer 17 in the shape of a circular ring.
- the second zone 16 thus extends in an area between the second diameter D2 and a third diameter D3 of the mounting plate 3.
- the first diameter D1 of the installation plate 3, in which the first zone 15 of the base layer is provided, and/or the second diameter D2, in which the second zone 16 of the base layer adjoins the separating layer 17, essentially corresponds to a maximum extension of the magnetic stirring bar 4, for example a length L of an elongate magnetic stirring rod (see FIG. 2).
- the first diameter D1 and the second diameter D2 are preferably only slightly different, so that the separating layer 17 is a thin layer compared to the first and second zones 15, 16.
- the thickness of the separating layer is between about 90 ⁇ m and about 110 ⁇ m.
- the third diameter D3 corresponds to an overall diameter of the mounting plate 3.
- the first, second and third diameters D1, D2 and D3 are not shown to scale in FIG. in order to better illustrate the separating layer, the difference is shown in FIG shown too large in relation to the individual diameters between the second diameter D2 and the first diameter D1.
- the base material of the base layer of the first and second zones 15, 16 and the separating layer material of the separating layer 17 differ in that the separating layer material has a greater electrical resistance than the base material.
- the release liner material is an electrical non-conductor (insulator) and the base material is an electrical conductor.
- the base material can be an aluminum alloy, in particular an aluminum alloy containing silicon, magnesium and manganese (aluminium-magnesium-silicon alloy), such as the alloy referred to as AISil MgMn according to European standard EN-AW 6082 (material number 3.2315).
- the separating layer material can contain, in particular, aluminum oxide (Al2O3).
- the separating layer material of the separating layer 17 is preferably formed by conversion from the base material of the base layer, in particular by producing an oxidic layer by anodic oxidation of the base layer.
- An exemplary manufacturing method for the installation plate 3 is described further below with reference to FIG. 5 .
- the sample or a vessel containing it (not shown in the figures) is placed on the mounting plate 3 and the magnetic stirring rod 4 is introduced into the sample or the vessel.
- Switching on the magnetic drive 6 causes the drive magnet (not shown in the figures) to rotate, which in turn causes a stirring movement of the magnetic stirring rod 4 in the sample or the vessel and thus a thorough mixing of the sample.
- the installation plate 3 is penetrated by a magnetic field during operation of the magnetic stirrer 1, which is generated by the interaction of the drive magnet (not shown) and the magnetic stirring rod 4 and is shown schematically in Fig. 2 by magnetic field lines 20.
- This changing magnetic field induces electrical eddy currents 21, shown purely schematically in Fig. 2.
- the separating layer 17 is provided essentially in the area of the mounting plate 3 in which the magnetic field lines 20 penetrate the mounting plate. This can bring about the greatest possible weakening or prevention of the eddy currents 21 that occur.
- a base layer of the mounting plate is provided.
- the base layer is formed as a cylindrical layer (i.e. having a circular top 11 and bottom 12, respectively) of base material, e.g. the aluminum-magnesium-silicon alloy described above, of diameter D3 (see Figure 3).
- a piece corresponding to the first zone 15 (see Figs. 1-3) of the base layer is removed, for example cut out.
- the separating layer or the separating layer material is formed on the first edge and/or the second edge of the first or second zone.
- the separating layer is preferably formed by conversion from the base material of the base layer, in that an oxidic layer is produced on the first and/or second edge by anodic oxidation of the base layer.
- the separating layer can be formed by passivating the base layer at the first and/or second edge.
- a fourth step S4 of the method the first zone 15 is inserted into the second zone 16 of the base layer, so that the separating layer 17 (see FIGS. 1-3) is formed between the first and the second zone.
- the merging of Both zones of the base layer can be done, for example, by a thermal press fit.
- the separating layer 17 is thus formed in a region of the base layer, extending continuously from the top 11 to the bottom 12 and forming a zoning of the base layer.
- the separating layer can be formed in step S3 in such a way that this layer is also formed on the upper side 11 of the sample receiving element and thus forms the protective layer 14 .
- the separating layer can be a layer formed separately from the base layer, in particular a plastic layer, which is applied, for example, in the area between the two zones of the base layer or is used as a ring.
- the zoning of the mounting plate by the separating layer is also not limited to the embodiment described above.
- more than two zones of the base layer can also be formed by the separating layer.
- the zoning of the base layer can also be formed differently than by concentric circles (see Fig. 1-3), eg by a spiral-shaped separating layer, so that a continuous area of the base layer is formed, which is however radially interrupted by the separating layer.
- the separating layer can also divide the base layer of the mounting plate into at least two circular sectors (sectors of a circle), a circular sector being understood to mean a partial area of a circular area that is delimited by an arc of a circle and two circle radii.
- the separating layer can also divide the base layer of the mounting plate into at least two circular segments, a circular segment being understood to mean a partial area of a circular area delimited by an arc of a circle and a chord. Other zonings or a combination of these zonings are also possible within the scope of the present invention.
- the mounting plate itself can deviate from the circular configuration described above.
- the first zone 15 and the second zone 16 of the base layer are formed from the same base material.
- the first zone and the second zone, or generally at least two zones of the base layer to be formed from different base materials.
- Plastic, non-magnetic or non-conductive stainless steel, glass, ceramics, etc. can also be used as base materials.
- the base layer and optionally also the separating layer can have further layers horizontally, ie parallel to the top 11 and/or bottom 12 of the set-up plate.
- the separating layer 17 does not have to extend continuously from the top
- the underside 12 of the erection board can also be discontinuous, i.e. only partially formed between the top and the underside.
- the mounting plate has at least one recess instead of or in addition to the zoning of the base layer formed by the separating layer described above.
- the at least one recess is provided in at least one area of the mounting plate. It extends at least partially from the top 11 to the bottom
- the recess can be designed as a hole penetrating the mounting plate from the top to the bottom.
- the recess or hole can be provided, for example, in the area of the central circular area with the first diameter described above with reference to Figs. 1-3 (ie instead of the first zone 15 in Figs. 1-3).
- the at least one recess preferably a plurality of holes, can be provided in an annular area of the mounting plate, for example in an annular area containing the separating layer 17 in FIGS. 1-3.
- Such a recess, in particular a hole, in the mounting plate can also interrupt, ie weaken or prevent, eddy currents 21 occurring during operation of the magnetic stirrer.
- the present invention is not limited to a laboratory device in the form of a magnetic stirrer. Rather, the invention can also be applied to other laboratory devices that generate a changing magnetic field during operation.
- the invention is not limited to a mounting plate as a sample receiving element.
- the sample receiving element can have a so-called heat-on attachment.
- a heat-on attachment is an attachment for a heating plate and represents the thermal coupling between the heating plate and the sample vessel.
- the present invention can also be applied to a sample receiving element designed as a pot or another vessel.
- the pot or the vessel can be designed to hold a sample to be treated with the laboratory device.
- the zoning or formation of a separating layer according to the invention can be formed, for example, in a base of the heat-on attachment or the pot or vessel.
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Automatic Analysis And Handling Materials Therefor (AREA)
Abstract
L'invention concerne un élément porte-échantillon destiné à être utilisé dans ou avec un appareil de laboratoire (1), l'élément porte-échantillon (3) étant conçu pour contenir un échantillon à traiter au moyen de l'appareil de laboratoire (1) et étant pénétré par un champ magnétique (20) pendant que l'appareil de laboratoire est en fonctionnement, et l'élément porte-échantillon (3) étant conçu pour interrompre, au moins en partie, un courant électrique (21) qui est induit par des variations du champ magnétique qui pénètre dans l'élément porte-échantillon (3).
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE202021100315.4U DE202021100315U1 (de) | 2021-01-22 | 2021-01-22 | Probenaufnahmeelement für ein Laborgerät |
PCT/EP2021/087224 WO2022156989A1 (fr) | 2021-01-22 | 2021-12-22 | Élément porte-échantillon pour un appareil de laboratoire |
Publications (1)
Publication Number | Publication Date |
---|---|
EP4265059A1 true EP4265059A1 (fr) | 2023-10-25 |
Family
ID=79687156
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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EP21844297.8A Pending EP4265059A1 (fr) | 2021-01-22 | 2021-12-22 | Élément porte-échantillon pour un appareil de laboratoire |
Country Status (5)
Country | Link |
---|---|
US (1) | US20240139697A1 (fr) |
EP (1) | EP4265059A1 (fr) |
CN (1) | CN116965152A (fr) |
DE (1) | DE202021100315U1 (fr) |
WO (1) | WO2022156989A1 (fr) |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3043335A1 (de) * | 1980-11-17 | 1982-06-24 | Helmut Dipl.-Ing. 8990 Lindau Herz | Magnet-ruehreinrichtung |
DE4140595C2 (de) | 1991-12-10 | 1995-06-14 | Alfred Langer | Segment-Heizadapter zum Beheizen von Glasrundkolben oder kugelförmigen Glasbehältern auf planen Heizplatten |
DE20201349U1 (de) * | 2002-01-30 | 2002-04-25 | IKA - Werke GmbH & Co. KG, 79219 Staufen | Magnetrührer mit einer beheizbaren Aufstellplatte |
DE102006005155B3 (de) | 2006-02-04 | 2007-08-23 | Hans Heidolph Gmbh & Co. Kg | Magnetrührer mit Heizplatte |
DE102008029901B4 (de) | 2008-06-24 | 2010-10-28 | Ika-Werke Gmbh & Co. Kg | Magnetrührer mit Aufstellfüßen |
DE102013010275C5 (de) | 2013-06-18 | 2016-09-15 | Ika-Werke Gmbh & Co. Kg | Magnetrührer mit SAW-Sensor |
DE102015120101A1 (de) | 2015-11-19 | 2017-05-24 | Hans Heidolph Gmbh & Co. Kg | Laborgerät |
DE202018001492U1 (de) | 2018-03-20 | 2018-05-03 | Heidolph Instruments GmbH & Co. KG | Laborgerätsystem und Laborgerät |
CN111672446B (zh) * | 2020-07-09 | 2023-06-27 | 苏州北开生化设备有限公司 | 一种用于化学合成的多维玻璃反应釜及其工作方法 |
-
2021
- 2021-01-22 DE DE202021100315.4U patent/DE202021100315U1/de active Active
- 2021-12-22 WO PCT/EP2021/087224 patent/WO2022156989A1/fr active Application Filing
- 2021-12-22 EP EP21844297.8A patent/EP4265059A1/fr active Pending
- 2021-12-22 US US18/273,385 patent/US20240139697A1/en active Pending
- 2021-12-22 CN CN202180095543.4A patent/CN116965152A/zh active Pending
Also Published As
Publication number | Publication date |
---|---|
WO2022156989A1 (fr) | 2022-07-28 |
CN116965152A (zh) | 2023-10-27 |
DE202021100315U1 (de) | 2022-04-25 |
US20240139697A1 (en) | 2024-05-02 |
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