EP4069652A1 - Anlage zur behandlung von glasbehältern mit einer kammer zur dosierung einer behandlungssubstanz mit doppelblende und zugehöriges verfahren - Google Patents
Anlage zur behandlung von glasbehältern mit einer kammer zur dosierung einer behandlungssubstanz mit doppelblende und zugehöriges verfahrenInfo
- Publication number
- EP4069652A1 EP4069652A1 EP20829951.1A EP20829951A EP4069652A1 EP 4069652 A1 EP4069652 A1 EP 4069652A1 EP 20829951 A EP20829951 A EP 20829951A EP 4069652 A1 EP4069652 A1 EP 4069652A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- container
- metering chamber
- treatment substance
- installation
- treatment
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000126 substance Substances 0.000 title claims abstract description 206
- 239000011521 glass Substances 0.000 title claims abstract description 94
- 238000009434 installation Methods 0.000 title claims abstract description 91
- 238000000034 method Methods 0.000 title claims abstract description 64
- 238000009826 distribution Methods 0.000 claims description 42
- 238000001514 detection method Methods 0.000 claims description 22
- 230000000694 effects Effects 0.000 claims description 21
- 238000011144 upstream manufacturing Methods 0.000 claims description 16
- 230000033001 locomotion Effects 0.000 claims description 11
- 230000008569 process Effects 0.000 claims description 6
- 230000026058 directional locomotion Effects 0.000 claims 1
- 239000000047 product Substances 0.000 description 13
- 239000006185 dispersion Substances 0.000 description 7
- 230000001276 controlling effect Effects 0.000 description 6
- 150000002500 ions Chemical class 0.000 description 6
- 230000003287 optical effect Effects 0.000 description 6
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 5
- 230000004888 barrier function Effects 0.000 description 5
- 238000013461 design Methods 0.000 description 5
- 238000012545 processing Methods 0.000 description 5
- 238000013519 translation Methods 0.000 description 5
- 239000003513 alkali Substances 0.000 description 4
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 4
- 235000011130 ammonium sulphate Nutrition 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 230000000670 limiting effect Effects 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- 239000011358 absorbing material Substances 0.000 description 3
- 239000001166 ammonium sulphate Substances 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 238000007496 glass forming Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000003303 reheating Methods 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 238000000137 annealing Methods 0.000 description 2
- 239000005388 borosilicate glass Substances 0.000 description 2
- 238000004891 communication Methods 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 230000003301 hydrolyzing effect Effects 0.000 description 2
- 238000011065 in-situ storage Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000036961 partial effect Effects 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 235000011837 pasties Nutrition 0.000 description 2
- -1 polyethylene Polymers 0.000 description 2
- 230000000284 resting effect Effects 0.000 description 2
- 230000000717 retained effect Effects 0.000 description 2
- 239000005361 soda-lime glass Substances 0.000 description 2
- 229910001415 sodium ion Inorganic materials 0.000 description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 description 2
- 235000011152 sodium sulphate Nutrition 0.000 description 2
- 150000003464 sulfur compounds Chemical class 0.000 description 2
- HSEYYGFJBLWFGD-UHFFFAOYSA-N 4-methylsulfanyl-2-[(2-methylsulfanylpyridine-3-carbonyl)amino]butanoic acid Chemical compound CSCCC(C(O)=O)NC(=O)C1=CC=CN=C1SC HSEYYGFJBLWFGD-UHFFFAOYSA-N 0.000 description 1
- 239000007832 Na2SO4 Substances 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 235000019270 ammonium chloride Nutrition 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 239000010836 blood and blood product Substances 0.000 description 1
- 229940125691 blood product Drugs 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000000593 degrading effect Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000013528 metallic particle Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 230000010355 oscillation Effects 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000007142 ring opening reaction Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 210000002700 urine Anatomy 0.000 description 1
- 230000003313 weakening effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C21/00—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface
- C03C21/007—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface in gaseous phase
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C23/00—Other surface treatment of glass not in the form of fibres or filaments
- C03C23/008—Other surface treatment of glass not in the form of fibres or filaments comprising a lixiviation step
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B1/00—Packaging fluent solid material, e.g. powders, granular or loose fibrous material, loose masses of small articles, in individual containers or receptacles, e.g. bags, sacks, boxes, cartons, cans, or jars
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B3/00—Packaging plastic material, semiliquids, liquids or mixed solids and liquids, in individual containers or receptacles, e.g. bags, sacks, boxes, cartons, cans, or jars
- B65B3/003—Filling medical containers such as ampoules, vials, syringes or the like
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B55/00—Preserving, protecting or purifying packages or package contents in association with packaging
- B65B55/24—Cleaning of, or removing dust from, containers, wrappers, or packaging ; Preventing of fouling
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/001—General methods for coating; Devices therefor
- C03C17/003—General methods for coating; Devices therefor for hollow ware, e.g. containers
- C03C17/004—Coating the inside
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C23/00—Other surface treatment of glass not in the form of fibres or filaments
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C23/00—Other surface treatment of glass not in the form of fibres or filaments
- C03C23/007—Other surface treatment of glass not in the form of fibres or filaments by thermal treatment
Definitions
- the present invention relates to the general technical field of installations and methods for treating glass containers.
- the invention relates more specifically to an installation for treating the inside face of the wall of a glass container, such as a bottle, which wall defines a receiving cavity for a product and an opening giving access to said cavity. 'reception, said installation comprising a source of a powdery or granular treatment substance and a means for distributing said treatment substance inside the receiving cavity of the container.
- the invention also relates to a method of treating the inner face of the wall of a glass container, such as a flask, which wall defines a receiving cavity for a product and an opening giving access to said cavity. receiving, said method comprising providing a source of a powdery or granular treatment substance and a step of dispensing said treatment substance inside the receiving cavity of the container by means of a means of distribution.
- Such a treatment is generally carried out by introducing into the interior of a glass container to be treated a reactive treatment substance which is capable, under the action of heat, of generating an acid gas capable of chemically reacting with it.
- alkali ions present in the glass of the container.
- the extraction of alkaline ions from the surface of the interior wall of the container thus makes it possible in particular to significantly improve the chemical resistance (or hydrolytic resistance) of the container.
- treatment installations comprising a means for distributing a treatment substance formed from ammonium sulphate (NH4) 2SO4, for example, in the form of a crystalline powder or in the form of tablets or briquettes, inside of hot glass containers.
- NH4 2SO4 ammonium sulphate
- the ammonium sulphate introduced into the container sublimates and forms a gas which reacts with the sodium contained in the glass in the immediate vicinity of the inner wall of the container.
- the sodium thus extracted from the glass then settles on the surface of the inner wall of the vessel in the form of a residual powdery compound of sodium sulfate Na2SO4, which can then be washed away.
- Installations designed to dispense a powdery treatment substance comprise a means for distributing the treatment substance in the form of a diffuse and continuous flow of treatment substance which flows freely over glass containers passing by on a conveyor positioned under the distribution means.
- the objects assigned to the present invention therefore aim to remedy the various drawbacks listed above and to propose a new installation, as well as a corresponding method, which make it possible to treat glass containers of any size and capacity in a particularly precise and efficient manner. , even at very high speeds.
- Another object of the invention aims to provide a new treatment plant, as well as a corresponding new treatment method, which make it possible to treat glass containers in a particularly reliable and repeatable manner.
- Another object of the invention aims to provide a new treatment installation, as well as a corresponding new treatment method, which make it possible to efficiently treat glass containers without degrading their mechanical strength.
- Another object of the invention aims to provide a new treatment installation, as well as a corresponding new treatment method, the implementation of which is particularly simple and economical.
- Another object of the invention aims to provide a new treatment installation, as well as a corresponding new treatment method, the implementation of which is particularly safe.
- Another object of the invention is to provide a new treatment plant, as well as a corresponding new treatment method, which make it possible to obtain glass containers having very good hydrolytic resistance.
- the objects assigned to the invention are achieved using an installation for treating the inside face of the wall of a glass container, such as a flask, which wall defines a receiving cavity for a product. and an opening giving access to said receiving cavity, said installation comprising a source of a powdery or granular treatment substance and a means for distributing said treatment substance inside the receiving cavity of the container, said installation being characterized in that said dispensing means comprises at least one metering chamber which extends between an inlet port supplied by said source of treatment substance and an opposite outlet port intended to be positioned above the opening of the container, as well as an upper shutter and a lower shutter of the metering chamber positioned in a stepped manner respectively at the level of the inlet port and the outlet port of the chamber dosage.
- the objects assigned to the invention are also achieved using a method of treating the inner face of the wall of a glass container, such as a flask, which wall defines a receiving cavity for a product and an opening providing access to said receiving cavity, said method comprising providing a source of a powdery or granular treatment substance and a step of distributing said treatment substance within the cavity of.
- said method being characterized in that said dispensing means comprises at least one metering chamber which extends between an inlet orifice supplied by said source of treatment substance and an opposing outlet port positioned at the above the opening of the container, as well as an upper shutter and a lower shutter of the metering chamber positioned in a stepped manner respectively at the level of the inlet opening and the outlet opening of the metering chamber.
- FIG. 1 illustrates, partially and schematically, a preferred embodiment of an installation according to the invention.
- Such an installation is advantageously designed to be arranged and implemented in combination with a conveyor, on which runs a container to be treated;
- Figure 2 illustrates, in a partial schematic view in front section, a detail of the distribution means of the installation of Figure 1;
- Figure 3 illustrates, in a partial schematic view in longitudinal section, a detail of the distribution means of the installation of Figure 1.
- the invention relates to an installation 1 for treating a glass container 2, such as a flask.
- the invention further relates, according to a second independent aspect, to a method of treating such a glass container 2.
- the container 2 concerned by the installation 1 and method in accordance with the invention comprises a wall 3 delimiting a receiving cavity 4 for a product (or substance) and an opening 5 giving access to said receiving cavity 4, which glass wall 3 has an inner face 6, located opposite said receiving cavity 4 and preferably intended to come into direct contact with said product, and an opposite outer face 7.
- the installation 1 and the treatment method according to the invention are, in this case, the installation 1 and the method for treating the inner face 6 of the wall 3 of such a glass container 2.
- the installation 1 and the treatment method according to the invention preferably constitute an industrial installation and process, advantageously automated, intended to be integrated into industrial production lines and processes of glass containers.
- said installation 1 and said method are preferably designed to allow the treatment of a large number of glass containers 2 in a substantially uninterrupted manner.
- the term "glass” denotes a mineral glass.
- the glass constituting the wall 3 of the container 2 is transparent (or at least translucent) in the visible range. It can be either a colorless or colored glass, in particular to protect the fluid substance contained within the container from the effects of light, in particular in certain wavelength ranges (UV, etc.).
- the container 2 concerned by the invention may have any shape suited to its function, such as for example a flask or bottle shape.
- the wall 3 of the container 2 is advantageously formed by a bottom 8 of glass, a side wall 9 of glass which rises from the periphery of the bottom 8, and a neck 10 provided with 'a ring 11 which delimits the opening 5 of the container 2, to allow the reception cavity 4 to be placed in communication with the outside.
- said opening 5 is designed to be able to be closed by a stopper or a cap, removable or perforable.
- the product intended to be received in the cavity 4 of the container 2 is advantageously fluid, that is to say capable of flowing, for example a liquid, pasty substance (such as a liquid with a degree of high viscosity) or powdery.
- it is a product or substance of a pharmaceutical nature, such as for example a medicament, possibly intended to be administered parenterally (general or locoregional) or alternatively to be ingested or absorbed by a patient, or alternatively.
- a substance of a diagnostic nature such as for example a chemical or biological reagent.
- the container 2 can be designed to contain a substance of a biological nature (or body fluid), such as for example blood, a blood product or by-product, urine, etc.
- the invention is however not limited to the treatment of containers 2 for pharmaceutical or diagnostic use and may in particular relate to a container designed to contain a liquid, pasty or pulverulent substance for use. industrial (product storage chemicals, etc.), scientific (laboratory glassware), veterinary, food, or even cosmetics.
- the installation 1 comprises a source 12 of a treatment substance 13, that is to say - say of an advantageously reactive substance, intended to obtain the desired treatment effect. More specifically, it is a powdery or granular treatment substance 13, advantageously formed of crystals or grains with an average size typically between 500 ⁇ m to 1600 ⁇ m). As such, said powdery or granular treatment substance 13 is advantageously able to flow freely under its own weight under the effect of gravity.
- a source 12 may comprise a reservoir or a hopper 14, capable of receiving and at least temporarily storing a certain quantity of treatment substance 13 ready for use.
- the source 12 could comprise a device for manufacturing or preparing in situ of said treatment substance 13.
- the installation 1 further comprises a means 15 for distributing the treatment substance 13 inside the receiving cavity 4 of the container 2, via the opening 5 of the latter.
- the distribution means 15 is advantageously designed to dose and deliver a predetermined (or at least determinable) quantity of said treatment substance 13.
- the distribution means 15 comprises at least one chamber 16 for dosing said substance 13 for treatment. Defining within it a recess 17 intended to receive the treatment substance 13, the metering chamber 16 extends between an inlet port 18 supplied by the source 12 of treatment substance 13 and an opposite outlet port 19 ( and therefore distinct from the inlet orifice 18) intended to be positioned above, and preferably opposite, the opening 5 of a container 2 to be treated (FIG. 1).
- Said metering chamber 16 is advantageously arranged vertically, the inlet port 18 forming an upper orifice, through which the treatment substance 13 can enter the internal recess 17 of the metering chamber 16, while the 'outlet 19 forms a lower orifice, advantageously intended to be positioned opposite and in line with the opening 5 of the container 2, and through which the substance 13 of treatment contained in the metering chamber 16 can be distributed, evacuated, under the effect of gravity, in the direction of the opening 5 of said container 2 to be treated placed under the outlet orifice 19 of the metering chamber 16.
- the installation 1 further comprises an upper shutter 20 (or upper valve) and a lower shutter 21 (or lower valve) of the metering chamber 16, which are positioned in a stepped manner respectively at the level of the inlet port 18 and outlet port 19 of the metering chamber 16.
- the metering chamber 16 is thus provided with an upper shutter 20 and a lower shutter 21, provided to respectively close the inlet port 18 and the outlet port 19 of the metering chamber 16.
- said upper 20 and lower 21 shutters are suitable to evolve between
- the metering chamber 16 extends longitudinally along a first axis A-A ', from the inlet port 18 to the outlet port 19 of the chamber 16 of dosage.
- the metering chamber 16 comprises at least a first portion 16A of the chamber, which extends along the first axis AA 'from the outlet port 19 towards the inlet port 18 of the metering chamber 16, and which defines a first recess portion 17A of cylindrical shape, preferably of circular section, oriented axially along the first axis A-A '.
- the volume of said first portion 17A of course is advantageously chosen as a function of the quantity of treatment substance 13 which it is desired to introduce into the container 2 to be treated.
- the diameter (or width) of said first portion 17A of course is for its part advantageously chosen less than the diameter (or width) of the opening 5 of the container 2 to be treated.
- the diameter of said first portion 17A of course can thus be between 3 mm and 20 mm, for containers 2 to be treated, the diameter of the opening 5 of which is between 10 mm and 30 mm.
- the quantity of treatment substance 13 metered by the metering chamber 16 can advantageously flow out of the metering chamber 16, when opening the lower shutter 21, in a substantially “straight” thread or generally. cylindrical. In this way, the risk of spatial dispersion of the treatment substance 13 at the outlet of the metering chamber 16 is greatly limited, and the introduction into the cavity 4 of the container 2 of substantially the entire quantity is thus favored.
- the metering chamber 16 can advantageously comprise a second chamber portion 16B, which axially extends said first chamber portion 16A to the inlet port 18 of the metering chamber 16, and which defines a second portion 17B of frustoconical shape (funnel shape) in order to guide the treatment substance 13 passing through the inlet port 18 of the metering chamber 16 when the upper shutter 20 is opened towards the second chamber portion 16B.
- the metering chamber 16 can define an internal recess of a different conformation from that described above.
- the metering chamber 16 is shaped and configured in such a way that the treatment substance 13 can flow out of the metering chamber 16, through the outlet orifice 19 of this. last, according to a sufficiently narrow distribution cone C relative to the opening 5 of the container 2 to be treated so that at least a predetermined quantity of the dispensed treatment substance 13 can be found inside the cavity 16 of the container 2 positioned under the outlet orifice 19 of the metering chamber 16. This ensures that the container 2 in question receives at least a predetermined quantity of the selected treatment substance 13 sufficient to obtain the desired level of treatment of said container 2.
- the metering chamber 16 is shaped and configured in such a way that the dispensing cone C is sufficiently narrow relative to the opening 5 so that substantially all of the quantity metered and dispensed by the metering chamber 16 can be found inside the cavity 4 of the container 1.
- said distribution cone C has a transverse section, included in a plane in which is inscribed the opening 5 of the container 2, which is of smaller dimensions.
- distributed cone is not to be considered, in the context of the invention, according to a strict mathematical definition of the term “cone”, but that one preferably understands by “distribution cone”, a fictitious envelope (whether conical, frustoconical, or even ideally substantially cylindrical) inside which is contained substantially all of the quantity of treatment substance 13 dosed and distributed by the dosing chamber 16 in the direction of the cavity 5 of the container 2. This avoids any problematic dispersion of treatment substance 13 on the ring and / or on the outer face 7 of the wall 3 of the container 2, or even next to said container 2.
- the installation 1 may comprise an outlet nozzle 22, arranged axially below and opposite the outlet orifice 19 of the metering chamber 16 and of the lower shutter 21, the latter then being interposed between the chamber. 16 dosing and the outlet nozzle 22.
- an outlet diameter advantageously less than or equal to the respective diameter of the first portion 17A of course, such a nozzle 22 makes it possible, if necessary, to further improve the precision of distribution of the substance 13 of treatment, in particular by limiting any effect of spatial dispersion of the treatment substance 13 which could be due to the configuration and operation of the lower shutter 21.
- the installation 1 comprises a frame 24, that is to say a support structure, intended to be immobilized relative to the ground, and the metering chamber 16 is immobilized relative to said frame 24.
- the metering chamber 16 can be immobilized relative to the ground, in particular during the operation of the installation 1 (and this both in translation and in rotation), the upper 20 and lower 21 shutters respectively remaining in position at the level. inlet 18 and outlet 19 of the metering chamber 16.
- Such a fixed, immobile nature of the metering chamber 16 contributes to the simplicity of design and implementation of the latter, to its robustness and its operational reliability, to the precision of the metering of the substance 13 for treatment by the metering chamber 16, as well as the speed and the spatial precision of the distribution of said treatment substance 13 inside the container 2 to be treated.
- the absence of movement of the metering chamber 16 contributes to limiting the risk of particles, in particular metallic particles, detaching by friction of the metering chamber 16 with the substance 13 of treatment when the grains or crystals of the latter are particularly hard and abrasive, and therefore limit the risk of contamination of the container 2 by such particles.
- the installation 1 advantageously comprises means for actuating the upper 20 and lower 21 shutters, configured to actuate the opening, respectively the closing, of said upper 20 and lower shutters 21.
- said means of actuation are designed and configured to actuate the opening (respectively closing) of the upper 20 and lower 21 shutters asynchronously, sequentially.
- the opening (respectively the closing) of the upper shutter 20 is therefore not simultaneous, concomitant, with the opening (respectively the closing) of the lower shutter 21.
- the actuating means of the upper 20 and lower 21 shutters can be designed and configured to simultaneously actuate the opening of the upper shutter 20 and the closing of the lower shutter 21, so that the internal recess 17 of the dosing chamber 16 is never in free communication with the exterior simultaneously through the inlet 18 and outlet 19 ports of the metering chamber 16.
- the means for actuating the upper 20 and lower 21 shutters are, on the contrary, designed and configured to actuate the opening, respectively the closing, of said upper 20 and lower 21 shutters simultaneously, synchronously.
- the opening (respectively closing) of the upper shutter 20 is therefore concomitant with the opening (respectively the closing) of the lower shutter 21.
- the upper shutter 20 retains outside of the dosing chamber 16 the treatment substance 13 coming from the source 12.
- this quantity of treatment substance 13 thus dosed and compacted then leaves the distribution chamber 16 through the outlet orifice 19 of the latter and falls, from substantially straight, vertical, in the direction of the opening 5 of the container 2 to be treated positioned under the outlet orifice 19, in the form of a dose of compact treatment substance 13 with low spatial dispersion.
- a new quantity of treatment substance 13 enters the metering chamber 16 through the inlet port 18 of the latter.
- the feeding and emptying of the metering chamber 16 with the treatment substance 13 can be carried out simultaneously, so that a plurality of containers 2 can be treated successively in this way. high rate, with one and the same metering chamber 16, without therefore having to resort to at least two metering chambers, one being supplied with substance 13 of treatment, while the other distributes into the container the substance 13 of treatment it contains.
- Each of the upper 20 and lower 21 shutters advantageously comprises a shutter element 25, 26 which is movably mounted or mounted within a shutter body fixed to (or formed at least in part by) the metering chamber 16, and which is able to move between at least one open position in which the closure element is positioned outside the flow of treatment substance 13 so as to allow the passage of the substance 13 through the inlet orifice 18 or corresponding outlet 19, and a closed position in which the closure element 25, 26 is on the contrary positioned across the flow of treatment substance 13 so as to interrupt the latter and prevent the passage of the substance 13 through the corresponding inlet 18 or outlet 19.
- the respective closure element 25, 26 of the upper 20 and lower 21 shutters is designed to move in a rectilinear movement in direction B-B ', CC' substantially orthogonal to an average direction of fall (average direction of flow) of the treatment substance 13 through the metering chamber 16, which facilitates the design of the dispensing means 15 and allows rapid opening / closing of the metering chamber 16.
- said mean direction of fall corresponds to the first axis A-A 'of vertical extension of the metering chamber 16.
- the respective closure element 25, 26 of the upper 20 and lower 21 shutters comprises a pair of coplanar scoops 25A, 25B, 26A, 26B (or hatches) mounted movable in mirror relation to each other.
- the upper 20 and lower 21 shutters thus form double-scoop guillotine valves (or double-blade knife valves).
- a "double shovel" configuration advantageously allows, for a given area of inlet 18 or outlet 19, to halve the time required to open, respectively to close, the inlet 18 or outlet 19 by the shutter 20, 21.
- the use of such a shutter element 25, 26 with double scoops 25A, 25B, 26A, 26B, in particular with regard to the lower shutter 21, advantageously allows opening / closing of the shutter 20, 21 centered on the orifice 18, 19 corresponding to the metering chamber 16, which makes it possible to limit the disturbance of the flow of the treatment substance 13, and therefore contributes to guaranteeing excellent precision in the distribution of the substance 13 of treatment in the container 2 to be treated.
- the means for actuating the upper 20 and lower 21 shutters are mutualised, that is to say they are common to each of said upper 20 and lower 21 shutters, in particular in order to simplify the design of the means of distribution 15.
- the actuating means are designed and configured to actuate the opening (respectively the closing) of the upper 20 and lower 21 shutters simultaneously, and the shutter element 25 , 26 of each of said shutters 20, 21 is designed to move in a rectilinear movement in direction B-B ', C-C' substantially orthogonal to the mean direction of fall of the treatment substance 13 through the dosing chamber 16 , and comprises a pair of coplanar shovels 25A, 25B, 26A, 26B mounted to be movable in mirror relation to one another.
- said actuating means are mutualized here, as mentioned above, and advantageously comprise: a pair of left 27A and right 27B spreaders, which are mounted in rectilinear linear translation with respect to the metering chamber 16 and which are secured to o a left shovel 25A, respectively to a right shovel 25B of the shutter element of the upper shutter 20, and to a left shovel 26A, respectively to a right shovel 26B of the element of closing the lower shutter 21, a pair of left 28A and right 28B levers, which are mounted to pivot relative to the metering chamber 16, and one end of which is connected to the left lifter 27A, respectively to the right lifter 27B, and two pairs of right 29A and left 29B electromagnets, each positioned at an opposite end of the left 28A and right 28B levers, so as to cause a pivoting of the levers 28A, 28B and a corresponding translation of the spreaders 27A, 27B and shovels 25A, 25B, 26A, 26B, when said electromagnets
- the lifting beams 27A, 27B could be mounted to pivot. relative to the metering chamber 16, so as to simultaneously actuate the opening of the upper shutter 20 and the closing of the lower shutter 21 and vice versa.
- suitable configurations of means for actuating the upper 20 and lower 21 shutters may be considered, depending in particular on the type and shape of the shutter element of said shutters, as well as the opening / closing kinematics. chosen.
- the installation 1 comprises a means 29 for pre-dosing the treatment substance 13, which is positioned between the source 12 of treatment substance 13 and the dosing chamber 16.
- the pre-metering means 29 Supplied by the source 12 of treatment substance 13, the pre-metering means 29 is provided to itself supply the metering chamber 16 with a pre-metered quantity of said treatment substance 13.
- the metering chamber 16 is therefore not supplied directly by the source 12 but, in an indirect and controlled manner, by the pre-metering means 29.
- the implementation of such a pre-metering means 29 upstream of the metering chamber 16 makes it possible to further improve the precision of the metering of the quantity of treatment substance 13 dispensed, by controlling in a controlled manner the quantity of treatment substance 13 received by the metering chamber 16.
- the pre-metering means 29 comprises a vibrating conveyor 30 configured to supply the treatment substance 13 from the source 12 of substance 13. treatment to the metering chamber 16.
- the vibrating conveyor 30 typically comprises a corridor 31, for example in the form of a rectilinear trough, to guide the treatment substance 13, and a vibrator (for example electric) provided to transmit to the corridor 31 oscillations or vibrations, the frequency of which is imprinted. an advance movement to the treatment substance 13 present in the lane.
- the pre-metering means 29 then also comprises control means (not shown) of the vibrating conveyor 30, which are designed and configured to control the duration and the frequency of vibration of the vibrating conveyor 30, in particular so as to finely control the quantity of treatment substance 13 delivered to the chamber 16 by the vibrating conveyor 30.
- control means not shown
- an upstream end 32 of the vibrating conveyor 30 is thus positioned below a discharge orifice of the hopper 14, to receive therefrom the treatment substance 13 and bring it to direction of the dosing chamber 16.
- a vibrating conveyor 30 advantageously makes it possible, over a given duration of supply to the metering chamber 16, to supply the latter in a substantially continuous and controlled manner, the treatment substance 13 being spread out in a layer of relatively constant thickness along the corridor under the effect of vibrations imparted to the latter.
- modulating the duration and the frequency of vibration of the vibrating conveyor 30, it is thus possible to parameterize, to dose, in a particularly fine manner the quantity of treatment substance 13 (for example, of the order of a few tens of milligrams) to dispense into the container 2 to be treated via the metering chamber 16.
- a vibration-absorbing material is placed below the, and in contact with the, corridor of the vibrating conveyor 30.
- This material which can typically be in the form of a foam (for example polyurethane or polyethylene) , makes it possible to attenuate at least locally the amplitude of the vibrations.
- a vibration-absorbing material makes it possible to further improve the homogeneity of the thickness of the layer of treatment substance 13, by limiting the risk of formation, along the length of the corridor of the vibrating conveyor 30, excess areas and areas lacking of treatment substance 13 by generating waves of grains of treatment substance 13 within the vibrating corridor.
- the presence of the vibration-absorbing material advantageously makes it possible to “smooth” this undulating phenomenon and to ensure a particularly stable and constant supply of the metering chamber 16 with treatment substance 13.
- a conveyor or screw conveyor could possibly be implemented instead of the vibrating conveyor 30 envisaged above.
- a vibrating conveyor 30 proves, on the one hand, to be more efficient as regards the precision of the pre-metering of the treatment substance 13 (in particular for the metering of quantities of a few tens of milligrams) and, of on the other hand, more robust and more reliable, in that it presents in particular no risk of seizing of moving parts.
- the installation 1 comprises a funnel 33, positioned below an outlet 34 of the pre-metering means 29, and for example below a downstream end 35 of the vibrating conveyor 30, to receive from said pre-dosing means 29 a pre-dosed amount of said treatment substance 13.
- the funnel 33 is provided with a discharge port 36, typically opposite a supply port 37 by the pre-metering means 29, which discharge port 36 is connected to the inlet port 18 of the metering chamber 16 via the upper shutter 20.
- the upper shutter 20 is interposed between the discharge orifice 36 of the funnel 33 and the inlet orifice 18 of the dosing chamber 16, so as to intercept the flow of treatment substance 13 leaving the funnel 33, and thus prohibit / authorize the supply of the dosing chamber 16 through the funnel 33.
- the funnel 33 thus makes it possible to collect the treatment substance 13 pre-dosed by the pre-dosing means 29, and which can leave the latter with a certain spatial dispersion, in order to collect it at the level of the base of the funnel 33 and to Then direct it in a channeled manner towards the inlet port 18 of the metering chamber 16.
- the outlet 34 of the pre-metering means 29, and in particular the downstream end 35 of the vibrating conveyor 30, is positioned at a height h2 of the supply orifice 37 which is between 5 and 20 mm.
- the treatment installation 1 may be of interest for the treatment of a glass container 2 which remains stationary relative to the distribution means 15 of the treatment substance 13 while the latter is in operation.
- said installation 1 is preferably designed to be implemented for the treatment of a glass container 2 moving relative to the distribution means 15, and in particular relative to the metering chamber 16 of the latter, while the distribution means 15 for its part remains stationary in the terrestrial frame of reference.
- the glass container 2 can be placed on a conveyor 38, with its bottom 8 resting on the conveyor 38 and its opening 5 facing upwards.
- the metering chamber 16 of the dispensing means 15 is for its part arranged above and facing the conveyor 38 so that the outlet orifice 19 of the metering chamber 16 can be positioned above and facing the opening 5 of the container 2 to be treated when the latter is set in motion by the conveyor 38 (FIG. 1).
- the installation 1 can, according to a variant, comprise such a conveyor 38 (for example with belt or with rollers).
- the installation 1 may not comprise, as such, a conveyor 38, but on the other hand be dimensioned and configured so as to be able to be arranged and implemented in combination with such an external conveyor 38.
- the installation 1 comprises a means 39 for detecting the glass container 2, which is connected to the actuating means of the lower shutter 21 to control the opening of the lower shutter 21 only when the container 2 is positioned under the metering chamber 16, and preferably below and facing the outlet opening 19 of the latter.
- the lower shutter 21 can advantageously be kept in the closed configuration in the absence of a container 2, and the distribution means 15 of the installation 1 therefore does not distribute the treatment substance 13 via the chamber 16. dosing in the absence of container 2 below the latter. This avoids unnecessary dispensing of treatment substance 13.
- the detection means 39 is configured to detect the actual presence of a glass container 2 under the metering chamber 16, and preferably below and opposite the outlet orifice 19 of the latter.
- said detection means 39 is configured to detect the arrival of the container 2 on the conveyor 38, upstream of the metering chamber 16 and preferably upstream of the outlet orifice 19 of the latter, that is to say before said container 2, moved by the conveyor 38, actually arrives below the metering chamber 16 and preferably below and opposite the outlet orifice 19 of the latter.
- the installation 1 advantageously comprises a control unit 40 which is connected, mechanically or electrically, on the one hand to the detection means 39 of the container 2, and on the other hand to the actuating means of the lower shutter 21, to synchronize the opening of the lower shutter 21 with the arrival of the container 2 under the metering chamber 16, and preferably below and opposite the outlet orifice 19 of the latter.
- Such synchronization can typically be obtained using a timer and in particular from the knowledge of the distance separating the detection zone of the container 2 by the detection means 39 from the position of the outlet orifice 19 of the metering chamber 16, the speed of movement of the container 2 on the conveyor 38, as well as the dimensions of the container 2.
- the detection means 39 is an optical barrier (or light barrier) and comprise either a light beam emitter (for example a laser, visible or infrared beam) positioned opposite a photoelectric cell, or a detection cell. comprising both a light beam emitter (for example a laser beam, visible or infrared) and a photoelectric cell and a light reflector positioned opposite a photoelectric cell, as illustrated in Figures 1 and 2.
- the detection cell 41 and the reflector 43 are advantageously positioned on either side. another of the path of movement of the container 2, at a known distance from the metering chamber 16, and preferably from the outlet orifice 19 of the latter.
- the detection cell 41 emits a light beam 42 (shown in dotted lines in FIG.
- the control unit 40 controls the opening of the lower shutter 21 by means of the actuating means of the latter, that is to say immediately (in the case of detection of the actual presence of a glass container 2 below the outlet orifice 19 of the metering chamber 16), or according to a predefined time delay (in the event of detection of the presence of a glass container 2 upstream of the outlet 19 of the metering chamber 16).
- such a detection means 39 of the optical barrier type will be designed and arranged so that the emitted light beam is interrupted by the neck 10 or the ring 11 of a container 2, and not by the body of the latter. , so as to allow finer synchronization of the operation of the lower shutter 21, and therefore a more precise distribution of the treatment substance 13 in the cavity 4 of the container 2, when the latter arrives below the outlet orifice 19 of the dosing chamber 16.
- detection means not necessarily optical, could be considered (proximity sensors, weight sensors, etc.).
- the installation 1 preferably comprises a central control unit 44, which is connected to said detection means 39 of the container 2 and to means for controlling the pre-dosing means 29 to start the pre-dosing means 29 at the time where the container 2 is detected upstream of the outlet 19 of the metering chamber 16.
- Said central control unit 44 may possibly be confused with or include the control unit 40 mentioned above.
- the central control unit 44 is therefore advantageously connected on the one hand to said detection means 39 of the container 2 and on the other hand to the control means of the vibrating conveyor 30, so as to put the vibrating conveyor 30 in vibration, at a predefined frequency and preferably for a predefined duration, as soon as the container 2 is detected upstream upstream of the outlet orifice 19 of the metering chamber 16.
- Such anticipation of the pre-dosing of the treatment substance 13 by the pre-dosing means 29 helps to further improve the rate of distribution of the treatment substance 13 by the installation 1, and therefore the rate of treatment, while at the same time ensuring a particularly precise dosage of the quantity of treatment substance 13 thus distributed.
- the invention also relates, as such, to a method of treating the inner face 6 of the wall 3 of a glass container 2 (such as a flask), which wall 3, in accordance with description of said container 2 which was given above - defines a reception cavity 4 for a product and an opening 5 giving access to said reception cavity 4.
- the treatment method according to the invention is preferably intended to be implemented using a treatment installation 1 in accordance with the invention, such as the latter was presented above.
- the treatment installation described above is advantageously intended to implement the treatment method according to the invention.
- the characteristics, definitions, effects and advantages described above in connection with the treatment installation advantageously apply mutatis mutandis to the treatment process according to the invention, and vice versa.
- the treatment installation according to the invention is obviously not limited to the sole implementation of the treatment method according to the invention, and the latter, in return, is not limited to an implementation. works using only a treatment facility as described above.
- the treatment method according to the invention comprises the supply of a source 12 of a powdery or granular treatment substance 13, which source 12 and treatment substance 13 are advantageously in accordance with the description which has been made above. in connection with the treatment facility 1.
- said source 12 may comprise a reservoir or a hopper 14, capable of receiving and storing at least temporarily a certain amount of ready-to-use treatment substance.
- the source 12 could comprise a device for manufacturing or preparing in situ of said treatment substance 13.
- Said method also comprises a step of distributing said treatment substance 13 inside the receiving cavity 4 of the receptacle 2.
- said distributing step is carried out using a distribution means. 15 comprising at least one metering chamber 16 which extends between an inlet port 18 supplied by said source 12 of treatment substance 13 and an opposite outlet port 19 positioned above, and preferably opposite, the 'opening 5 of the container 2, as well as an upper shutter 20 (or upper valve) and a lower shutter 21 (or lower valve) of the metering chamber 16 positioned in a stepped manner respectively at the level of the inlet port 18 and the outlet 19 of the metering chamber 16.
- said dispensing step is carried out using a dispensing device 15, metering chamber 16 and upper 20 and lower 21 shutters in accordance with those of the installation 1 according to the invention.
- a dispensing device 15 metering chamber 16 and upper 20 and lower 21 shutters in accordance with those of the installation 1 according to the invention.
- the implementation of such a metering chamber 16 and such upper 20 and lower 21 shutters, in accordance with the invention makes it possible to dose and distribute a precise, rapid and efficient manner.
- certain quantity of treatment substance 13 in a container 2 to be treated the opening 5 of which is positioned below the outlet orifice 19 of the metering chamber 16.
- the metering chamber 16 preferably remains stationary (in the terrestrial frame of reference, both in translation and in rotation) during the treatment of the container 2, the upper 20 and lower 21 shutters for their part remaining positioned at the level of the orifices. inlet 18 and outlet 19 of the metering chamber 16.
- the metering chamber 16 can be mounted stationary on a frame 24, which frame 24 is itself immobilized with respect to the ground.
- the treatment method may be of interest for the treatment of a glass container 2 which remains stationary relative to the distribution means 15 of the treatment substance 13 in operation of the latter.
- said treatment method more preferably relates to a glass container 2 which, at least during the aforementioned dispensing step, is in motion relative to the dispensing means 15, and in particular relative to the metering chamber 16. of the latter, while the distribution means 15 remains stationary in the terrestrial frame of reference.
- the glass container 2 can be placed on a conveyor 38, with its bottom 8 resting on the conveyor 38 and its orifice 5 facing upwards, the metering chamber 16 of the distribution means 15 being arranged above and in view of the conveyor 38 so that the outlet 19 of the metering chamber 16 comes above and opposite the opening of the container 3 to be treated when the latter is set in motion by the conveyor 38.
- each of the upper 20 and lower 21 shutters comprises a shutter member 25, 26 which moves in a rectilinear movement in a direction substantially orthogonal to an average direction of fall (average direction of flow) of said substance 13 of treatment at through the metering chamber 16.
- said closure element 25, 26 comprises a pair of coplanar shovels 25A, 25B, 26A, 26B mounted to be movable in mirror with respect to one another.
- the shovels 25A, 25B, 26A, 26B of each pair of shovels 25A, 25B, 26A, 26B thus move away from each other, by translation in the same plane, at the same speed and along the same length of stroke, to bring the corresponding shutter 20, 21 into the open configuration and thus allow the passage of the treatment substance 13 through the shutter 20, 21.
- the shovels 25A, 25B, 26A, 26B of each pair of shovels 25A, 25B, 26A, 26B approach each other, in the same way, to bring the corresponding shutter 20, 21 into the closed configuration and thus shut off the corresponding inlet 18 or outlet 19 of the metering chamber 16.
- the distribution means 15 implemented to allow the distribution of the treatment substance 13 can advantageously comprise actuation means upper 20 and lower 21 shutters designed and configured to actuate the opening, respectively closing, of the upper 20 and lower 21 shutters simultaneously, as described above in connection with the treatment installation 1.
- the opening of the lower shutter 21 is controlled only when the container 2 is positioned under the metering chamber 16, and more preferably still below and opposite the outlet orifice 19 of the latter, from so that the metering chamber 16 does not deliver the treatment substance 13 in the absence of the container 2 to be treated.
- the step of dispensing the treatment substance 13 is advantageously carried out only in the presence of a glass container 2 positioned under the metering chamber 16 of the dispensing means 15, which makes it possible to avoid dispensing. unnecessary substance 13 processing.
- the treatment method can implement as such a detection means 39 of the container 2 (such as an optical barrier), which is connected to the actuating means of the lower shutter 21 to control the opening.
- the treatment method preferably comprises an operation of pre-dosage of the treatment substance 13 originating from the source 12. of treatment substance 13, to supply the metering chamber 16 with a pre-metered quantity of said treatment substance 13.
- the dosing chamber 16 does not receive the treatment substance 13 in a massive manner, directly from the source 12 of the treatment substance 13, but on the contrary receives, in a controlled and regulated manner, a pre-dosed quantity of said substance 13. treatment.
- said pre-dosing operation is carried out using a pre-dosing means 29 in accordance with that described above in connection with the treatment installation 1.
- said pre-dosing step is advantageously carried out using a vibrating conveyor 30, such as that described above, which brings said treatment substance 13 from said source 12 of treatment substance 13 to chamber 16 of dosage.
- a vibrating conveyor 30 is particularly well suited in the case where the treatment substance 13 is powdery or granular, advantageously making it possible, over a given duration of supply of the metering chamber 16, to supply the latter. in a substantially continuous and controlled manner.
- the frequency and duration of vibration of the vibrating conveyor 30 By modulating the frequency and duration of vibration of the vibrating conveyor 30, it is possible to parameterize, pre-dose, in a particularly fine manner the quantity of treatment substance 13 (for example, of the order of a few tens of milligrams) to be dispensed into the container 2 to be treated via the metering chamber 16.
- the pre-dosing operation could nevertheless be carried out differently, depending in particular on the nature and quantity of the treatment substance 13 that is to be pre-dosed upstream of the dosing chamber 16.
- the treatment method comprises a step of detecting the container 2 to detect the arrival of the container 2 on said conveyor 38 upstream of the outlet 19 of the metering chamber 16, and to initiate the pre-metering operation when the receptacle 2 is detected upstream of the outlet orifice 19 of the metering chamber 16.
- a detection step can advantageously be implemented. implemented using the detection means 39 described above in connection with the treatment installation 1, and in particular an optical barrier.
- such anticipation of the step of pre-dosing the treatment substance 13 contributes to further improving the speed of distribution of the treatment substance 13, and therefore the rate of treatment, while ensuring a dosage particularly precise of the quantity of treatment substance 13 thus dispensed.
- the quantity of treatment substance 13 thus pre-dosed during the pre-dosing step is received by a funnel 33, an evacuation orifice 36 of which is connected to the inlet orifice 18 of the dosing chamber 16 via the upper shutter 20.
- the installation 1 and treatment method which have been described above can advantageously be implemented to carry out different types of treatment (doping, chemical hardening, etc.) of the inner face 6 of the wall of a glass container 2. , depending in particular on the nature of the treatment substance 13 used.
- said installation 1 and method more specifically constitute, respectively, installation 1 and dealkalization treatment method of the inner face 6 of the wall 3 of the glass container 2. It is understood, in this case, that the glass of said container 2 concerned is then a glass containing at least one alkaline species, such as sodium in particular.
- soda-lime-silica glass receptacle so-called “Type III” glass
- a borosilicate glass receptacle (“Type I” glass)
- such a dealkalinization treatment aims to extract, typically to a depth of several tens of nanometers, the alkali ions (and in particular the sodium ions) present in the glass in the vicinity of the surface of the inner face 6 of the glass. the wall 3 of the container 2.
- the glass in the vicinity of the surface of the inner face 6 of the wall 3 of the container 2 is thus, preferably significantly, depleted of alkali ions.
- the treatment substance 13 (or dealkalinization substance) is more specifically intended to react hot, under the effect of heat, to cause dealkalization of the glass, typically in the vicinity of the surface of the inner face 6 of the wall 3.
- said inner face 6 is then carried, before or after the distribution of the treatment substance 13 inside the cavity 4 of the container 2, at a processing temperature sufficient to cause the reaction of the processing substance.
- It may be a treatment substance 13 which, as such, is capable of itself coming into direct contact with the hot inner face 6 of the wall 3 of the container 2 in order to react, under the effect of heat, with one or more alkaline species present in the glass forming the wall 3 of the receptacle 2 or of a substance capable of decomposing under the effect of the heat prevailing in the cavity 4 of the receptacle 2, of the makes the temperature of the inner face 6 of the wall 3, to produce one or more new species or chemical substances, which (s) are able to come into contact with the surface of the inner face 6 of the wall 3 of the container 2 and reacting with one or more alkaline species present in the glass forming said wall 3 in order to obtain the desired dealkalization effect.
- said treatment substance 13 comprises a sulfur compound, and more preferably a compound containing sulfur combined with oxygen, in powdery (eg, crystalline) or granular form. More preferably still, said sulfur compound is an ammonium sulfate.
- a substance 13 of treatment based on powdery or granular ammonium sulphate is relatively easy and inexpensive to implement, and allows a particularly effective dealkalinization treatment of the glass container 2.
- other dealkalization treatment substances such as, for example, ammonium chloride or aluminum-ammonium sulfate
- the treatment installation 1 is then more specifically designed to distribute, in order to introduce, the treatment substance 13 into the receiving cavity 4 of the glass container 2, while the inner face 6 of the wall 3 of said container 2 made of glass is at a temperature of at least 350 ° C, preferably between 350 ° C and 850 ° C, preferably between 350 ° C and 800 ° C, more preferably between 350 ° C and 700 ° C, so as to allow the reaction of substance 13 under the effect of heat.
- the installation 1 can advantageously comprise a means for supplying a glass container 2 as described above, of which (at least) the inner face 6 of the wall 3 is at a temperature of at least 350 ° C, preferably between 350 ° C and 850 ° C, preferably between 350 ° C and 800 ° C, more preferably between 350 ° C and 700 ° C.
- this supply means may comprise a heating means, of any suitable known type (and for example, of the arch or oven type), designed to heat a pre-existing glass container 2 conforming to the above description, and whose inner side of the wall is initially at a temperature close (if not equal) to ambient temperature, so that the temperature of at least the inner side of the wall of the container reaches a value of at least 350 ° C, preferably between 350 ° C and 850 ° C, preferably between 350 ° C and 800 ° C, more preferably between 350 ° C and 700 ° C.
- the means for supplying the container 2 may comprise a system for collecting a glass container 2, in accordance with the description above, at the outlet of a hot forming machine of a glass container from a glass blank (for example, an IS machine), while said container 2 is still hot enough so that (at least) the inner face 6 of the wall 3 of said container 2 is at a temperature at least 350 ° C, preferably between 350 ° C and 850 ° C, preferably between 350 ° C and 800 ° C, more preferably between 350 ° C and 700 ° C.
- the installation 1 as such may not include such a means of supplying a receptacle 2 of which (at least) the inner face 6 of wall 3 is at a temperature of at least 350 ° C, preferably between 350 ° C and 850 ° C, preferably between 350 ° C and 800 ° C, more preferably between 350 ° C and 700 ° C, except for the conveyor 38 mentioned above, but it is nonetheless designed (in particular in terms of choice of materials, etc.) to be able to operate satisfactorily in the presence of 'a container 2 brought to such a temperature.
- the installation 1 as such could not be specifically designed to introduce the treatment substance 13 into the receiving cavity 4 of the glass container 2 while the inner face 6 of the wall 3 of the latter is at a temperature of at least 350 ° C, preferably between 350 ° C and 850 ° C, preferably between 350 ° C and 800 ° C, more preferably between 350 ° C and 700 ° C, but on the contrary while said inner face 6 is at room temperature.
- the installation 1 could then comprise a means for reheating the container 2, such as an annealing arch, positioned downstream of the distribution means 15, to bring the inner face 6 of the wall 3 of the container 2 to a temperature of at least 350 ° C, preferably between 350 ° C and 850 ° C, preferably between 350 ° C and 800 ° C, more preferably between 350 ° C and 700 ° C, once the treatment substance 13 dispensed into container 2.
- the step of distributing the treatment substance 13 in the receiving cavity 4 of the glass container 2 is carried out, according to a preferred variant, while the inner face 6 of the wall 3 of said glass container 2 is at a temperature of at least 350 ° C, preferably between 350 ° C and 850 ° C, preferably between 350 ° C and 800 ° C, more preferably between 350 ° C and 700 ° C.
- the treatment method can advantageously comprise a step of supplying a glass container 2, as described above, of which (at least) the inner face 6 of the wall 3 is at a temperature of at least minus 350 ° C, preferably between 350 ° C and 850 ° C, preferably between 350 ° C and 800 ° C, more preferably between 350 ° C and 700 ° C.
- a step of supplying the container 2 can comprise a heating operation, using any known suitable heating means, of a pre-existing glass container.
- the step of supplying the container 2 may comprise an operation of collecting a glass container 2 conforming to the description above, at the outlet of a hot forming machine of a glass container from a glass blank, while said container 2 is still hot enough so that (at least) the inner face 6 of the wall 3 of said container 2 is at a temperature of at least 350 ° C , preferably between 350 ° C and 850 ° C, preferably between 350 ° C and 800 ° C, more preferably between 350 ° C and 700 ° C.
- the method according to the invention therefore does not require the implementation of a particular heating operation, the inner face 6 of the wall 3 of the container 2 being brought to a temperature of at least 350 °.
- Such a forming operation can be carried out using any known installation for forming glass containers, such as for example an IS machine in the case of a container made of molded glass.
- the implementation of the method according to the invention is thereby simplified, in particular when the latter is implemented in an industrial context of manufacturing glass containers.
- the step of distributing the treatment substance 13 in the receiving cavity 4 of the glass container 2 can be carried out while the inner face 6 of the wall 3 of said glass container 2 is at room temperature.
- the treatment method may comprise, after said dispensing step, a step of reheating the container 2 in which the treatment substance 13 has been dispensed, to carry the inner face 6 of the wall 3 of said container 2. at a temperature of at least 350 ° C, preferably between 350 ° C and 850 ° C, preferably between 350 ° C and 800 ° C, more preferably between 350 ° C and 700 ° C.
- a reheating step can, for example, be carried out in an annealing arch at the within which the container 2 is placed at the end of said step of dispensing the treatment substance 13.
- the installation and treatment method could alternatively constitute the installation and method for treating doping, chemical hardening, etc., of the inner face 6 of the wall 3 of the glass container 2, depending in particular on the nature of the treatment substance 13 used, and this when one seeks in particular to dose and distribute accurately, quickly and efficiently a certain amount of the treatment substance 13 in a container 2 to be treated, the opening 5 of which is positioned below the outlet 19 of the metering chamber 16.
- the treatment installation 1 is preferably designed and arranged so that the outlet 19 of the metering chamber 16 (or, where appropriate, the lower end 23 of the nozzle 22 connected said outlet orifice 19) can be positioned above and facing the opening 5 of the container 2 (as envisaged above), at a distance d preferably between 1 cm and 20 cm, and more preferably still between 1 cm and 5 cm (for example, 15 mm) from said opening 5.
- the outlet orifice 19 of the metering chamber 16 (or, where appropriate , the lower end 23 of the nozzle 22 connected to said outlet orifice 19) is advantageously positioned above and opposite the opening 5 of the container 2 (as envisaged above), at a distance d preferably between 1 cm and 20 cm, and more preferably still between 1 cm and 5 cm (for example, 15 mm) of said opening 5.
- the invention finds its industrial application in the design, production and implementation of installations and methods for treating the inner face of the wall of glass containers, and in particular containers for pharmaceutical or diagnostic use.
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Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1913822A FR3104151B1 (fr) | 2019-12-05 | 2019-12-05 | Installation de traitement de recipients en verre comprenant une chambre de dosage de substance de traitement a double obturateur et procede afferent |
| PCT/FR2020/052207 WO2021111066A1 (fr) | 2019-12-05 | 2020-11-27 | Installation de traitement de recipients en verre comprenant une chambre de dosage de substance de traitement a double obturateur et procede afferent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| EP4069652A1 true EP4069652A1 (de) | 2022-10-12 |
Family
ID=69811154
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP20829951.1A Pending EP4069652A1 (de) | 2019-12-05 | 2020-11-27 | Anlage zur behandlung von glasbehältern mit einer kammer zur dosierung einer behandlungssubstanz mit doppelblende und zugehöriges verfahren |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US11926560B2 (de) |
| EP (1) | EP4069652A1 (de) |
| CN (1) | CN115003641A (de) |
| BR (1) | BR112022010829A2 (de) |
| CA (1) | CA3163750A1 (de) |
| FR (1) | FR3104151B1 (de) |
| WO (1) | WO2021111066A1 (de) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3105932B1 (fr) * | 2020-01-08 | 2021-12-17 | Sgd Sa | Procede de traitement de recipients en verre comprenant un controle optique d’une quantite de substance de traitement distribuee et installation de traitement afferente |
| DE102023116335A1 (de) * | 2022-06-23 | 2023-12-28 | Docter Optics Se | Verfahren zur Herstellung eines optischen Elementes aus Glas |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB531145A (en) * | 1939-07-13 | 1940-12-30 | United Glass Bottle Mfg Ltd | Improvements in or relating to methods and means for improving the durability of glass containers |
| GB1212881A (en) * | 1967-04-25 | 1970-11-18 | Glaverbel | Process for modifying glass and other materials |
| JP3047357B2 (ja) * | 1989-11-17 | 2000-05-29 | 浅井硝子株式会社 | コウジ酸配合化粧品用硝子瓶容器及びその製造方法 |
| CN1087326A (zh) * | 1992-11-16 | 1994-06-01 | 杭州人民玻璃厂 | 玻璃瓶内表面处理方法及自动投粉机 |
| JPH10212143A (ja) * | 1997-01-30 | 1998-08-11 | Toyo Glass Co Ltd | ノボラック樹脂系ポジ型ホトレジスト用ガラス容器及び内面処理方法 |
| US6722294B2 (en) * | 2002-08-06 | 2004-04-20 | Vitro Global, S.A. | Method and apparatus for feeding a pulverized material |
| US20090000336A1 (en) * | 2005-11-30 | 2009-01-01 | Gerresheimer Essen Gmbh | Inner Treatment Method and Device for the Inner Treatment of Glass Containers |
| WO2007118491A1 (de) * | 2006-04-13 | 2007-10-25 | Gerresheimer Essen Gmbh | Dosierverfahren und dosiergerät zur innenvergütung von glasbehältern |
| FR2944007B1 (fr) * | 2009-04-03 | 2012-06-08 | Sgd Sa | Procede de fabrication d'un recipient en verre et recipient correspondant. |
| CN101857356B (zh) * | 2009-04-07 | 2014-03-26 | 尼普洛株式会社 | 用于生产医用玻璃容器的方法和用于医用玻璃容器的内表面处理的燃烧器 |
| WO2011122067A1 (ja) * | 2010-03-30 | 2011-10-06 | 東洋ガラス株式会社 | ガラス容器の内面処理方法及びガラス容器 |
| WO2011125241A1 (ja) * | 2010-04-07 | 2011-10-13 | 東洋ガラス株式会社 | ガラス容器の内面処理方法及びガラス容器 |
| US9045364B2 (en) * | 2012-11-30 | 2015-06-02 | Owens-Brockway Glass Container Inc | Surface treatment process for glass containers |
| DE102014214083C5 (de) * | 2014-07-18 | 2021-04-08 | Schott Ag | Vorrichtung und Verfahren zum thermischen Behandeln eines ringförmigen Bereichs einer inneren Oberfläche eines aus einem Borosilikat-Rohrglas hergestellten Glasbehälters |
| US10065884B2 (en) * | 2014-11-26 | 2018-09-04 | Corning Incorporated | Methods for producing strengthened and durable glass containers |
| FR3031740B1 (fr) * | 2015-01-15 | 2017-02-24 | Sgd Sa | Recipient recouvert d'un revetement de protection et de retention, kit de fabrication d'un revetement de protection et de retention et procede de fabrication afferent |
| BR112017022783B1 (pt) * | 2015-04-24 | 2022-04-05 | Nipro Corporation | Processo para produzir um recipiente de vidro. |
| PL3238832T5 (pl) * | 2016-04-29 | 2024-06-03 | Wagner International Ag | Urządzenie transportujące proszek do transportowania proszku powlekającego do aplikatora proszku, instalacja do powlekania proszkowego i sposób obsługi urządzenia transportującego proszek |
| FR3052161B1 (fr) * | 2016-06-02 | 2018-06-29 | Sgd S.A. | Procede de formation d'un revetement barriere a la surface d'un recipient et installation afferente |
| WO2019049770A1 (ja) * | 2017-09-06 | 2019-03-14 | 富士フイルム株式会社 | 薬液収容体 |
| FR3078329B1 (fr) * | 2018-02-27 | 2022-09-30 | Sgd Sa | Procede de traitement d'un recipient a paroi en verre et installation afferente |
-
2019
- 2019-12-05 FR FR1913822A patent/FR3104151B1/fr active Active
-
2020
- 2020-11-27 CA CA3163750A patent/CA3163750A1/en active Pending
- 2020-11-27 BR BR112022010829A patent/BR112022010829A2/pt unknown
- 2020-11-27 EP EP20829951.1A patent/EP4069652A1/de active Pending
- 2020-11-27 WO PCT/FR2020/052207 patent/WO2021111066A1/fr not_active Ceased
- 2020-11-27 US US17/782,375 patent/US11926560B2/en active Active
- 2020-11-27 CN CN202080084517.7A patent/CN115003641A/zh active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| CN115003641A (zh) | 2022-09-02 |
| CA3163750A1 (en) | 2021-06-10 |
| US20230016184A1 (en) | 2023-01-19 |
| FR3104151A1 (fr) | 2021-06-11 |
| WO2021111066A1 (fr) | 2021-06-10 |
| US11926560B2 (en) | 2024-03-12 |
| FR3104151B1 (fr) | 2021-11-26 |
| BR112022010829A2 (pt) | 2022-08-23 |
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