EP4051436A1 - Vorrichtung und verfahren zur extraktion von magnetteilchen - Google Patents
Vorrichtung und verfahren zur extraktion von magnetteilchenInfo
- Publication number
- EP4051436A1 EP4051436A1 EP20796840.5A EP20796840A EP4051436A1 EP 4051436 A1 EP4051436 A1 EP 4051436A1 EP 20796840 A EP20796840 A EP 20796840A EP 4051436 A1 EP4051436 A1 EP 4051436A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- fluid
- chamber
- magnetic
- permanent magnet
- extraction device
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000006249 magnetic particle Substances 0.000 title claims abstract description 101
- 238000000605 extraction Methods 0.000 title claims abstract description 59
- 238000000034 method Methods 0.000 title claims description 23
- 239000012530 fluid Substances 0.000 claims abstract description 52
- 239000000843 powder Substances 0.000 claims abstract description 44
- 238000001914 filtration Methods 0.000 claims abstract description 41
- 239000007789 gas Substances 0.000 claims description 76
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 72
- 239000003345 natural gas Substances 0.000 claims description 34
- 230000008569 process Effects 0.000 claims description 19
- 238000004140 cleaning Methods 0.000 claims description 16
- 239000002245 particle Substances 0.000 claims description 16
- 239000011236 particulate material Substances 0.000 claims description 10
- 238000011144 upstream manufacturing Methods 0.000 claims description 8
- 230000000295 complement effect Effects 0.000 claims description 5
- 238000012545 processing Methods 0.000 claims description 5
- 239000003915 liquefied petroleum gas Substances 0.000 claims description 3
- 229930195733 hydrocarbon Natural products 0.000 description 12
- 150000002430 hydrocarbons Chemical class 0.000 description 12
- 239000004215 Carbon black (E152) Substances 0.000 description 10
- 239000007788 liquid Substances 0.000 description 8
- 230000004888 barrier function Effects 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 238000004891 communication Methods 0.000 description 4
- 230000005484 gravity Effects 0.000 description 4
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 3
- 229910000831 Steel Inorganic materials 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N carbon dioxide Natural products O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 239000006148 magnetic separator Substances 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 239000002002 slurry Substances 0.000 description 3
- 229910001220 stainless steel Inorganic materials 0.000 description 3
- 239000010935 stainless steel Substances 0.000 description 3
- 239000010959 steel Substances 0.000 description 3
- 239000013008 thixotropic agent Substances 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 239000004411 aluminium Substances 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 230000000712 assembly Effects 0.000 description 2
- 238000000429 assembly Methods 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 239000001569 carbon dioxide Substances 0.000 description 2
- 229910002092 carbon dioxide Inorganic materials 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000000356 contaminant Substances 0.000 description 2
- 230000003628 erosive effect Effects 0.000 description 2
- 239000000696 magnetic material Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 238000007790 scraping Methods 0.000 description 2
- 125000006850 spacer group Chemical group 0.000 description 2
- 238000005200 wet scrubbing Methods 0.000 description 2
- NLOAOXIUYAGBGO-UHFFFAOYSA-N C.[O] Chemical compound C.[O] NLOAOXIUYAGBGO-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- MBMLMWLHJBBADN-UHFFFAOYSA-N Ferrous sulfide Chemical class [Fe]=S MBMLMWLHJBBADN-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- UBAZGMLMVVQSCD-UHFFFAOYSA-N carbon dioxide;molecular oxygen Chemical compound O=O.O=C=O UBAZGMLMVVQSCD-UHFFFAOYSA-N 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 230000003749 cleanliness Effects 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 239000010779 crude oil Substances 0.000 description 1
- 238000013016 damping Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000003780 insertion Methods 0.000 description 1
- 230000037431 insertion Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 1
- 235000013980 iron oxide Nutrition 0.000 description 1
- VBMVTYDPPZVILR-UHFFFAOYSA-N iron(2+);oxygen(2-) Chemical class [O-2].[Fe+2] VBMVTYDPPZVILR-UHFFFAOYSA-N 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- JTJMJGYZQZDUJJ-UHFFFAOYSA-N phencyclidine Chemical class C1CCCCN1C1(C=2C=CC=CC=2)CCCCC1 JTJMJGYZQZDUJJ-UHFFFAOYSA-N 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 229910052761 rare earth metal Inorganic materials 0.000 description 1
- 150000002910 rare earth metals Chemical class 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000002990 reinforced plastic Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C—MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C1/00—Magnetic separation
- B03C1/02—Magnetic separation acting directly on the substance being separated
- B03C1/28—Magnetic plugs and dipsticks
- B03C1/284—Magnetic plugs and dipsticks with associated cleaning means, e.g. retractable non-magnetic sleeve
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C—MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C1/00—Magnetic separation
- B03C1/02—Magnetic separation acting directly on the substance being separated
- B03C1/28—Magnetic plugs and dipsticks
- B03C1/288—Magnetic plugs and dipsticks disposed at the outer circumference of a recipient
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C—MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C2201/00—Details of magnetic or electrostatic separation
- B03C2201/20—Magnetic separation of bulk or dry particles in mixtures
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C—MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03C2201/00—Details of magnetic or electrostatic separation
- B03C2201/28—Parts being designed to be removed for cleaning purposes
Definitions
- the invention relates to devices for extraction of magnetic detritus, especially black powder, from fluid flows, in particular from gases, most preferably from natural gas, and to processes for extracting magnetic detritus, especially black powder, from such fluid flows.
- Black powder is the commonly used term in the technical field that refers to solid materials that are present in natural gas handling systems.
- the black powder is typically suspended in (fast-)flowing natural gas streams and can collect in pipe lines and other components associated with natural gas handling systems.
- Black powder is typically comprised of very fine powder made up of very hard, abrasive particles of iron oxides, iron sulphides and further mineral contaminants, often having particle dimensions in the region of 10 microns or less. It can form through chemical reaction of the natural gas with the pipelines (which are mostly ferrous steel) and handling equipment, for example through a reaction of hydrogen sulphide with iron in the pipeline wall but may also be a by-product of microbes in the pipelines or result from mechanical erosion of ferrous materials such as the pipe line itself.
- Black powder can clog and damage instrumentation, sensors and valves, prematurely wear pipes and other components e.g. through corrosion; give rise to flow losses, and lead to a need to overly frequently replace or service components of the gas handling system, e.g. in the gas transport systems, refining systems, and end use systems. Its presence in a natural gas stream can also result in a lower quality end product for its intended use, e.g. in gas fired power stations.
- a further alternative technique that has been proposed is the use of a magnetic filter assembly.
- rod-like magnets extend into an incoming flow of natural gas, and magnetic particles of the black powder are captured directly onto the surface of the magnet assemblies. In that manner, magnetic particles of the black powder are extracted from the gas stream.
- US2010155336 AA discusses a pipeline filter with a pipeline mounting structure for mounting the pipeline filter in a pipeline, a screen support connected to the mounting structure and formed for releasably securing a screen filter to the pipeline filter and a magnetic filter support through which a magnetic filtering device is securable to the mounting structure. Cleaning again requires removal of filter and magnetic filtering device with associated shut down.
- WO 2016/200427 Al discusses a still further alternative magnetic black powder removal system in which black powder flowing within a hydrocarbon pipeline is converted into a magnetorheological slurry by implementing wet scrubbing in the hydrocarbon pipeline using particular thixotropic agents. A magnetic field is then applied to the magnetorheological slurry to control the flow of the magnetorheological slurry through the hydrocarbon pipeline.
- the use of wet scrubbing and the need to use special thixotropic agents can be disadvantageous.
- a magnetic particle (e.g. black powder) extraction device for extraction of magnetic particles (e.g. black powder) from a fluid flow.
- the device comprises a housing having a first chamber and a second chamber, and a separator between the first chamber and the second chamber.
- At least one permanent magnet is provided, preferably more than one permanent magnet.
- the first chamber comprises a fluid-inlet; a fluid-outlet; and a flow- path from the fluid-inlet to the fluid-outlet.
- the first chamber may thus form a flow- path for the fluid that is to be cleaned of magnetic particles.
- the second chamber has an inner volume of a dimension to receive the at least one permanent magnet.
- the second chamber may in that manner accommodate the at least one permanent magnet.
- the at least one permanent magnet is movable between a filtering position enveloped by the fluid flow-path and a non-filtering position that is remote from the flow-path.
- the filtering position is preferably proximate a second-chamber side of the separator, and the remote position is preferably more distanced from the second chamber side of the separator.
- Remote preferably refers to a position in which the permanent magnet is removed to the extent that it no longer exerts a significant magnetic field in the fluid flow-path.
- the permanent magnet During extraction use of the magnetic particle extraction device, the permanent magnet is positioned in its filtering position. In that position the permanent magnets magnetic field attracts and captures magnetic (i.e. permanently or non-permanently magnetic) particles of the black powder entrained in the passing fluid, on the first chamber side of the separator.
- magnetic i.e. permanently or non-permanently magnetic
- the captured particulates will continue to collect on the separator surface, in the magnetic field, until such time as the built-up particulates must be removed from the filtering device. At that time, flow of fluid may be stopped, and the permanent magnet may be moved from its filtering position to its non-filtering position remote from the flow-path, and remote from the separator collection surface, retreating inward to the second chamber.
- this clearing of accumulated black powder from the extraction element can be achieved by moving the permanent magnet from its filtering position enveloped by the flow-path to its non-filtering position in the second chamber.
- This has advantages associated with reduced downtime and lower risk of wear and damage but may also make more frequent cleaning of the magnetic filter elements economical allowing for smaller and/or less expensive filter components.
- the first chamber and the second chamber are substantially in pressure equilibrium, preferably wherein a pressure difference between the first chamber and the second chamber is maximally 500kPa, preferably 250kPa, preferably lOOkPa, preferably maximally 50kPa, and more preferably maximally lOkPa.
- a pressure difference between the first chamber and the second chamber is maximally 500kPa, preferably 250kPa, preferably lOOkPa, preferably maximally 50kPa, and more preferably maximally lOkPa.
- a strong (and thus bulky) separator to withstand the pressure and prevent escape of flow of the fluid and the magnetic particles (e.g. black powder) out of the first chamber and into the second chamber.
- the separator may be advantageous to have a relatively thin separator delineating the first chamber and second chamber.
- said at least one permanent magnet is positioned in the second chamber in both its filtering and non-filtering positions. This advantageously provides shielding of the magnet from direct contact with black powder by way of the separator even in its filtering position.
- the separator preferably forms a barrier to transfer of black powder from the first chamber to the second chamber.
- the separator is preferably thin.
- the separator may be from 0.5mm to 10mm thick, preferably from 0.5mm to 5mm thick, and preferably from 1mm to 3mm thick, adjacent to the permanent magnet when in its filtering position. Bringing the permanent magnet into proximity with second chamber side of the separator provides a magnetic field at the first chamber side surface of the separator causing collection of magnetic particles of black powder on the first chamber side surface of the separator, thus extracting it from the fluid stream.
- the separator itself is preferably non-magnetic, preferably being composed of stainless steel.
- Other non-magnetic materials including reinforced plastics, or aluminium are also contemplated as the material for the separator or in combination with stainless steel.
- the extraction device is provided with a pressure equalization conduit extending between the first and second chambers.
- the pressure equalization conduit may allow fluid (e.g. gas) to pass between the first and second chambers thereby allowing a substantial pressure equilibrium.
- the pressure equalization conduit preferably comprises a particulate filter such as a filter tube or pad commonly known in the art. Any flow of gas through the conduit will be low and so the filter element will not be exposed to high levels of detritus from the fluid.
- the pressure equalization conduit may pass through the separator or may be an independent conduit, possibly external to the housing.
- the separator may be provided with at least one sheath, preferably more than one sheath, as a protrusion of the separator.
- the sheath or sheaths may extend away from a generally planar base of the separator into the flow- path of the first chamber. This can increase the magnetic surface area to which the fluid is exposed as it flows past the separator surface.
- Each sheath may form a blind channel having internal dimensions to receive a bar or rod-shaped permanent magnet. That is, each sheath has a closed end toward a first chamber end and an open end toward a second chamber end, and a sidewall joining the closed end and the open end.
- the sheath is preferably elongate having a hollow inner volume complementary in shape to a rod or bar shaped permanent magnet.
- the permanent magnet is retractably positionable within the sheath via the open end. When in its filtering position within the sheath, the magnet exerts a magnetic field through the sheath’s sidewall and at a first chamber side surface of the sheath. This attracts magnetic particles and captures them upon the surface of the sheath. The magnetic particles do not come into direct contact with the permanent magnet because of the barrier function of the sheath.
- the permanent magnet Upon moving the permanent magnet to its non-filtering position at least partially withdrawn from the sheath, and thus distanced from the separator, the permanent magnet no longer exerts a magnetic field within the flow-path and the magnetic particles are no longer held against the separator (i.e. sheath) first chamber side surface. The magnetic particles can then be readily removed, even passively due to gravity, from the first chamber side surface of the separator.
- the permanent magnets are rods or bars, and may be a single magnet or more preferably comprised of a stack of magnets. In this manner a strong magnetic field can be closely concentrated around the rod or bar, as is known in the art of magnets.
- the black powder extraction device is provided with an array of permanent magnets retractably movable into the flow path of the first chamber, and preferably with an array of complementary sheaths as protrusions of the separator into the flow path, the sheaths accepting the array of permanent magnets.
- the housing and/or other components of device are able to withstand internal pressures of at least 1000 kPa, preferably at least 3000 kPa, more preferably at least 10,000 kPa, and more preferably at least 20,000 kPa.
- the housing may be constructed of an appropriately thick (carbon-)steel shell with appropriately pressure resistant gaskets, seals and flanges.
- the fluid inlet may be connected to a pressurized supply of fluid, preferably wherein the fluid is at a pressure of at least 1000 kPa, preferably at least 3000 kPa, more preferably at least 10,000 kPa, and more preferably at least 20,000 kPa.
- the fluid is a hydrocarbon gas, natural gas, methane oxygen, carbon dioxide, hydrogen or nitrogen.
- a diffuser or baffle may be provided in the fluid-inlet to disperse the incoming fluid flow across the magnetic filter for optimal black powder capture.
- the permanent magnet upon moving the permanent magnet to its non-filtering position, the permanent magnet no longer exerts a magnetic field within the flow-path and the magnetic particles are no longer held against the separator (e.g. the sheath outer surface) and can be readily removed.
- the separator e.g. the sheath outer surface
- this is achieved by halting flow along the flow path, e.g. by closing the fluid inlet, thereafter moving the permanent magnet or magnets to the non-filtering position and allowing the captured magnetic particles to fall under gravity from the separator surface.
- the first chamber is preferably provided with a a detritus collection area below the separator surface in the first chamber, preferably a sump.
- a detritus release outlet is provided in the detritus collection area for removal of detritus from the first chamber.
- the release outlet is preferably arranged in communication with the sump and is further preferably in communication with a pressure lower than that in the first chamber, preferably open to atmospheric pressure.
- the detritus release outlet can thus be opened so that back-pressure from the fluid pipeline will force the detritus in the sump through the release outlet for appropriate external collection and handling.
- a cyclone separator may be provided upstream of the fluid-inlet or downstream of the fluid-outlet.
- a mechanical filter may be provided upstream of the fluid-inlet or downstream of the fluid-outlet.
- a cyclone separator may be provided upstream of the fluid-inlet and a mechanical filter downstream of the fluid-outlet.
- the magnetic filter removes magnetic particles before they encounter the barrier filter, the barrier filter does not become clogged with such contaminants and therefore the usefulness of the barrier filter is increased. Furthermore, while the barrier filter may not retain particles below a certain size, the magnetic filtration is not size-dependent. The overall efficiency of the filtration system is therefore greatly improved with use of the magnetic filter.
- a particle extraction device for extraction of magnetic particles from a fluid, (e.g. a stream of natural gas), the extraction device comprising a housing having a fluid-inlet, a fluid-outlet, and a flow- path from the fluid-inlet to the fluid-outlet along which the fluid can flow.
- a pipeline for fluid is adjoined to the fluid-inlet and the fluid-outlet.
- a magnetic filter preferably an array of magnetic filter elements, comprising one or more permanent magnets.
- the magnetic filter further comprises one or more sheaths that impinge upon or extend into the flow-path, and into which the array of magnetic filter elements can be retractably positioned. The sheaths form a physical barrier around the magnetic filter elements. This can help to prevent, or prevent, black powder from contacting the magnetic filter elements directly.
- the magnetic filter preferably comprises an array of sheaths intruding into the flow-path, and a complementary array of permanent magnets retractably positioned within said sheaths.
- a process for extracting detritus, preferably black powder, from a fluid stream, for example natural gas comprises the steps of; a. providing at least one filter element, the filter element comprising a collection surface; b. providing a permanent magnet behind the collection surface to generate a magnetic field passing through the collection surface; c. passing a fluid containing magnetic particles through the magnetic field and trapping magnetic particles on the collection surface. d. moving the permanent magnet away from the collection surface to reduce or eliminate the magnetic field at the collection surface, and e. removing particles from the collection surface.
- the process may preferably be implemented using the devices and apparatuses as described herein.
- the flow speed passed the filter element is 25ms 1 or less, more preferably 15ms 1 or less, more preferably 10ms 1 or less, most preferably 5ms 1 or less.
- magnetic particles may be more readily extracted by the magnetic filter elements.
- the permanent magnet is shielded from direct contact with the magnetic particles by the filter element, the filter element forming separator membrane.
- the step of reducing or eliminating the magnetic field from the collection surface preferably comprises moving the permanent magnet away from the collection surface, preferably rearwardly away from the collection surface.
- a strong magnetic field at the collection surface of the filter element may provide for efficient and effective capture of magnetic particles.
- the fluid is passed through a cyclone cleaning system, preferably before or after step c.
- the fluid is passed through a mechanical filter, preferably before or after step c.
- the fluid is passed through a cyclone separator prior to step c. and passed through a mechanical filter after step c.
- the filter element is positioned in a housing, said housing comprising a fluid-inlet, a fluid-outlet, and a flow-path from the fluid-inlet to the fluid-outlet, the filter element extending into the flow-path, wherein the fluid-inlet is connected to a pressurized source of fluid containing magnetic particles, and the fluid-outlet is connected to additional gas processing equipment.
- the source of fluid may be at a pressure of at least 1000 kPa, preferably at least 3000 kPa, more preferably at least 10,000 kPa, and more preferably at least 20,000 kPa.
- the fluid is a hydrocarbon gas, natural gas, methane, oxygen, carbon dioxide, hydrogen or nitrogen.
- Removal of the collected particles from the filter element preferably comprises the steps of reducing or halting gas flow, reducing or removing the magnetic field at the collection surface, and thereafter allowing the particulate material to fall to a sump.
- the process may further comprise a step of providing a sump-outlet and ejecting magnetic material in the sump via the sump outlet under back-pressure from the fluid outlet.
- Gas in the present application refers to compositions that are predominantly in the gaseous state at the temperatures of pressures of use. Gas flows that include a minor weight portion of suspended solids or liquids, condensate or evaporated liquids, are considered to be gas flows within the meaning of the invention. For example, it is typical that a stream of natural gas, especially at its source, will contain a percentage of liquid hydrocarbons and/or water. Reference to gas thus includes instances in which the gas, especially if hydrocarbon gas, contains aerosolized aqueous or hydrocarbon liquids or separated aqueous or hydrocarbon liquids traveling along walls of a pipeline.
- the invention is preferably concerned with removal of magnetic particles from natural gas
- the invention may also concern removal of magnetic particles from other gas streams, for example from flows of methane, carbon dioxide gas, oxygen, hydrogen, nitrogen, and mixtures thereof, for example air.
- Preferred gases of the invention are methane, carbon dioxide gas, oxygen, hydrogen, nitrogen, and mixtures thereof, for example air.
- the fluid is natural gas and preferably that the process further comprises steps of processing the natural gas to provide power-station grade natural gas, domestic-grade natural gas, compressed natural gas, or liquefied petroleum gas.
- the apparatus described above is used for extraction of magnetic particles from a flow of liquid, for example for extraction of black powder from a flow of crude oil, or other liquid hydrocarbon streams.
- the various aspects of the invention discussed herein may provide for reliable extraction of magnetic particles (e.g. black powder) from a flow of fluid (e.g. natural gas), while at the same time avoiding the disadvantages of mechanical filter pads and the problems of cleaning of use of wetting/thixotropic agents found in the prior art.
- a flow of fluid e.g. natural gas
- FIG. 1 shows a separator system for extracting magnetic particles from a fluid flow
- FIG. 2 shows a side elevation of a single separator arrangement
- FIG. 3 shows a magnetic particle extraction device of the separator of figure 2
- FIG.4 shows a side elevation of the magnetic particle extraction device of figure 3
- FIG.5 is a cross-section of the magnetic particle extraction device of figure 3;
- FIG.6 is a cross-section of the magnetic particle extraction device of figure 4 along line A- A;
- FIG.7 is top view into a lower shell of the magnetic particle extraction device of figure 3;
- FIG.8 is a schematic illustration of magnetic fields in the view of figure 7;
- FIG.9A is a schematic illustration of magnetic particle extraction device with an array of magnets in a filtering position
- FIG.9B is a schematic illustration of magnetic particle extraction device with an array of magnets in a non-filtering position.
- FIG.10 shows a diffuser suitable to be positioned within a fluid-inlet of the magnetic particle extraction device of Figure 3.
- FIG. 1 shows a separator system 100 comprising a gas inlet header (or manifold) 20 providing pressurized gas to separator system inlet pipe spools 40; and a gas outlet header 30, that receives pressurized, cleaned gas from the separator system outlet pipe spool 50.
- the inlet pipe spools 40 are in communication with and provide the gas to inlets 65 of magnetic particle extraction devices 60.
- the outlets 66 of the magnetic particle extraction devices 60 connect to cyclone separators 90, downstream of the magnetic particle extraction devices 60.
- mechanical filters may be used in place of or in combination with the cyclone separators 90, downstream of the magnetic particle extraction devices 60. Further alternatively mechanical filters and/or cyclone separators 90 may be included upstream of the magnetic particle extraction devices 60. In some embodiments, the magnetic particle extraction devices 60 may be directly coupled to the gas outlet, that is without other intervening filters or separators.
- a source of upstream pressurized gas e.g. natural gas
- a source of upstream pressurized gas e.g. natural gas
- inlet header 20 from where it is then supplied via inlet pipe spools 40 to the magnetic particle extraction devices 60.
- magnetic particles are extracted from the gas.
- the system is preferably used for extracting black powder suspended in a hydrocarbon (e.g. natural gas) pipeline, preferably being an in-situ pipeline in service.
- the pipeline can be operational to transport hydrocarbons between locations.
- the gas passes from outlets of the magnetic particle extraction devices 60 downstream to the cyclone separators 90 where remaining particles in the gas (if any) are removed from the gas by cyclonic separation.
- the cleaned gas stream then passes to the outlet pipe spools 50, and outlet header 30 to exit the separator system.
- the outlet header 30 may be connected (directly or indirectly) to further transport gas pipelines, to gas handling equipment, to gas processing equipment, a gas compression system for provision of compressed natural gas or liquefied petroleum gas; to a power station; or to a domestic or industrial gas pipe network.
- three separator arrangements 80 are provided in parallel flow (as opposed to series flow).
- This preferred arrangement allows gas flow through one or two of the separator arrangements to be temporarily halted e.g. for cleaning operations, while maintaining continuous system gas flow through the remaining, open, separator arrangement(s).
- One or more inlet conduit valves 41, 42 and outlet conduit valves 43, 44 may be provided to selectively route the gas through one or more or all of separator arrangements. These valves may be operated manually or automatically via a pneumatic actuator or an electrical actuator.
- the separator system 100 could alternatively be provided with just two or more than three parallel separator arrangements.
- the separator system 100 may also comprise just one separator arrangement, without a parallel flow path, and in that case gas flow may be halted, or reduced in flow rate, during cleaning of maintenance of the separator arrangement.
- One of the separator arrangements shown in the system of figure 1 is illustrated in side elevation in figure 2.
- the gas flow enters via the header 20, and then follows a route passing through the magnetic particle extraction device 60, the cyclone separator 90, the outlet pipe spool 50, the inlet pipe spool 40, and then on to the outlet header 30 where it may recombine with gas from other parallel flow separator arrangements 80.
- the magnetic particle extraction device 60 included in the separator system 100 of claim 1 is shown in more detail in figures 3 to 7.
- the magnetic particle extraction device 60 is provided with a pressure vessel having a housing 61 comprised of a lower shell portion 62 generally defining a first (preferably lower) chamber 601 therein; and an upper shell 63 generally defining a second (or upper) chamber 602 therein.
- the lower shell 62 and upper shell 63 are separably attached at a pressure resistant flange 64.
- the pressure vessel 61 is preferably rated to withstand internal pressures of at least 1000 kPa, preferably at least 3000 kPa, more preferably at least 10,000 kPa, and more preferably at least 20,000 kPa, in line with an ability to withstand typical pressures that may be found in industrial scale natural gas pipelines.
- the lower shell portion 62 comprises a fluid-inlet 65 for receipt of a gas flow from an inlet pipe spool 40. There is further provided a fluid-outlet 66 for outlet of gas to an outlet pipe spool 50. A flow-path for gas is provided running from the fluid-inlet 65 to the fluid-outlet 66, through the interior of the lower shell 62 (first chamber).
- a pressure equalization conduit 69 is provided to allow for pressure equalization between the first chamber 601 and the second chamber 602.
- the pressure equalization conduit 69 in a simple form may be an open line allow fluid communication between the first chamber 601 and the second chamber 602.
- a filter element 70 e.g. a mechanical filter may be provided in the pressure equalization conduit 69 to prevent or reduce the passage of particulate material, e.g. particles of 3 micron or greater in a dimension, from the first chamber 601 to the second chamber 602.
- the illustrated magnetic particle extraction device 60 is provided with a lower preferably funnelled end, forming a sump 67 into which particulate material extracted from gas can fall under gravity during a cleaning operation.
- the sump 67 is further provided with a sump outlet 68, preferably in the form of a valve, which is selectively openable to release particulate material that has collected in the sump 67.
- the illustrated magnetic particle extraction device 60 is provided with an opening for receipt of lifting gear for affecting retractable movement of elements within the second chamber.
- the housing may be composed of steel or other known materials capable of withstanding pressures in use.
- FIG. 6 cross-sections of the magnetic particle extraction device 60 illustrated in figures 3 and 4 are provided illustrating the interior of the housing 61.
- the cross-section of figure 6 is a cross-section along the line A-A of figure 4.
- the interior of the housing 61 is generally divided into a first (lower) chamber 601 in the lower shell 62, and a second (upper) chamber 602 in the upper shell 63.
- the first chamber 601 and the lower chamber 602 are divided by a separator 603 delimiting the two chambers.
- the separator 603 comprises a separator plate and seals the chambers against exchange of particulate material and preferably also of liquids and gas.
- the separator has a first-chamber side 606 and a second chamber side.
- the separator 603 extends as a plurality of blind-tubes into the interior of lower shell 62, which impinge upon a gas flow-path running from the fluid-inlet 65 to the fluid-outlet 66.
- the blind-tubes form sheaths 604 having a closed end 610 toward the first chamber 601 and an open end 611 toward the second chamber 602, with a sidewall 612 extending therebetween.
- magnetic rods 605 can be inserted into sheaths 604 for a filtering position and operation and withdrawn from sheaths 604 for a non-filtering position and/or cleaning operation.
- a further inner-housing 608 may be provided in the second chamber 602, which may receive the retracted magnets 605, and provide additional protection against fouling of the magnets’ 605 surface.
- Figure 7 is a view from above, into the lower shell 62 with separator 603 in place showing open ends 611 of the sheaths 604 with magnets 605 inserted therein in a filtering position.
- the magnets 605 are sheaths 604 are arranged in two offset rows to provide a large area of surface contact with a gas passing from fluid-inlet 65 to fluid-outlet 66. A greater number of rows, or only a single row, or more or fewer magnets may be provided as needed.
- Figure 8 schematically illustrates the magnetic field generated about the magnets 605.
- the magnetic field extends through the sheaths 604 of the separator 603 and into a gas flow as it passes over the first chamber side surface 606 of the sheathes.
- the magnetic fields of the magnets preferably overlap, e.g. as illustrated to exposure substantially all flowing gas to the magnetic fields.
- the magnetic particle content of the gas at the fluid-outlet is less than 20% of the magnetic particle content of the gas at the fluid-inlet, by weight, preferably less than 5%, more preferably less than 1%.
- a diffuser 72 or baffle may be provided in the fluid- inlet 65 to disperse the incoming gas flow across the magnetic filter.
- An example of a suitable diffuser 72 that may be inserted or incorporated into the fluid-inlet 65 is shown in figure 9.
- the gas speed past the magnetic filter elements is 25ms 1 or less, more preferably 15ms 1 or less, more preferably 10ms 1 or less, most preferably 5ms 1 or less.
- the separator 603 is substantial enough to prevent ingress of particulate material to the second chamber 602, it is also preferably thin to avoid damping of the magnetic field when the magnets 605 are in place for filtering.
- the present invention advantageously allows for the separator 603 and its sheaths 604 to be thin despite the high pressures involved in industrial handling of natural gas streams. This advantage can be achieved by maintaining the second chamber 602 at about pressure equilibrium with the first chamber 601. The pressure differential across the separator 603 can so be minimized and consequently the separator 603 can be made thin without risk of physical collapse or a breach.
- the sheaths 604, and preferably all of the separator 603, is are non-magnetic. Suitable materials for the sheaths and separator are preferably stainless steel, and may also include plastics, or other non-magnetic metals such as aluminium. Hard materials are preferred to avoid erosion.
- a separator 603 provides for an advantageous cleaning of the magnetic particle extraction device 60 that is easy and/or speedy for an operator.
- extracted magnetic particles such as black powder can preferably be removed without any need to internally access the housing 61 or preferably without a need to directly access a rod magnet’s surface for wiping or scraping of extracted material therefrom.
- figures 9A and 9B This is schematically illustrated in figures 9A and 9B.
- the array of magnets 605 and sheaths 604 has been rotated by 90° about a vertical axis as compared to figure 8, for ease of explanation.
- the array of magnets 605 are in their filtering position, inserted within sheaths 604.
- the magnets 605 exert a magnetic field through a sidewall 612 of the sheaths 604 and into a gas flow passing from the fluid-inlet 65 to the fluid outlet 66 over the sheaths’ first chamber side surface 606.
- Magnetic particles suspended in a passing gas are thus extracted from that gas and held against the collecting surface 606.
- the pressures in the first chamber 601 and in the second chamber 602 are close to, or at, equilibrium so that there is only a small pressure differential across the separator 603, allowing the separator 603 to be thin.
- Operating pressures may be in the region of at least 3,000kPa, at least 6,000kPa, as much as 10,000 kPa, and possibly 20,000 kPa.
- gas flow through the magnetic particle extraction device 60 is greatly reduced or preferably halted using e.g. valves 41-44.
- the housing magnetic particle extraction device 60 remains under pressure, but there is a minimal or no flow of gas.
- the magnets 605 no longer exert a magnetic field within the gas flow path so that the captured magnetic particles are no longer held against the first chamber side surface 606 of the sheaths 604. Those magnetic particles then fall under gravity to the sump 67 where they are collected. Once the magnetic particles have fallen away from the sheaths 604 so that they are suitably clean, the array of magnets 605 is reinserted in the array of sheaths 604 and the gas flow restarted whereby filtering of gas can recommence.
- clearing of the extracted magnetic particles from the first chamber side surface of the separator’s 603 sheaths 604 can be done without depressurization, without disassembly and without exposure of the array of magnets 605 to the external environment. Downtime, complexity, risk of damage and wear can possibly be reduced.
- magnetic particles collected in the sump 67 can be expelled without disassembly or depressurization of the system.
- Sump 67 is provided with a magnetic particle release outlet 68.
- the outlet 68 comprises a valve leading to a lower pressure volume, such as atmospheric pressure.
- the magnetic particle release outlet 68 is closed to maintain pressure in the first chamber 601.
- the magnetic particle release outlet 68 can be opened so that pressure in the first chamber 601 drives magnetic particles in the sump 67 out via the magnetic particle release outlet 68.
- Removal of particles form the sump 67 may be carried out at as necessary, possibly at every cleaning operation of the sheaths 604, more preferably every 3 to 10 cleaning operations, or most preferably based on a weight or volume threshold as may be detected in the sump 67.
- a downwardly facing conical vane 89 is provided around the lower end of the array of sheaths 604.
- This vane 89 acts as a baffle obstructing return of particulate material from the lower part of the first chamber 601 to upper part of the first chamber 601. This can maintain cleanliness and prevent re pollution of gas passing along the flow-path between the fluid-inlet 65 and fluid-outlet 66
- the magnets 605 used in the invention are preferably elongate and constructed to provide a magnetic field along radially about the long axis.
- Such magnets are commercially available and are comprised of a plurality of magnets and soft ferrous metal spacers arranged in an alternating sequence to form a stack, adjacent magnets being arranged with like poles facing.
- a non-magnetic case may be provided sealed around the stack of magnets and spacers to create a rod-like magnet, which magnet 605 can then be used for retractable insertion into the sheaths 604 of the present invention.
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Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
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EP19206755.1A EP3815790A1 (de) | 2019-11-01 | 2019-11-01 | Vorrichtung und verfahren zum zuführen und transportieren von gegenständen |
PCT/EP2020/080515 WO2021084071A1 (en) | 2019-11-01 | 2020-10-30 | Magnetic particle extraction device and method |
Publications (1)
Publication Number | Publication Date |
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EP4051436A1 true EP4051436A1 (de) | 2022-09-07 |
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ID=68426221
Family Applications (2)
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EP19206755.1A Withdrawn EP3815790A1 (de) | 2019-11-01 | 2019-11-01 | Vorrichtung und verfahren zum zuführen und transportieren von gegenständen |
EP20796840.5A Pending EP4051436A1 (de) | 2019-11-01 | 2020-10-30 | Vorrichtung und verfahren zur extraktion von magnetteilchen |
Family Applications Before (1)
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EP19206755.1A Withdrawn EP3815790A1 (de) | 2019-11-01 | 2019-11-01 | Vorrichtung und verfahren zum zuführen und transportieren von gegenständen |
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WO (1) | WO2021084071A1 (de) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
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US12070756B2 (en) | 2016-06-30 | 2024-08-27 | Adey Holdings (2008) Limited | Magnetic rod guide for a filter |
TWI781820B (zh) * | 2021-11-10 | 2022-10-21 | 泰翰實業有限公司 | 流體物料磁性雜質分離機、總成及其方法 |
WO2023161660A1 (en) * | 2022-02-28 | 2023-08-31 | Adey Holdings (2008) Limited | Magnetic filter |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
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US20100155336A1 (en) | 2007-02-22 | 2010-06-24 | Simonson Roger M | Pipeline filter |
WO2009137930A1 (en) | 2008-05-13 | 2009-11-19 | Simonson Roger M | Pipeline magnetic separator system |
GB2476825B (en) * | 2010-01-12 | 2011-12-07 | Eclipse Magnetics Ltd | Magnetic filtration apparatus |
PL2834009T3 (pl) * | 2012-04-03 | 2018-05-30 | Spiro Enterprises B.V. | Układ obiegu płynu dla obiegowej ilości płynu zawierający magnetyczny separator do oddzielania zawieszonych cząstek mających ferromagnetyczne właściwości i odpowiedni sposób |
US9675979B2 (en) | 2015-06-08 | 2017-06-13 | Saudi Arabian Oil Company | Controlling flow of black powder in hydrocarbon pipelines |
GB201604280D0 (en) * | 2016-03-14 | 2016-04-27 | Eclipse Magnetics Ltd | Magnetic filtration apparatus |
NL2017443B1 (en) * | 2016-09-09 | 2018-03-15 | Mhd Tech B V | Device and method for magnetic separation |
-
2019
- 2019-11-01 EP EP19206755.1A patent/EP3815790A1/de not_active Withdrawn
-
2020
- 2020-10-30 WO PCT/EP2020/080515 patent/WO2021084071A1/en unknown
- 2020-10-30 EP EP20796840.5A patent/EP4051436A1/de active Pending
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EP3815790A1 (de) | 2021-05-05 |
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