EP2313319B1 - Procede de conditionnement de produit fluide dans un distributeur - Google Patents
Procede de conditionnement de produit fluide dans un distributeur Download PDFInfo
- Publication number
- EP2313319B1 EP2313319B1 EP09772731A EP09772731A EP2313319B1 EP 2313319 B1 EP2313319 B1 EP 2313319B1 EP 09772731 A EP09772731 A EP 09772731A EP 09772731 A EP09772731 A EP 09772731A EP 2313319 B1 EP2313319 B1 EP 2313319B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- reservoir
- fluid
- inert gas
- air
- vacuum
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Not-in-force
Links
- 239000012530 fluid Substances 0.000 title claims abstract description 84
- 238000000034 method Methods 0.000 title claims abstract description 24
- 230000003750 conditioning effect Effects 0.000 title description 10
- 239000011261 inert gas Substances 0.000 claims abstract description 71
- 238000004806 packaging method and process Methods 0.000 claims abstract description 16
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims abstract description 12
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229910052786 argon Inorganic materials 0.000 claims abstract description 6
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 4
- 239000003570 air Substances 0.000 description 39
- 238000007789 sealing Methods 0.000 description 11
- 239000007789 gas Substances 0.000 description 8
- 238000004321 preservation Methods 0.000 description 5
- 239000002537 cosmetic Substances 0.000 description 2
- 239000006071 cream Substances 0.000 description 2
- 238000002788 crimping Methods 0.000 description 2
- 239000000499 gel Substances 0.000 description 2
- 238000012858 packaging process Methods 0.000 description 2
- 238000010926 purge Methods 0.000 description 2
- 239000012080 ambient air Substances 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005429 filling process Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000011800 void material Substances 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B31/00—Packaging articles or materials under special atmospheric or gaseous conditions; Adding propellants to aerosol containers
- B65B31/02—Filling, closing, or filling and closing, containers or wrappers in chambers maintained under vacuum or superatmospheric pressure or containing a special atmosphere, e.g. of inert gas
- B65B31/025—Filling, closing, or filling and closing, containers or wrappers in chambers maintained under vacuum or superatmospheric pressure or containing a special atmosphere, e.g. of inert gas specially adapted for rigid or semi-rigid containers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
- B05B11/00—Single-unit hand-held apparatus in which flow of contents is produced by the muscular force of the operator at the moment of use
- B05B11/0005—Components or details
- B05B11/0097—Means for filling or refilling the sprayer
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
- B05B11/00—Single-unit hand-held apparatus in which flow of contents is produced by the muscular force of the operator at the moment of use
- B05B11/01—Single-unit hand-held apparatus in which flow of contents is produced by the muscular force of the operator at the moment of use characterised by the means producing the flow
- B05B11/02—Membranes or pistons acting on the contents inside the container, e.g. follower pistons
- B05B11/028—Pistons separating the content remaining in the container from the atmospheric air to compensate underpressure inside the container
Definitions
- the present invention relates to a fluid product conditioning method in a fluid dispenser comprising a reservoir filled with fluid product defining an opening and a fluid dispenser member such as a pump or a valve.
- the dispensing member is intended to be mounted in a sealed manner on the opening of the reservoir to thereby constitute the fluid dispenser.
- This type of dispenser is frequently used in the fields of cosmetics, perfumery or pharmacy to condition various fluid products, such as perfumes, creams, gels, lotions, or powders.
- Some fluid products are likely to deteriorate when in contact with the air. For example, they may dry out or oxidize.
- the documents are known EP-0 509 179 and EP-0 481 854 . These documents describe vacuum filling and sealing processes.
- a vacuum chamber is used in which the reservoir and / or the dispensing member to be sealed to the reservoir are arranged. In the filling process, the vacuum chamber contains only the reservoir, and fluid is injected into the reservoir, while a vacuum prevails inside the enclosure. This ensures that there will be no inclusion of air inside the fluid product.
- the object of the present invention is to remedy the aforementioned disadvantage of the prior art by defining a new packaging method which can be used in place of or in addition to the vacuum filling and sealing processes of the art. prior.
- the present invention provides a fluid product conditioning method in a fluid dispenser comprising a fluid reservoir defining an opening and a fluid dispenser member, such as a pump or a valve, for to be mounted in a sealed manner on the opening of the reservoir, an inert gas, such as nitrogen or argon, being present in the reservoir above the fluid during the sealed assembly of the dispenser member on the opening of the reservoir, such that the fluid product is in contact with the inert gas in the reservoir, characterized in that the step of sealing assembly of the dispensing member on the opening of the reservoir is carried out under vacuum , the inert gas is at least partially removed from the reservoir during this evacuation step, so that the reservoir is subjected to a vacuum of inert gas.
- an inert gas such as nitrogen or argon
- the air initially contained in the reservoir is removed, for example by suction, and then the inert gas is allowed to enter the reservoir instead of air.
- the inert gas is allowed to enter the reservoir instead of air.
- the fluid filling and / or sealing of the dispensing member on the reservoir can be carried out at atmospheric pressure with inert gas inside the reservoir above the fluid.
- the packaging method of the invention may comprise a step of filling the reservoir with fluid, the air being replaced by the inert gas before and / or after this filling step.
- the filling step is carried out under vacuum of air or inert gas, the tank being returned to atmospheric pressure by letting inert gas enter the tank.
- the purge is performed with an inert gas at a pressure at least equal to atmospheric pressure, this to ensure that the fluid does not come into contact with the air.
- a gas heavier than air such as argon, the inert gas can remain inside the tank above the fluid even at atmospheric pressure.
- the tank thus filled with fluid and inert gas can pass to the next station where the dispensing member is sealingly mounted on the tank, this operation can be performed at atmospheric pressure.
- a gas evacuation before assembly is preferable, especially when it is an "airless" tank, which should contain only fluid.
- the spirit of the invention lies in the fact of performing at least some fluid product conditioning operations in an inert gas atmosphere at least at the reservoir, so that after conditioning, the fluid product is not in contact with air, but in contact with an inert gas that does not interact with the fluid and thus guarantees its perfect preservation.
- the present invention consists of a packaging process which is carried out by means of a suitable packaging device for the purpose of producing a fluid dispenser which incorporates the results of the packaging process.
- the two conditioning devices represented on the Figures 1 and 2 are very similar in that they each comprise a vacuum chamber 4, an inlet of inert gas 43 connected to a source of inert gas G, an outlet 44 connected to a vacuum pump V to evacuate the enclosure 4, and a filling station 5 or a waterproof mounting station 6.
- the enclosure 4 comprises a lower bucket 41 and an upper bell 42 or 42 ', tightly attached to one another to create an interior space in which we can make a vacuum prevail.
- the inlet of inert gas 43 and the outlet 44 are located at the bell 42, 42 '.
- bell 42 is equipped with a filling station 5 through which fluid product P can be injected into the interior of the bell.
- the bell 42 ' is equipped with a sealed mounting station 6, which may for example be a crimping station or snap.
- the packaging method and the packaging devices of the invention are intended to condition fluid product P inside a fluid dispenser comprising, inter alia, a fluid reservoir and a dispenser member, such as a pump or a valve, intended to be mounted sealingly on the reservoir.
- the dispensing member can be of any kind as mentioned above, and is therefore not limited only to a pump or a valve.
- the tank it can also be of any kind, of constant or variable capacity, rigid or deformable nature, or further comprising a movable element to vary its capabilities. Given the purpose of the present invention, namely a perfect preservation of the fluid within the tank, it is of course preferable that the amount of fluid extracted from the tank is not replaced by an equivalent volume of outside air .
- the tank 1 is of the piston-follower type. More specifically, the reservoir 1 comprises a cylindrical sliding shaft 11 which is extended by forming a neck 12 defining internally an opening 13 communicating the interior of the barrel 11 with the outside.
- the reservoir 1 also comprises a follower piston 14 which is slidably engaged inside the barrel 11.
- the follower piston 14 is intended to move inside the barrel 11 as fluid is extracted therefrom. .
- the displacement of the follower piston 14 is generated by a depression created inside the reservoir. All this is quite conventional for this type of piston-follower tank.
- the dispensing member 2 is only shown on the figure 2 .
- a fixing ring 3 is used which is only very schematically. It may be a crimping ring or a snap ring. It is even possible to use a screw ring. The essential thing is that the ring 3 carries a tight assembly of the pump 2 on the neck 12 of the tank.
- the tank 1 is introduced inside the cup 41 of the chamber 4, and the bell 42 completes the chamber 4 to isolate the interior of the chamber 4 from the outside.
- the interior of the tank 1, as well as the outside of the tank, are subjected to the same pressure prevailing inside the chamber 4.
- the filling station 5 extends inside the bell 42 so as to penetrate at least partially inside the neck 12 to inject fluid into the tank.
- the air that is present inside the chamber 4 is evacuated through the outlet 44 connected to the vacuum pump V.
- the vacuum pump V there is a void of air inside the enclosure 4.
- air inside the chamber 4 there is more or less air inside the chamber 4: we can make a vacuum that tends to 100%.
- an inert gas is introduced inside the chamber 4 through the inlet 43 connected to the source of inert gas G. Since there is an air gap inside the enclosure 4, it is sufficient to let the inert gas enter the enclosure G through the inlet 43.
- the filling operation can be performed under vacuum, but this is not an air vacuum, but a vacuum of inert gas.
- the enclosure 4 filled with inert gas it can evacuate the enclosure by means of the vacuum pump V through the outlet 44.
- the enclosure is then partially or completely emptied of its contents, which is the inert gas.
- the filling operation can then begin under this vacuum of inert gas.
- the vacuum of inert gas can be broken and the chamber 4 can then be opened by moving the cup 41 relative to the bell 42.
- the tank is then at atmospheric pressure and / or ambient air, depending on which a vacuum or not was made in the enclosure.
- the opening of the chamber 4 causes a dispersion in the atmosphere of the inert gas.
- a substantially heavy inert gas as is the case with argon
- the empty space of fluid inside the tank above the fluid can remain filled with inert gas. It then suffices during a subsequent sealed mounting step to mount the dispensing member 2 in the opening of the reservoir 12 sealingly.
- the empty space of fluid inside the tank is then mainly filled with inert gas. It is thus possible to implement the present invention without producing a vacuum.
- the opening of the enclosure 4 when the filling operation has been carried out under vacuum, the opening of the enclosure 4 generates an introduction of air inside the tank 1 above the fluid product. It is in this case preferable to perform a sealed mounting operation of the dispenser member on the reservoir under vacuum conditions.
- inert gas may be introduced into the tank after the filling operation, which has been carried out at atmospheric pressure. It will be necessary to purge with an inert gas, which will ensure complete protection of the fluid filled.
- a complete fluid product dispenser is introduced inside the enclosure 4.
- the dispenser comprises a reservoir 1, such as that of the figure 1 as well as a dispensing member 2 arranged in an unsealed manner in the opening 12 of the reservoir.
- the distributor also comprises a fixing ring 3 which is non-definitively mounted and therefore not sealed on the dispensing member 2.
- the reservoir 1 is filled with fluid product P to a level close to the opening 12.
- there remains a space E which is empty of fluid and which is therefore initially filled with air.
- the enclosure is closed: however the space E is subjected to the same pressure as that prevailing in the rest of the enclosure outside the tank, since there is no sealing between the dispensing member 2 and the reservoir.
- the air initially contained inside the chamber 4 is replaced by an inert gas.
- This operation can be carried out in the same way as in the first implementation of the figure 1 .
- the air of the enclosure can be evacuated through the outlet 44 using the vacuum pump V, then inert gas can be introduced inside the chamber 4 emptied of its air through the 43 to the gas source G.
- the air contained inside the chamber 4 can be removed by the injection pressure of inert gas inside the chamber.
- the air is flushed or vented through exit 44 directly open to the atmosphere. In both cases, we end up with an enclosure 4 filled with inert gas. Therefore, the space E is filled with inert gas.
- the implementations of the packaging method according to the invention Figures 1 and 2 can be performed successively or independently of one another.
- the filling operation and / or the sealed mounting operation can be carried out under vacuum or not. If inert gas remains above the fluid within the tank 1 after the filling operation, the mounting operation can be carried out at atmospheric pressure. However, this will rarely be used, because the operation of the dispenser will not be optimal, especially for "airless" distributors without outside air intake.
Landscapes
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Vacuum Packaging (AREA)
- Nozzles (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0854438A FR2933380B1 (fr) | 2008-07-01 | 2008-07-01 | Procede de conditionnement de produit fluide dans un distributeur |
PCT/FR2009/051262 WO2010001049A2 (fr) | 2008-07-01 | 2009-06-30 | Procede de conditionnement de produit fluide dans un distributeur |
Publications (2)
Publication Number | Publication Date |
---|---|
EP2313319A2 EP2313319A2 (fr) | 2011-04-27 |
EP2313319B1 true EP2313319B1 (fr) | 2011-12-07 |
Family
ID=40297652
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP09772731A Not-in-force EP2313319B1 (fr) | 2008-07-01 | 2009-06-30 | Procede de conditionnement de produit fluide dans un distributeur |
Country Status (8)
Country | Link |
---|---|
US (1) | US8726615B2 (es) |
EP (1) | EP2313319B1 (es) |
CN (1) | CN102076566B (es) |
AT (1) | ATE536309T1 (es) |
BR (1) | BRPI0913917A2 (es) |
ES (1) | ES2378336T3 (es) |
FR (1) | FR2933380B1 (es) |
WO (1) | WO2010001049A2 (es) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR3019531B1 (fr) * | 2014-04-04 | 2019-08-09 | Techniplast | Procede d'extraction de liquide d'un appareil de distribution de liquide par injection de gaz |
FR3036389B1 (fr) * | 2015-05-18 | 2019-08-23 | Aptar France Sas | Procede et dispositif de remplissage de reservoir. |
US20170361966A1 (en) * | 2016-06-16 | 2017-12-21 | Muffin Incorporated | Vial filling system with localized clean zone |
WO2019011960A1 (en) * | 2017-07-11 | 2019-01-17 | Becton Dickinson France | DEVICE FOR EMPTYING AND BLEEDING AERATION TUBE OF A MEDICAL CONTAINER |
FR3083721B1 (fr) | 2018-07-12 | 2020-12-18 | Aptar France Sas | Dispositif de distribution de produit fluide et son procede de remplissage et de bouchage. |
FR3087360B1 (fr) * | 2018-10-19 | 2021-06-04 | Promens Sa | Procede de remplissage d'un reservoir d'un dispositif de distribution du type sans reprise d'air |
CN110282168A (zh) * | 2019-05-20 | 2019-09-27 | 珠海市维启自动化设备有限公司 | 粉末充进机 |
JP7504922B2 (ja) * | 2019-05-23 | 2024-06-24 | ジー.デー ソチエタ ペル アツィオニ | 容器、特にカートリッジに、製薬産業の液体製品を充填するための充填ユニット |
CN110888310B (zh) * | 2019-12-03 | 2024-06-25 | 珠海市维启自动化设备有限公司 | 减压式碳粉充填机 |
WO2021171321A1 (en) * | 2020-02-28 | 2021-09-02 | Taramar Seeds Ehf. | Cosmetic formulations with an argon blanket and an internal argon reservoir and methods for making same |
WO2022271186A1 (en) * | 2021-06-25 | 2022-12-29 | Thrivo Technologies Inc. | Systems and Methods of Preserving Customized Cosmetic Products |
Family Cites Families (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2054492A (en) * | 1932-07-30 | 1936-09-15 | American Can Co | Method of and apparatus for gassing and sealing products in cans |
US2973609A (en) * | 1959-09-28 | 1961-03-07 | Reddi Wip Inc | Radial machine for aseptic canning and the like |
DE1232602B (de) * | 1963-04-04 | 1967-01-19 | Novima A G | Verfahren und Vorrichtung zum Fuellen von Aerosolbehaeltern |
IT1205619B (it) * | 1981-11-30 | 1989-03-23 | Aerosol Inventions Dev | Procedimento di confezionamento di liquido da distribuire sotto pressione e confezione ottenuta mediante attuazione di tale procedimento |
FR2582509B1 (fr) * | 1985-05-29 | 1987-08-21 | Sandoz Lab | Appareil pour le remplissage de dispositifs de pulverisation d'un aerosol |
NL8603176A (nl) * | 1986-12-12 | 1988-07-01 | Calumatic Bv | Werkwijze en inrichting voor het verlagen van de hoeveelheid zuurstof in de ruimte boven de vulling binnen een houder. |
GB8809937D0 (en) * | 1988-04-27 | 1988-06-02 | Mclennon J L Ltd | Method of & apparatus for packaging |
FR2653744B1 (fr) * | 1989-10-31 | 1992-03-06 | Valois | Procede pour conditionner sous vide des produits notamment cosmetiques et pharmaceutiques a l'interieur de reservoirs deformables obtures par une pompe de distribution sans reprise d'air, dispositif pour le mettre en óoeuvre et distributeurs ainsi obt. |
EP0446513B1 (en) * | 1990-03-16 | 1994-11-02 | Kabushiki Kaisha Top | Pump assembly |
FR2668118B1 (fr) | 1990-10-17 | 1993-12-24 | Valois | Procede de conditionnement de produits liquides a pateux en distributeur sous vide, dispositif pour le mettre en óoeuvre et distributeurs ainsi obtenus. |
FR2704516B1 (fr) * | 1993-04-28 | 1995-07-21 | Remy Equipement | Procede de bouchage sous gaz inerte de recipients et dispositif pour sa mise en oeuvre. |
US6345739B1 (en) * | 1996-02-02 | 2002-02-12 | Daizo Co., Ltd. | Method for producing a double aerosol device and container therefor |
DE19817735C1 (de) | 1998-04-21 | 1999-11-11 | Fehland Engineering Gmbh | Getränkeabfüllvorrichtung |
JP2003212212A (ja) * | 2002-01-22 | 2003-07-30 | Nippon Tansan Gas Co Ltd | 密封充填装置 |
ATE490932T1 (de) * | 2002-06-26 | 2010-12-15 | Daizo Co Ltd | Verpackungsbehulter zum austragen von mehreren inhalten, verpackungsprodukt mit dem verpackungsbehulter und verfahren zur herstellung des verpackungsprodukts |
US7124788B2 (en) * | 2003-07-10 | 2006-10-24 | Precision Valve Corporation | Means and method for filling bag-on-valve aerosol barrier packs |
US7198074B2 (en) * | 2003-10-01 | 2007-04-03 | Epicurean International Corporation | Motorized vacuum/pressure pump and stopper |
TWI322124B (en) * | 2004-03-04 | 2010-03-21 | Murray Melrose David | Headspace sealing and displacement method for removal of vacuum pressure |
US20070062162A1 (en) * | 2005-09-19 | 2007-03-22 | Martin Lehmann | Method and apparatus for cleaning containers to be sealed and containing a filler from oxygen gas |
US20070241132A1 (en) * | 2006-04-17 | 2007-10-18 | The Procter & Gamble Company | Pressurized package |
US7779608B2 (en) * | 2007-02-02 | 2010-08-24 | Lim Walter K | Pressurized containers and methods for filling them |
-
2008
- 2008-07-01 FR FR0854438A patent/FR2933380B1/fr active Active
-
2009
- 2009-06-30 WO PCT/FR2009/051262 patent/WO2010001049A2/fr active Application Filing
- 2009-06-30 ES ES09772731T patent/ES2378336T3/es active Active
- 2009-06-30 CN CN2009801250266A patent/CN102076566B/zh not_active Expired - Fee Related
- 2009-06-30 AT AT09772731T patent/ATE536309T1/de active
- 2009-06-30 EP EP09772731A patent/EP2313319B1/fr not_active Not-in-force
- 2009-06-30 US US13/002,268 patent/US8726615B2/en not_active Expired - Fee Related
- 2009-06-30 BR BRPI0913917A patent/BRPI0913917A2/pt not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
WO2010001049A2 (fr) | 2010-01-07 |
WO2010001049A3 (fr) | 2010-02-25 |
US8726615B2 (en) | 2014-05-20 |
CN102076566B (zh) | 2012-12-05 |
FR2933380A1 (fr) | 2010-01-08 |
EP2313319A2 (fr) | 2011-04-27 |
ES2378336T3 (es) | 2012-04-11 |
FR2933380B1 (fr) | 2013-01-18 |
CN102076566A (zh) | 2011-05-25 |
ATE536309T1 (de) | 2011-12-15 |
BRPI0913917A2 (pt) | 2015-10-20 |
US20110146207A1 (en) | 2011-06-23 |
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