EP2054622B1 - Delivery pump - Google Patents
Delivery pump Download PDFInfo
- Publication number
- EP2054622B1 EP2054622B1 EP07786115A EP07786115A EP2054622B1 EP 2054622 B1 EP2054622 B1 EP 2054622B1 EP 07786115 A EP07786115 A EP 07786115A EP 07786115 A EP07786115 A EP 07786115A EP 2054622 B1 EP2054622 B1 EP 2054622B1
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- EP
- European Patent Office
- Prior art keywords
- feed
- pump
- pump according
- radial wheel
- feed pump
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- 230000008859 change Effects 0.000 description 2
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- 238000006073 displacement reaction Methods 0.000 description 2
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Images
Classifications
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F04—POSITIVE - DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS FOR LIQUIDS OR ELASTIC FLUIDS
- F04B—POSITIVE-DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS
- F04B15/00—Pumps adapted to handle specific fluids, e.g. by selection of specific materials for pumps or pump parts
- F04B15/06—Pumps adapted to handle specific fluids, e.g. by selection of specific materials for pumps or pump parts for liquids near their boiling point, e.g. under subnormal pressure
- F04B15/08—Pumps adapted to handle specific fluids, e.g. by selection of specific materials for pumps or pump parts for liquids near their boiling point, e.g. under subnormal pressure the liquids having low boiling points
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F04—POSITIVE - DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS FOR LIQUIDS OR ELASTIC FLUIDS
- F04D—NON-POSITIVE-DISPLACEMENT PUMPS
- F04D15/00—Control, e.g. regulation, of pumps, pumping installations or systems
- F04D15/0066—Control, e.g. regulation, of pumps, pumping installations or systems by changing the speed, e.g. of the driving engine
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F04—POSITIVE - DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS FOR LIQUIDS OR ELASTIC FLUIDS
- F04D—NON-POSITIVE-DISPLACEMENT PUMPS
- F04D29/00—Details, component parts, or accessories
- F04D29/18—Rotors
- F04D29/22—Rotors specially for centrifugal pumps
- F04D29/2205—Conventional flow pattern
- F04D29/2222—Construction and assembly
- F04D29/2227—Construction and assembly for special materials
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F04—POSITIVE - DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS FOR LIQUIDS OR ELASTIC FLUIDS
- F04D—NON-POSITIVE-DISPLACEMENT PUMPS
- F04D29/00—Details, component parts, or accessories
- F04D29/18—Rotors
- F04D29/22—Rotors specially for centrifugal pumps
- F04D29/2238—Special flow patterns
- F04D29/225—Channel wheels, e.g. one blade or one flow channel
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F04—POSITIVE - DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS FOR LIQUIDS OR ELASTIC FLUIDS
- F04D—NON-POSITIVE-DISPLACEMENT PUMPS
- F04D29/00—Details, component parts, or accessories
- F04D29/60—Mounting; Assembling; Disassembling
- F04D29/605—Mounting; Assembling; Disassembling specially adapted for liquid pumps
Definitions
- the invention relates to a feed pump with a variable speed drive for a metered flow rate delivery, wherein the feed pump is designed as a single-stage centrifugal pump in a impeller space of a pump housing without a sealing gap rotationally arranged radial centrifugal type for conveying a fluid between a pump inlet and a pump outlet.
- the drive motor has a PEEK split tube inside which a rotor protected by a stainless steel coating is located. Ceramic bearings of the pump shaft and the drive rotor are lubricated by a partial flow of the pumped liquid taken from the pump housing.
- the open impeller has a diameter between 1 and 2 inches and the impeller driving rotor of the roller bearing DC motor has a diameter between 1.5 and 2 inches.
- the single-stage pumping device with the open impeller should reach maximum speeds of up to 60,000 rpm.
- Suction nozzle, discharge nozzle and a downstream of the impeller type of spiral space are arranged in an outer pump housing part, while an inner pump housing part has the cantilevered impeller and a mounting for a variable speed DC canned motor as a drive motor.
- a metering pump is realized as centrifugal centrifugal type, which is designed for continuous operation in a partial load operating point field. Its flow limits are in the range of 0 ml / min to 3600 ml / min at delivery height limits of 20 m to 300 m.
- the impeller rotates without contact within an impeller space and a return flow within the wheel sidewalls is permitted. This ensures a wear-free operation of the impeller.
- the centrifugal pump is designed for an extreme part-load operation, whereby small amounts are conveyed pulsation-free.
- the diameter of the impeller space is at most 4% larger than an outer diameter of a radial wheel arranged therein and the impeller space is provided with one or more, acute-angled or tangential to Radialradaußen pressmesser arranged pump outlet channels.
- the delivery of the centrifugal pump results from a proportion of static pressure, which builds up due to the centrifugal force within the impeller space and a dynamic proportion in the form of the dynamic pressure, which occurs at the transition from the impeller space to the pump outlet in the form of a Druckstutzen- or outlet channel.
- the dynamic pressure component at the outlet opening from the impeller space corresponds to a maximum.
- the addition of the centrifugal delivery head component and the delivery head component due to the back pressure to a total delivery head of the pump results in the high pressure factor for this type of pump.
- a sealing of the impeller space relative to the atmosphere or the tempering takes place with one or more shaft seals between a housing wall of the impeller space and a rotary Radialrad- or a shaft part penetrating them.
- These can be known shaft seals or low-friction mechanical seals.
- Such seals can be dispensed with if a hermetically sealed, magnetically coupled drive transmits a torque to the radial wheel. This can also be designed as a tear-resistant hysteresis coupling.
- Next can be connected to the radial wheel an electric, pneumatic or hydraulic drive.
- Such a drive motor is attached to the pump or Temperiergephase and connected via a guided through this housing shaft with the radial wheel.
- the arranged in the drive motor bearing the rotor shaft can be found in a conventional manner at the same time as storage of the pump shaft and the radial wheel use.
- the feed pump is connected to a control device, which is connected to an internal or external volume flow measurement and independent of a back pressure of a system with the drive motor generates an adjustable constant volume flow.
- a control device With the control device, a variable speed range of the drive motor with a quantity factor up to the value 5000 is generated in the switching or control range between minimum and maximum delivery. And in the speed range of the drive motor from 0 to 35000 revolutions / min is a centrifugal pump delivery pressure between 0 to 300 bar.
- centrifugal pump operating data are only possible due to the contrary to all known design rules interpretation of radial wheel and housing of the pump unit for an extreme permanent part-load operation.
- the pump unit, drive motor, switching or control device and associated electronic operating, measuring and control elements are combined to form an assembly-capable module.
- Fig. 1 is a delivery pump in a single-stage design shown.
- a radial wheel 2 centrifugal type is arranged to rotate.
- the radial wheel 2 has delivery channels 3 and is centrally through a pump inlet 4 flows.
- the radial wheel 2 is connected to transmit power to a variable speed drive 5 and has an outer diameter D LA , which may be up to 50 mm.
- the radial wheel rotates in an impeller space 6, the inner diameter D LRI is designed to be only 4% larger than the outer diameter D LA of the radial wheel 2.
- the area of the pump inlet 4 is defined by a contact surface 12 located in the immediate vicinity of the pump interior, against which a line to be connected for a delivery fluid bears sealingly.
- An analogous training is on the - here below the drawing plane, only partially visible as a semicircle - pump outlet 13 is present.
- External temperature control for example, coolant
- Coolant are fed through the optional axial or radial ports 14, 15 the temperature control chambers 7.1 to 7.3 and derived.
- Pump unit and drive motor 5 are combined to form a structural unit and held in a support member 16.
- the support element 16 provides the prerequisite for the modular design or installation in an existing system.
- Fig. 3 shows a perspective view of a radial wheel 2.
- the radial wheel 2 is designed disc-shaped and provided in this example with a hub 2.1. Within the hub 2.1 is a force-transmitted connection with the shaft 10, not shown here of the drive 5. Within the radial wheel 2, four conveyor channels 3 are arranged. In addition, a plurality of conveying recesses 18 are arranged on the impeller periphery 17, which are designed in the form of blind holes. With the help of these delivery wells, the pressure coefficient of the centrifugal impeller is significantly improved.
- the pressure and suction side shrouds 19, 20 a plurality of radially extending conveyor grooves 21.
- the feed grooves 21 also improve the pressure digit of one Fig. 1 in an impeller room 6 built-in impeller.
- the impeller in the axial direction penetrating compensation bores 22 serve to equalize pressure within the pump housing and at the same time as an assembly aid in the preparation of a connection to the drive.
- Fig. 4 shows a section through an impeller 2. It can be seen that here only a total of four conveyor channels 3 are used. Their diameter is adjusted so that they do not intersect an adjacent conveyor channel in the region of the impeller inlet 23. Thus, the maintenance of a defined impeller inlet diameter is guaranteed.
- the depth T of the conveying recesses 18 is selected as a function of the desired residual volume of a fully assembled pump.
- any other shape such as grooves, slots or the like, find application, with which in the range of the impeller outer diameter, an energy transfer is possible.
- Fig. 5 shows a cross section through the feed pump. Due to the generous temperature control room 7.2, which is in operative connection with the other temperature control room, a permanent extreme partial load operation is guaranteed.
- the non-contact arrangement of the impeller within the impeller space avoids sealingly abutting friction surfaces. This measure prevents the generation of mechanical frictional heat, prevents fretting and consequent contamination of a pumped liquid with abraded particles and improves reliability through significantly extended periods of use. In addition, the cleanability counteracting sealing gaps are avoided.
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Structures Of Non-Positive Displacement Pumps (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Eye Examination Apparatus (AREA)
- Control Of Non-Positive-Displacement Pumps (AREA)
- Measuring Pulse, Heart Rate, Blood Pressure Or Blood Flow (AREA)
- Lubrication Of Internal Combustion Engines (AREA)
- Fluid-Driven Valves (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
Description
Die Erfindung betrifft eine Förderpumpe mit einem drehzahlveränderbaren Antrieb für eine dosierende Fördermengenabgabe, wobei die Förderpumpe als einstufige Kreiselpumpe mit in einem Laufradraum eines Pumpengehäuses ohne Dichtspalt rotierend angeordneten Radialrad zentrifugaler Bauart zur Förderung eines Fluids zwischen einem Pumpeneinlass und einem Pumpenauslass ausgebildet ist.The invention relates to a feed pump with a variable speed drive for a metered flow rate delivery, wherein the feed pump is designed as a single-stage centrifugal pump in a impeller space of a pump housing without a sealing gap rotationally arranged radial centrifugal type for conveying a fluid between a pump inlet and a pump outlet.
Im Bereich der Forschungs- und Entwicklungsprozesse der chemischen und pharmazeutischen Industrie besteht die Forderung nach immer schnelleren Entwicklungen zu geringeren Kosten. In der Produktion solcher Stoffe werden flexiblere, kleinere und umweltschonendere Prozesse verlangt. Dies führt zum Einsatz verfahrenstechnischer Komponenten, die teilweise mit sehr kleinen Füllvolumina und kontinuierlichem Stofffluss betrieben werden. Aufgrund der Forderung eines flexiblen Einsatzes solcher Anlagen, ist eine gute Spülbarkeit der gesamten Anlage mit den darin montierten Aggregaten mit Hilfe von besonderen Spülmedien notwendig.In the area of research and development processes in the chemical and pharmaceutical industry, there is a demand for ever faster developments at lower costs. In the production of such substances more flexible, smaller and more environmentally friendly processes are required. This leads to the use of procedural components, which are sometimes operated with very small filling volumes and continuous material flow. Due to the requirement of a flexible use of such systems, a good flushability of the entire system with the units mounted therein with the help of special flushing media is necessary.
Solche Anlagen erfordern einen präzisen, konstanten, frei einstellbaren und pulsationsfreien Volumenstrom von flüssigen Stoffen. Für hochpräzise kontinuierliche Volumenströme im Bereich von null Millilitern pro Minute bis zu einer dreistelligen Anzahl von Litern pro Stunde werden Verdrängerpumpen in Form von Mikrozahnring- und Zahnradpumpen sowie in Form von Membran- und Kolbenpumpen verwendet. Nachteil solcher Verdrängerpumpen sind die mangelhafte Zuverlässigkeit infolge Reibung zwischen den relativ zueinander bewegten, abzudichtenden Bauteilen und deren pulsierender Förderstrom. Ein dadurch bedingter Wartungsaufwand und die Kosten für Verschleißteile sowie für deren Wechsel behindern schnelle Forschungs- und Entwicklungsarbeiten und stören einen Produktionsprozess empfindlich.Such systems require a precise, constant, freely adjustable and pulsation-free volume flow of liquid substances. For high-precision, continuous flow rates ranging from zero milliliters per minute up to three-digit liters per hour, positive displacement pumps are used in the form of micro gear and gear pumps as well as diaphragm and piston pumps. Disadvantage of such positive displacement pumps are the lack of reliability due to friction between the relatively moving, sealed components and their pulsating flow. A consequent maintenance and the cost of wearing parts and their replacement hinder rapid research and development and interfere with a production process sensitive.
Durch die
Die Druckschrift
Nachteilig bei dieser Spaltrohrmotorkonstruktion ist die Vielzahl von Spalten, die aufgrund der komplexen Strömungsführung zwischen Pumpe und Spaltrohrmotor die Reinigung der Pumpe stark behindern. Da ein Teil der Förderflüssigkeit permanent den Motor und dessen Spaltraum durchströmt, entsteht durch die Reibungswärme der Wälzlager sowie die Verlustwärme des Spaltrohrmotors ein unzulässig hoher Wärmeeintrag in die Förderflüssigkeit.A disadvantage of this canned motor design is the large number of columns, which hinder the cleaning of the pump due to the complex flow guidance between the pump and canned motor. Since a part of the pumped liquid flows through the motor and its gap permanently, created by the frictional heat of the bearings and the heat loss of the canned motor an unacceptably high heat input into the fluid.
Der Erfindung liegt das Problem zugrunde, zur Förderung und Dosierung von flüssigen Stoffen im Milliliter-Bereich von chemischen, pharmazeutischen und/oder kosmetischen Komponenten eine Pumpeneinheit zu entwickeln, deren Fördermenge pulsationsfrei und präzise einstellbar über einen großen Bereich für unterschiedliche Fördermedien mit unterschiedlichen Eigenschaften variabel ist und für schnelle Produktwechsel die Pumpe leicht zu reinigen ist.The invention is based on the problem, for the promotion and dosage of liquid substances in the milliliter range of chemical, pharmaceutical and / or cosmetic components to develop a pump unit, the flow rate pulsation-free and precisely adjustable over a wide range for different Flow media with different properties is variable and for quick product change the pump is easy to clean.
Die Lösung des Problems erfolgt mit den Merkmalen von Anspruch 1. Damit ist eine Dosierpumpe als Kreiselpumpe zentrifugaler Bauart verwirklicht, die für einen Dauerbetrieb in einem Teillast-Betriebspunktefeld ausgelegt ist. Dessen Fördermengengrenzen liegen im Bereich von 0 ml/min bis 3600 ml/min bei Förderhöhengrenzen von 20 m bis 300 m. Das Laufrad rotiert innerhalb eines Laufradraumes berührungsfrei und eine Rückströmung innerhalb der Radseitenräume wird zugelassen. Dies gewährleistet einen verschleißfreien Betrieb des Laufrades. Und im völligen Gegensatz zu allen geltenden Kreiselpumpen-Auslegebestimmungen ist die Kreiselpumpe für einen extremen Teillastbetrieb ausgelegt, wodurch kleine Mengen pulsationsfrei gefördert werden.The problem is solved with the features of
Der Durchmesser des Laufradraumes ist maximal 4 % größer ausgebildet als ein Außendurchmesser eines darin angeordneten Radialrades und der Laufradraum ist mit einem oder mehreren, spitzwinklig oder tangential zum Radialradaußendurchmesser angeordneten Pumpenauslasskanälen versehen. Infolgedessen ergibt sich die Förderhöhe der Kreiselpumpe aus einem Anteil von statischen Druck, der sich infolge der Zentrifugalkraft innerhalb des Laufradraumes aufbaut sowie einem dynamischen Anteil in Form des Staudrucks, der sich am Übergang vom Laufradraum zum Pumpenauslass in Form eines Druckstutzen- oder Austrittskanals einstellt. Die Staudruckkomponente an der Austrittsöffnung aus dem Laufradraum entspricht einem Maximum. Aus der Addition der zentrifugalen Förderhöhenkomponente und der durch den Staudruck bedingten Förderhöhenkomponente zu einer Gesamtförderhöhe der Pumpe, ergibt sich die für diese Pumpenbauart hohe Druckziffer.The diameter of the impeller space is at most 4% larger than an outer diameter of a radial wheel arranged therein and the impeller space is provided with one or more, acute-angled or tangential to Radialradaußendurchmesser arranged pump outlet channels. As a result, the delivery of the centrifugal pump results from a proportion of static pressure, which builds up due to the centrifugal force within the impeller space and a dynamic proportion in the form of the dynamic pressure, which occurs at the transition from the impeller space to the pump outlet in the form of a Druckstutzen- or outlet channel. The dynamic pressure component at the outlet opening from the impeller space corresponds to a maximum. The addition of the centrifugal delivery head component and the delivery head component due to the back pressure to a total delivery head of the pump results in the high pressure factor for this type of pump.
Im völligen Gegensatz hierzu sind herkömmliche Kreiselpumpen ausgelegt, bei denen sich der Druckaufbau überwiegend durch eine Geschwindigkeitsverzögerung infolge einer Vergrößerung des dem Laufrad nachgeordneten Strömungsraumes in Fließrichtung ergibt.In complete contrast, conventional centrifugal pumps are designed in which the pressure build-up predominantly by a speed delay due to an increase in the downstream of the impeller flow space results in the flow direction.
Um bei einer Reinigung der Förderpumpe oder einer Umstellung auf andere Fördermittel mit minimalen Verlusten an wertvollen Fördermitteln auszukommen, weist das Pumpengehäuse mit einem darin angeordneten Radialrad im Bereich zwischen einem Pumpeneintritt und einem Pumpenaustritt, deren Querschnittsflächen durch Anlageflächen von daran anzuschließenden Leitungen definiert sind, ein Restvolumen gleich oder kleiner 50 Milliliter auf. Bei einem Chargen- oder Produktwechsel ergibt sich ein minimaler Verlust bei schnellerer Reinigbarkeit der Pumpe.To get along with minimal loss of valuable funding in a cleaning of the feed pump or a conversion to other funding, has the pump housing with a radial wheel disposed in the region between a pump inlet and a pump outlet whose cross-sectional areas are defined by contact surfaces of lines to be connected, a residual volume equal to or less than 50 milliliters. A batch or product change results in a minimal loss with faster pump cleanability.
Für die Förderung der unterschiedlichen Fördermittel ist das Pumpengehäuse mit einer Temperiereinrichtung versehen. Somit ist eine einfache Temperaturanpassung möglich. Dabei kann die Temperiereinrichtung als ein Wärmetauscher ausgebildet sein, der die fluidberührten Teile des Pumpengehäuse ganz oder teilweise umgibt. Dazu durchdringen flüssigkeitsdichte Verbindungen die Temperiereinrichtung und stellen eine fluidführende Verbindung zwischen einer Anlage und dem Laufradraum her. In Abhängigkeit von der Temperatur des Förderfluids ist das Pumpengehäuse innerhalb der Temperiereinrichtung angeordnet, um das Förderfluid zu kühlen oder zu heizen.For the promotion of different funding, the pump housing is provided with a tempering device. Thus, a simple temperature adjustment is possible. In this case, the tempering device may be formed as a heat exchanger which completely or partially surrounds the wetted parts of the pump housing. For this purpose, liquid-tight connections penetrate the tempering device and establish a fluid-conducting connection between a system and the impeller space. Depending on the temperature of the delivery fluid, the pump housing is disposed within the tempering device to cool or heat the delivery fluid.
Das Radialrad weist mindestens zwei Förderkanäle auf und am Radialradaußendurchmesser sind mehrere Fördervertiefungen angeordnet. Diese am Radialrad angeordnete Fördervertiefungen sind als Sackbohrungen, Taschen oder zahnförmige Ausnehmungen gestaltet. Die Förderkanäle sind als offene Vertiefungen in Form von Schaufelkanälen, Nuten oder Rillen ausgebildet. Bei einer Ausbildung des Radialrades als ein geschlossenes Laufrad kann eine saug- und/oder druckseitige Deckscheibe an sich bekannte Fördernuten aufweisen.The radial wheel has at least two delivery channels and at the Radialradaußendurchmesser several conveyor wells are arranged. These arranged on the radial wheel conveyor wells are designed as blind holes, pockets or tooth-shaped recesses. The delivery channels are formed as open recesses in the form of blade channels, grooves or grooves. In one embodiment of the radial wheel as a closed impeller, a suction and / or pressure-side cover disk can have known conveying grooves.
Beim Radialrad ist die Anzahl und die Anordnung von den Eintrittsöffnungen der Förderkanälen so gewählt, dass sie einen Radialradeintrittsdurchmesser nicht vergrößern. Somit wird bei den kleinen Abmessungen eine maximale Fläche am Laufrad für die Erzeugung der Zentrifugalkräfte erlangt.In the radial wheel, the number and arrangement of the inlet openings of the delivery channels is chosen so that they do not increase a Radialradeintrittsdurchmesser. Thus, with the small dimensions, a maximum area on the impeller for generating the centrifugal forces is obtained.
Eine Abdichtung des Laufradraumes gegenüber der Atmosphäre oder der Temperiereinrichtung erfolgt mit einer oder mehreren Wellendichtungen zwischen einer Gehäusewand vom Laufradraum und einem diese durchdringenden rotierenden Radialrad- oder einem Wellenteil. Dies können bekannte Wellendichtringe oder reibungsarme Gleitringdichtungen sein. Auf solche Dichtungen kann verzichtet werden, wenn ein hermetisch dichter, magnetgekuppelter Antrieb ein Drehmoment auf das Radialrad überträgt. Dieser kann auch als eine abreißsichere Hysterese-Kupplung ausgebildet sein. Weiter kann mit dem Radialrad ein elektrischer, pneumatischer oder hydraulischer Antrieb verbunden sein. Ein solcher Antriebsmotor ist am Pumpen- oder Temperiergehäuse befestigt und über eine durch dieses Gehäuse geführte Welle mit dem Radialrad verbunden. Die im Antriebsmotor angeordnete Lagerung der Rotorwelle kann in an sich bekannter Weise zugleich als Lagerung der Pumpenwelle und des Radialrades Verwendung finden.A sealing of the impeller space relative to the atmosphere or the tempering takes place with one or more shaft seals between a housing wall of the impeller space and a rotary Radialrad- or a shaft part penetrating them. These can be known shaft seals or low-friction mechanical seals. Such seals can be dispensed with if a hermetically sealed, magnetically coupled drive transmits a torque to the radial wheel. This can also be designed as a tear-resistant hysteresis coupling. Next can be connected to the radial wheel an electric, pneumatic or hydraulic drive. Such a drive motor is attached to the pump or Temperiergehäuse and connected via a guided through this housing shaft with the radial wheel. The arranged in the drive motor bearing the rotor shaft can be found in a conventional manner at the same time as storage of the pump shaft and the radial wheel use.
Zusätzlich kann eine Wärmesperre zwischen Antriebsmotor und dem Temperiergehäuse und/oder Pumpengehäuse angeordnet sein, wobei der Antriebsmotor über eine durchgeführte Welle mit dem Radialrad verbunden ist. Verbindungszonen zwischen den Teilen des Pumpengehäuses und dem Temperiergehäuse sind rotationssymmetrisch gestaltet und gegeneinander abgedichtet. Dies ermöglicht eine verbesserte Abdichtung, die bei der Förderung von Kleinstmengen von gefährlicher oder kostbarer Fluide in Form von flüssigen Chemikalien und/oder Lösungen wichtig ist. Durch den regelbaren Antrieb der für einen Dauerbetrieb im extremen Teillastbereich ausgelegten Kreiselpumpe ist eine gleichmäßige pulsationsfreie einstellbare Förderung von Kleinstmengen solcher Fluide möglich.In addition, a heat barrier between the drive motor and the tempering and / or pump housing may be arranged, wherein the drive motor is connected via a shaft performed with the radial wheel. Connecting zones between the parts of the pump housing and the temperature control housing are rotationally symmetrical and sealed against each other. This provides an improved seal important in the promotion of very small quantities of hazardous or valuable fluids in the form of liquid chemicals and / or solutions. Due to the controllable drive of the centrifugal pump designed for continuous operation in the extreme part-load range, a uniform pulsation-free adjustable delivery of very small amounts of such fluids is possible.
Weiterhin ist die Förderpumpe mit einer Regeleinrichtung verbunden, wobei diese mit einer internen oder externen Volumenstrommessung verbunden ist und unabhängig von einem Gegendruck einer Anlage mit dem Antriebsmotor einen einstellbaren konstanten Volumenstrom erzeugt. Mit der Regeleinrichtung wird im Schalt- oder Regelbereich zwischen minimaler und maximaler Fördermenge ein veränderbarer Drehzahlbereich des Antriebsmotors mit einem Mengenfaktor bis zum Wert 5000 erzeugt. Und im Drehzahlbereich des Antriebsmotors von 0 bis 35000 Umdrehungen/min liegt ein Kreiselpumpen-Förderdruck zwischen 0 bis 300 Bar. Solche Kreiselpumpenbetriebsdaten sind nur aufgrund der entgegen allen bekannten Auslegeregeln erfolgten Auslegung von Radialrad und Gehäuse der Pumpeneinheit für einen extremen dauerhaften Teillastbetrieb möglich. Für einfache Einbaumöglichkeiten sind Pumpeneinheit, Antriebsmotor, Schalt- oder Regeleinrichtung und damit verbundene elektronische Bedien-, Mess- und Steuerungselemente zu einem montagefähigen Modul zusammengefasst.Furthermore, the feed pump is connected to a control device, which is connected to an internal or external volume flow measurement and independent of a back pressure of a system with the drive motor generates an adjustable constant volume flow. With the control device, a variable speed range of the drive motor with a quantity factor up to the value 5000 is generated in the switching or control range between minimum and maximum delivery. And in the speed range of the drive motor from 0 to 35000 revolutions / min is a centrifugal pump delivery pressure between 0 to 300 bar. Such centrifugal pump operating data are only possible due to the contrary to all known design rules interpretation of radial wheel and housing of the pump unit for an extreme permanent part-load operation. For simple installation options, the pump unit, drive motor, switching or control device and associated electronic operating, measuring and control elements are combined to form an assembly-capable module.
Ausführungsbeispiele der Erfindung sind in den Zeichnungen dargestellt und werden im folgenden näher beschrieben. Es zeigen die
- Fig. 1
- eine Förderpumpe im Längsschnitt,
- Fig. 2
- eine perspektivische Ansicht auf die Pumpeneinheit, die
- Fig. 3
- eine perspektivische Ansicht auf ein Laufrad, die
- Fig. 4
- ein Laufrad im Schnitt und die
- Fig. 5
- einen Querschnitt durch die Förderpumpe
- Fig. 1
- a feed pump in longitudinal section,
- Fig. 2
- a perspective view of the pump unit, the
- Fig. 3
- a perspective view of an impeller, the
- Fig. 4
- an impeller in the section and the
- Fig. 5
- a cross section through the feed pump
In
Das Pumpengehäuse 1 ist mit einer Temperiereinrichtung 7 versehen, die in diesem Ausführungsbeispiel in das Pumpengehäuse integriert ist. Es sind auch andere Bauformen möglich. Kühlräume 7.1 bis 7.3 umgeben den Laufradraum 6 und auch ein an das Pumpengehäuse 1 angrenzendes Dichtungsgehäuse 8. Innerhalb des Dichtungsgehäuses 8 ist als eine Art Wellendichtung eine Dichtung 9 angeordnet, die in dem Ausführungsbeispiel als ein Lippendichtring dargestellt ist. In Abhängigkeit vom verwendeten Förderfluid kann die Dichtung 9 auch als eine Gleitringdichtung ausgebildet sein. Die Dichtung 9 kann in Abhängigkeit von der gewählten Verbindung zwischen Laufrad und einer Welle 10 des Antriebes dichtend am Laufrad 2, an einer Laufradnabe 2.1 oder an der Welle 10 anliegen. Die Temperierräume 7.1 bis 7.3 werden durch externe Mittel beaufschlagt. Dadurch werden die vom Förderfluid berührten Teile des Pumpengehäuse zuverlässig gekühlt, da die Kreiselpumpe für einen Dauerbetrieb in einem Teillast-Betriebspunktefeld ausgelegt ist, dessen Fördermengengrenzen im Bereich von 0 Milliliter/Min. bis 3600 Milliliter/Min. bei einer Förderhöhengrenze von 20 Meter - 300 Meter liegen. Infolge der dafür notwendigen hohen Drehzahl des Antriebes 5 sind zusätzliche Kühlmittel 11 am Außenumfang des Antriebes 5 angeordnet. Und der Antrieb 5 ist kräfteübertragend mit der Temperiereinrichtung 7 verbunden oder daran befestigt.The
Die Fläche des Pumpeneinlasses 4 ist definiert durch eine in unmittelbarer Nähe des Pumpeninnenraumes gelegene Anlagefläche 12, an der eine anzuschließende Leitung für ein Förderfluid dichtend anliegt. Eine analoge Ausbildung ist an dem - hier unterhalb der Zeichenebene befindlichen, nur teilweise als Halbkreis sichtbaren - Pumpenauslass 13 vorhanden. Die Befestigung von daran anzuschließenden Pumpenleitungen - hier nicht dargestellt - erfolgt durch bekannte Mittel, beispielsweise Überwurfmuttern. Durch die unmittelbare Heranführung einer Pumpenleitung an den Laufradraum 6 und durch die geringen Durchmesserunterschiede zwischen Laufrad-Außendurchmesser DLA und Innendurchmesser DLRI des Laufradraumes 6, ergibt sich innerhalb des Pumpengehäuses mit montiertem Radialrad für ein Förderfluid ein Restvolumen von gleich oder kleiner 50 Milliliter. Diese sehr geringe Menge hat den Vorteil, dass bei einem Wechsel des wertvoller Förderfluide nur geringste Verluste auftreten.The area of the
Aus der
Externe Temperiermittel, beispielsweise Kühlmittel, werden durch die wahlweise verwendbaren axialen oder radialen Anschlüsse 14, 15 den Temperierräumen 7.1 bis 7.3 zugeführt und abgeleitet. Pumpeneinheit und Antriebsmotor 5 sind zu einer baulichen Einheit zusammengefasst und in einem Tragelement 16 gehalten. Das Tragelement 16 bietet die Voraussetzung für den modulartigen Aufbau oder Einbau in eine bestehende Anlage.External temperature control, for example, coolant, are fed through the optional axial or
Anstelle der hier gezeigten Fördervertiefungen 18 in Form von Bohrungen kann auch jede andere Form, beispielsweise Nuten, Schlitze oder dergleichen, Anwendung finden, mit denen im Bereich des Laufrad-Außendurchmessers eine Energieübertragung möglich ist.Instead of the conveying
Durch den minimierten Laufradraum 6 ergeben sich zwischen dem Außendurchmesser DLA des Radialrades und dem einhüllenden, umgebenden Durchmesser DLRI des Laufradraumes 6 eine radiale Spaltweite, die im einstelligen Millimeterbereich liegt. Bei einer ausgeführten Kreiselpumpe liegt der radiale Spalt zwischen Laufrad und Gehäuse im Bereich von 2 mm. Im Bereich der axialen Laufradseiten liegt der Spalt zwischen Laufrad und Gehäuse in einer analogen Größenordnung. Durch diese Gestaltung von dem ein minimales Restvolumen aufweisenden Bereiches im Gehäuse kann die Pumpe sehr schnell und zuverlässig durch ein Spülmedium gereinigt werden. Und mit geringsten Verlusten von Förderproduktteilen an geänderte Förderbedingungen oder Anlagen angepasst werden. Durch die kontinuierliche Rotation des zentrifugalen Laufrades 2 ergibt sich ein pulsationsfreier Betrieb dieser Förderpumpe.The minimized
Durch den minimierten Spalt zwischen Laufrad-Außendurchmesser und Laufradraum nähert sich die Umfangskomponente des Laufrades gleichzeitig der Umfangsgeschwindigkeit an und in Kombination mit einer schrägwinklig, vorzugsweise tangential, zum Laufrad 2 angeordneten Pumpenauslass 13 ergibt sich für diese Kreiselpumpe an deren Austrittsöffnung ein maximal möglicher Staudruck. In Verbindung mit dem drehzahlgeregelten Motor sind große Förderhöhen bei einem minimalen Restvolumen innerhalb des Pumpengehäuses realisierbar.Due to the minimized gap between impeller outer diameter and impeller space, the peripheral component of the impeller simultaneously approaches the peripheral speed and in combination with an obliquely inclined, preferably tangential,
Die berührungsfreie Anordnung des Laufrades innerhalb des Laufradraumes vermeidet dichtend aneinanderliegende Reibungsflächen. Diese Maßnahme verhindert die Erzeugung mechanischer Reibungswärme, verhindert einen Reibverschleiß sowie eine dadurch bedingte Verschmutzung einer Förderflüssigkeit mit abgeriebenen Partikeln und verbessert die Betriebssicherheit durch wesentlich verlängerte Nutzungszeiten. Außerdem werden der Reinigbarkeit entgegenwirkende Dichtspalte vermieden.The non-contact arrangement of the impeller within the impeller space avoids sealingly abutting friction surfaces. This measure prevents the generation of mechanical frictional heat, prevents fretting and consequent contamination of a pumped liquid with abraded particles and improves reliability through significantly extended periods of use. In addition, the cleanability counteracting sealing gaps are avoided.
- 1 =1 =
- Pumpengehäusepump housing
- 2 =2 =
- Radialradradial
- 2.1 =2.1 =
- Nabehub
- 3 =3 =
- Förderkanäleconveying channels
- 4 =4 =
- Pumpeneinlasspump inlet
- 5 =5 =
- regelbarer Antriebadjustable drive
- 6 =6 =
- Laufradraumimpeller chamber
- 7 =7 =
- Temperiereinrichtungtempering
- 7.1 - 7.3=7.1 - 7.3 =
- Kühlräumerefrigerators
- 8 =8 =
- Dichtungsgehäuseseal housing
- 9 =9 =
- Dichtungpoetry
- 10 =10 =
- Welle,Wave,
- 11 =11 =
- Kühlmittelcoolant
- 12 =12 =
- Anlageflächecontact surface
- 13 =13 =
- Pumpenauslasspump outlet
- 14, 15 =14, 15 =
- Anschlüsse für TemperiermittelConnections for temperature control
- 16 =16 =
- Tragelementsupporting member
- 17 =17 =
- Laufradumfangwheel circumference
- 18 =18 =
- Fördervertiefungenconveyor wells
- 19, 20 =19, 20 =
- Deckscheibecover disc
- 21 =21 =
- Fördernutentransporting grooves
- 22 =22 =
- Ausgleichsbohrungenequalization bores
- 23 =23 =
- Laufradeintrittimpeller inlet
- DLA =D LA =
-
Außendurchmesser Radialrad 2Outer
diameter radial wheel 2 - DLRI =D LRI =
-
Innendurchmesser Laufradraum 6Inner
diameter impeller space 6
Claims (20)
- Feed pump with a variable-speed drive (5) for metered dispensing of feed quantity, the feed pump being constructed as a single-stage centrifugal pump with a radial wheel (2) of centrifugal structure, arranged rotationally, without a sealing gap, in an impeller chamber (6) of a pump casing (1), in order to convey a fluid between a pump inlet (4) and a pump outlet (13), the radial wheel (2) being connected to a drive motor of variable rotational speed having a five-digit range of revolutions per minute, the radial wheel (2) receiving the flow centrally, being provided with feed ducts (3) and having an outside diameter of up to 50 mm, characterized in that, for use in a process engineering system with continuous feed quantities, the centrifugal pump is constructed for partial-load operation, the feed quantities of which lie in the range of 0 ml/min to 3600 ml/min and with lifts of 20 m to 300 m, in that an inside diameter (DLR1) of the impeller chamber (6) is constructed to be at most 4% larger than an outside diameter (DLA) of the radial wheel (2), in that a seal (9) is arranged between the impeller chamber (6) and the radial wheel (2) and/or its shaft (10), and in that the impeller chamber (6) is provided on the circumference with one or more pump outlet ducts (13) arranged at an acute angle or tangentially to the outside diameter of the radial wheel.
- Feed pump according to Claim 1, characterized in that the pump casing (1), with a radial wheel (2) arranged in it, has a residual volume equal to or smaller than 50 milliliters in the region between a pump inlet (4) and a pump outlet (13), the cross-sectional areas of which are defined by bearing surfaces of lines to be connected to them.
- Feed pump according to Claim 1 or 2, characterized in that the pump casing (1) is provided with a heat regulating device (7 - 7.3).
- Feed pump according to Claim 3, characterized in that the heat regulating device (7) is constructed as a heat exchanger, and completely or partially surrounds the parts of the pump casing (1) and/or of the impeller chamber (6) contacted by the pumped fluid.
- Feed pump according to one or more of Claims 1 to 4, characterized in that fluid-tight connections extend through the heat regulating casing (7) and connect a system to the impeller chamber (6).
- Feed pump according to one or more of Claims 1 to 5, characterized in that the radial wheel (2) has at least two feed ducts (3), and a plurality of feed depressions (18) are arranged on the outside diameter (DLA) of the radial wheel.
- Feed pump according to Claim 6, characterized in that the feed depressions (18) on the radial wheel (2) are configured as blind bores, pockets or tooth-shaped recesses.
- Feed pump according to Claim 6 or 7, characterized in that the feed ducts (3) are constructed as open depressions in the form of blade channels, grooves or flutes.
- Feed pump according to one of Claims 1 to 8, characterized in that suction-side and/or delivery-side impeller cover discs are provided with feed grooves known per se.
- Feed pump according to one of Claims 1 to 9, characterized in that the number and the arrangement of the inlet orifices of the feed ducts (3) of the radial wheel (2) do not enlarge a radial-wheel inlet diameter.
- Feed pump according to one of Claims 1 to 10, characterized in that a hermetically leak-tight magnet-coupled drive transmits a torque to the radial wheel (2).
- Feed pump according to one of Claims 1 to 11, characterized in that an electric, pneumatic or hydraulic drive is connected to the radial wheel (2).
- Feed pump according to one or more of Claims 1 to 12, characterized in that the drive motor (5) is fastened to the pump device (1) or heat regulating device (7) and is connected by means of a shaft (4) extending through it to the radial wheel (2).
- Feed pump according to one or more of Claims 1 to 12, characterized in that a thermal barrier is arranged between the drive motor (5) and the heat regulating device (7) and/or pump casing (1), and the drive motor (5) is connected to the radial wheel (2) via a shaft (4) which extends through the thermal barrier.
- Feed pump according to one or more of Claims 1 to 14, characterized in that connection zones between the parts of the pump casing (1) and the heat regulating device (7) have a rotationally symmetrical configuration and are sealed relative to one another.
- Feed pump according to one or more of Claims 1 to 15, characterized in that a regulating device is connected to an internal or external volume flow measurement device and generates an adjustable constant volume flow by means of the drive motor (5) independently of the back-pressure of the system.
- Feed pump according to one or more of Claims 1 to 16, characterized in that a variable rotational speed range of the drive motor (5) generates a quantity factor up to the value of 5000 in the switching or regulating range between a minimum and maximum feed quantity.
- Feed pump according to one or more of Claims 1 to 17, characterized in that, in the rotational speed range of the drive motor (5) of 0 to 35 000 revolutions/minute, a centrifugal pump feed pressure lies between 0 and 30 bar.
- Feed pump according to one or more of Claims 1 to 18, characterized in that the radial wheel (2) and the casing of the centrifugal pump are constructed for extreme continuous part-load operation.
- Feed pump according to one or more of Claims 1 to 19, characterized in that the pump, drive motor, switching or regulating device and associated electronic operating, measuring and control elements are combined into a mountable module.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SI200730187T SI2054622T1 (en) | 2006-08-26 | 2007-07-17 | Delivery pump |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102006040130A DE102006040130A1 (en) | 2006-08-26 | 2006-08-26 | Delivery pump for delivery and dosing of fluid materials e.g. chemical, pharmaceutical or cosmetic components, has variable-speed drive and is configured as single-stage centrifugal pump having radial wheel |
PCT/EP2007/006315 WO2008025410A1 (en) | 2006-08-26 | 2007-07-17 | Delivery pump |
Publications (2)
Publication Number | Publication Date |
---|---|
EP2054622A1 EP2054622A1 (en) | 2009-05-06 |
EP2054622B1 true EP2054622B1 (en) | 2009-12-16 |
Family
ID=38610560
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP07786115A Active EP2054622B1 (en) | 2006-08-26 | 2007-07-17 | Delivery pump |
Country Status (13)
Country | Link |
---|---|
US (1) | US8021133B2 (en) |
EP (1) | EP2054622B1 (en) |
JP (1) | JP2010501782A (en) |
CN (1) | CN101506526B (en) |
AT (1) | ATE452292T1 (en) |
AU (1) | AU2007291652B2 (en) |
DE (2) | DE102006040130A1 (en) |
DK (1) | DK2054622T3 (en) |
NO (1) | NO337736B1 (en) |
SI (1) | SI2054622T1 (en) |
TW (1) | TWI345031B (en) |
WO (1) | WO2008025410A1 (en) |
ZA (1) | ZA200900924B (en) |
Families Citing this family (12)
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DE102004022141A1 (en) * | 2004-05-05 | 2005-11-24 | Heidelberger Druckmaschinen Ag | Device for conveying and simultaneously aligning sheets |
US9347458B2 (en) | 2010-12-21 | 2016-05-24 | Pentair Flow Technologies, Llc | Pressure compensating wet seal chamber |
EA027255B1 (en) | 2010-12-21 | 2017-07-31 | ПЕНТЭЙР ФЛОУ ТЕКНОЛОДЖИС, ЭлЭлСи | Pressure compensating wet seal chamber |
CN102828964A (en) * | 2012-09-18 | 2012-12-19 | 杨鑫强 | Porous flywheel pump |
WO2014137206A1 (en) * | 2013-03-07 | 2014-09-12 | Chaushevski Nikola | Rotational chamber pump |
DK3242034T3 (en) * | 2013-03-19 | 2019-08-12 | Flow Control LLC | LOW PROFILE PUMP WITH THE ABILITY TO BE INSTALLED IN VARIOUS CONFIGURATIONS |
JP6428410B2 (en) * | 2015-03-18 | 2018-11-28 | 株式会社島津製作所 | Liquefied carbon dioxide pump and supercritical fluid chromatograph equipped with it |
CN108005912A (en) * | 2016-10-31 | 2018-05-08 | 北京精密机电控制设备研究所 | A kind of high back pressure big flow highway turbine pump |
DE102016225908A1 (en) * | 2016-12-21 | 2018-06-21 | KSB SE & Co. KGaA | Vortex pump |
CN109826798A (en) * | 2017-11-23 | 2019-05-31 | 浙江富莱欧机电有限公司 | A kind of freq uency conversion supercharging pump |
DE102018126395A1 (en) * | 2018-10-23 | 2020-04-23 | Moog Gmbh | Electrohydrostatic drive with an enlarged operating range |
CN115182829B (en) * | 2022-07-15 | 2023-05-12 | 哈尔滨工业大学 | Large-pressure-difference high-rotation-speed floating ring sealing test bed |
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GB203659A (en) * | 1922-09-09 | 1924-03-20 | Unchokeable Pump Ltd | Improvements in and relating to centrifugal pumps |
US1988875A (en) * | 1934-03-19 | 1935-01-22 | Saborio Carlos | Wet vacuum pump and rotor therefor |
DE1115586B (en) * | 1957-07-12 | 1961-10-19 | Eugen Soeding | Channel pump with additional ribs on the outside of the wheel walls |
US3647314A (en) * | 1970-04-08 | 1972-03-07 | Gen Electric | Centrifugal pump |
US3915351A (en) * | 1974-08-19 | 1975-10-28 | Alexander Enrico Kiralfy | Cordless electrically operated centrifugal pump |
US4480592A (en) * | 1982-11-30 | 1984-11-06 | Goekcen Mehmet R | Device for converting energy |
IT1187933B (en) * | 1986-02-25 | 1987-12-23 | Gilardini Spa | ROTARY PUMP FOR LIQUIDS |
US4704071A (en) * | 1986-06-17 | 1987-11-03 | Mccullough Ross M | Method and apparatus for pumping liquids |
US4798176A (en) * | 1987-08-04 | 1989-01-17 | Perkins Eugene W | Apparatus for frictionally heating liquid |
DE3843428C2 (en) * | 1988-12-23 | 1993-12-09 | Klein Schanzlin & Becker Ag | Centrifugal pump impeller with low specific speed |
JPH03111697A (en) * | 1989-09-22 | 1991-05-13 | Jidosha Denki Kogyo Co Ltd | Small centrifugal pump |
US5341768A (en) * | 1993-09-21 | 1994-08-30 | Kinetic Systems, Inc. | Apparatus for frictionally heating liquid |
US5540550A (en) * | 1994-01-21 | 1996-07-30 | Nikkiso Co., Ltd. | Solid impeller for centrifugal pumps |
DE10024955A1 (en) * | 2000-05-22 | 2001-11-29 | Richter Chemie Tech Itt Gmbh | Centrifugal pump with magnetic coupling |
WO2004034405A2 (en) * | 2002-09-26 | 2004-04-22 | Atomix, Llc | Roto-dynamic fluidic system |
US7089886B2 (en) * | 2003-04-02 | 2006-08-15 | Christian Helmut Thoma | Apparatus and method for heating fluids |
US7316501B2 (en) * | 2004-05-20 | 2008-01-08 | Christian Thoma | Apparatus and method for mixing dissimilar fluids |
US7387262B2 (en) * | 2004-05-28 | 2008-06-17 | Christian Thoma | Heat generator |
-
2006
- 2006-08-26 DE DE102006040130A patent/DE102006040130A1/en not_active Withdrawn
-
2007
- 2007-07-17 AT AT07786115T patent/ATE452292T1/en active
- 2007-07-17 AU AU2007291652A patent/AU2007291652B2/en not_active Ceased
- 2007-07-17 JP JP2009525937A patent/JP2010501782A/en active Pending
- 2007-07-17 CN CN2007800317433A patent/CN101506526B/en active Active
- 2007-07-17 SI SI200730187T patent/SI2054622T1/en unknown
- 2007-07-17 DK DK07786115.1T patent/DK2054622T3/en active
- 2007-07-17 WO PCT/EP2007/006315 patent/WO2008025410A1/en active Application Filing
- 2007-07-17 DE DE502007002365T patent/DE502007002365D1/en active Active
- 2007-07-17 EP EP07786115A patent/EP2054622B1/en active Active
- 2007-08-09 TW TW096129312A patent/TWI345031B/en not_active IP Right Cessation
-
2009
- 2009-02-09 ZA ZA2009/00924A patent/ZA200900924B/en unknown
- 2009-02-10 NO NO20090626A patent/NO337736B1/en not_active IP Right Cessation
- 2009-02-26 US US12/393,438 patent/US8021133B2/en active Active
Also Published As
Publication number | Publication date |
---|---|
US20090191065A1 (en) | 2009-07-30 |
ZA200900924B (en) | 2009-12-30 |
CN101506526B (en) | 2011-06-08 |
DE102006040130A1 (en) | 2008-02-28 |
EP2054622A1 (en) | 2009-05-06 |
DE502007002365D1 (en) | 2010-01-28 |
NO337736B1 (en) | 2016-06-13 |
US8021133B2 (en) | 2011-09-20 |
WO2008025410A1 (en) | 2008-03-06 |
NO20090626L (en) | 2009-05-08 |
AU2007291652A1 (en) | 2008-03-06 |
JP2010501782A (en) | 2010-01-21 |
SI2054622T1 (en) | 2010-04-30 |
DK2054622T3 (en) | 2010-04-19 |
CN101506526A (en) | 2009-08-12 |
AU2007291652B2 (en) | 2011-08-18 |
TW200831787A (en) | 2008-08-01 |
TWI345031B (en) | 2011-07-11 |
ATE452292T1 (en) | 2010-01-15 |
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