EP1874632B1 - Method for heat treating a product contained in a package such as a tray - Google Patents
Method for heat treating a product contained in a package such as a tray Download PDFInfo
- Publication number
- EP1874632B1 EP1874632B1 EP06743801A EP06743801A EP1874632B1 EP 1874632 B1 EP1874632 B1 EP 1874632B1 EP 06743801 A EP06743801 A EP 06743801A EP 06743801 A EP06743801 A EP 06743801A EP 1874632 B1 EP1874632 B1 EP 1874632B1
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- EP
- European Patent Office
- Prior art keywords
- pack
- temperature
- gaseous fluid
- volume
- package
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B29/00—Packaging of materials presenting special problems
- B65B29/08—Packaging of edible materials intended to be cooked in the package
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B25/00—Packaging other articles presenting special problems
- B65B25/001—Packaging other articles presenting special problems of foodstuffs, combined with their conservation
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B31/00—Packaging articles or materials under special atmospheric or gaseous conditions; Adding propellants to aerosol containers
- B65B31/04—Evacuating, pressurising or gasifying filled containers or wrappers by means of nozzles through which air or other gas, e.g. an inert gas, is withdrawn or supplied
- B65B31/043—Evacuating, pressurising or gasifying filled containers or wrappers by means of nozzles through which air or other gas, e.g. an inert gas, is withdrawn or supplied the nozzles acting horizontally between an upper and a lower part of the container or wrapper, e.g. between container and lid
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B55/00—Preserving, protecting or purifying packages or package contents in association with packaging
- B65B55/02—Sterilising, e.g. of complete packages
- B65B55/12—Sterilising contents prior to, or during, packaging
- B65B55/19—Sterilising contents prior to, or during, packaging by adding materials intended to remove free oxygen or to develop inhibitor gases, e.g. vapour phase inhibitors
Definitions
- the present invention relates to a method of heat treatment of a product, in particular a food product, contained in a packaging such as a container having at least one deformable wall, in which the product contained in the packaging is heated by carrying it at a desired temperature, a temperature holding step is carried out by allowing the steam produced by the heating to escape through an opening in the package.
- Heating the product serves to promote its conservation. It can be a simple cooking, complete or partial, or a pasteurization or sterilization.
- pasteurization and sterilization are used to destroy certain bacteria by heating, to push back the deadline for consumption of the product.
- the consumable product is in particular a food product, such as vegetables, fruits or other fresh foods, blanched or pre-cooked, or frozen. It can also be cooked dishes, including for example meat or fish, or any food preparation.
- the packaging After heating, the packaging is closed while its content is still hot. During cooling, be it sudden or gradual, the volume of gas contained inside the package decreases which, the wall of the package being deformable, causes deformation thereof. When the package is formed by a flexible bag, this retraction can be a desired effect.
- the European patent no. 1,265,793 recommends that the package be closed only once the temperature of the product it contains has reached a precise value and that the inside of the package is still under pressure so that the package is not deformed after cooling. In fact, the volume of gas in excess pressure during the closure is found after cooling; a volume that correctly fills the normal interior volume of the package.
- This method is of some interest, but it requires on the one hand to monitor very precisely the temperature of the product inside the package, which is extremely difficult on an industrial scale and, on the other hand, of ensure that the opening of the packaging initially has a dimension such that controlled overpressure will be ensured inside the packaging at the time when it is closed.
- the object of the present invention is to propose a different solution to allow a release of steam during heating and to avoid excessive permanent deformation of the deformable wall of the packaging resulting from the heating.
- This goal is achieved thanks to the fact that we introduce a fluid in the package at the end of this temperature maintenance step, and the packaging is completely closed.
- the heating comprises a step of holding at temperature or "chambering" to obtain the value cooker (that is to say a value for cooking desired), pasteurizer or sterilizer desired, and during which let the steam escape.
- a gaseous fluid is introduced into the package to cause an increase in its internal volume by a temporary deformation of its deformable wall and / or cause increased pressure.
- the packaging can then be closed and, when the gas contained inside this package has regained its "normal" volume at room temperature, the packaging will have found a shape close to its initial shape, without excessive deformation.
- the package may be a semi-rigid tray closed with a flexible film and it is possible to choose to inject a slightly insufficient volume of gas so that after cooling, the outer surface of the film is slightly concave, thereby testifying that the product has actually undergone a heat treatment, while the walls of the tray retain their original shape.
- the invention makes it possible to avoid or control the deformations of the package.
- the final form is appreciated at room temperature and at "normal" atmospheric pressure.
- the ambient temperature is the normal storage temperature of the products contained in the package, ie, for frozen products, of the order of -18 ° C., for products stored in a cold room, order of 4 ° C and for products stored without cooling, of the order of 20 ° C.
- the gaseous fluid introduced has a temperature at least close to the temperature of the vapor of the package during the temperature maintenance step.
- the temperature of this fluid can even be used to promote pasteurization or sterilization.
- the gaseous fluid is a neutral gas, such as nitrogen, a gas mixture nitrogen / oxygen dioxide or air, preferably filtered.
- This gaseous fluid is chosen according to the products treated.
- the introduction of the gaseous fluid is managed so that when the package once closed will return to ambient temperature, the wall thereof is substantially undeformed or deformed in a controlled manner. It is possible to proceed empirically, by introducing, under the same conditions of introduction, different volumes of gaseous fluids in different packages, and then determining what is the volume of fluid introduced which leads to the desired final shape, so as to retain this volume as to be introduced industrially.
- the evaluation of the volume of vapor that escapes can be carried out by direct measurement or, indirectly, depending on the time during which the steam escapes, and taking into account the size of the opening of the package.
- the process can then be industrialized.
- the difference measured in volume may for example be of the order of ⁇ 5% to ⁇ 10%.
- the tray of the figure 1 comprises a receptacle portion 1 and a cover wall 2, such as a peelable film, disposed across the opening of this receptacle.
- Food products such as, for example, peeled potatoes 3 are arranged in this tray.
- this tray is made of plastic or aluminum, or a complex such as, for example, cardboard / plastic, cardboard / aluminum or aluminum / plastic and has a relatively thin wall, whose thickness is by example between 0.5 and 2 mm.
- the upper wall of this tray is formed by the film 2, which is sealed on the edge of the tray formed by the flange 1A of the receptacle.
- the materials chosen for the receptacle and the film are of all types known for this type of trays, for example based on aluminum or plastic, in particular polypropylene, possibly loaded as recommended by the patent application. EP No. 1,313,651 .
- the film constituting the upper wall 2 forms a wall which is easily deformable.
- the wall of the receptacle 1 is relatively thin, in fact all the walls of the tray are deformable, but the film 2 is more.
- this tray Before subjecting the product 3 contained in the tray to the heat treatment, this tray is closed incompletely, leaving an opening. On the figure 2 this opening is formed by an interruption 4A of the sealing bead 4 between two walls of the package, in this case between the rim 1A of the receptacle and the film 2.
- the opening 5 is formed by a hole in a wall of the package, in this case in the film 2, while the sealing bead 4 between the film 2 and the rim of the receptacle is continuous.
- the opening through which the vapor can escape during sealing has relatively small dimensions so that the inside of the packaging is put under overpressure during heating, because this overpressure favors the heart heating of the products. food.
- the vapor that emerges comes from, on the one hand, the vaporization of the water initially contained in the package, in particular in the products which are arranged inside, and on the other hand the expansion of the gas initially contained in the package.
- these two sources of off-gas are designated by "steam".
- the tray of Figures 1 and 2 is placed in a heating chamber 6. It is in particular a microwave oven or tunnel inside which microwaves are emitted by a generator.
- the tray is carried by a support 8.
- the support 8 may be a conveyor whose path passes through the interior of this tunnel which has an inlet and an outlet for the tray which are not shown.
- several trays can be simultaneously in the tunnel, the length of the latter and the advancement of the conveyor can be adjusted so that the parking time of a tray in the enclosure is sufficient to allow the desired heating .
- the tray and its contents are subjected to heating to, on the one hand, allow a rise in temperature of the product contained in the tray and, on the other hand, perform a temperature maintenance step.
- the temperature maintenance stage is conducted in such a way that the food product remains maintained at a temperature of the order of 80 ° C. to 100 ° C. for a period of given time, for example of the order of 3 to 5 minutes.
- the product is brought to a temperature of the order of 120 ° C to 130 ° C for the necessary time, for example of the order of 3 to 5 minutes.
- the steps of heating and temperature maintenance can be performed in the same microwave chamber. Alternatively, two microwave tunnels arranged end to end may be used, the first using a larger power to perform the temperature rise step, while the second only carries out the temperature holding step, with less power.
- heating by microwaves is only one example, knowing that other heating modes can be used, in particular heating by other electromagnetic waves such as high frequency waves, or else steam heating.
- the temperature maintenance step can be carried out as shown in FIG. figure 4 .
- its most deformable wall in this case the film 2
- the excess steam V escapes through the opening 4A.
- a gaseous fluid is introduced into the package as shown in FIG. figure 5 .
- This introduction can be carried out in the heating chamber as shown in FIG. figure 5 . It should be noted, however, that it can also be performed after the temperature maintenance step at the outlet of the heating chamber.
- this introduction of the fluid F is carried out by an injection cannula 9 which is engaged in the opening 4A.
- This cannula is connected to a gaseous fluid supply system represented symbolically by a square 10. It should be noted that the introduction of the cannula into the opening 4A is easy since, under the effect of the vapor evolution V, this opening is at least ajar, that is to say that the film 2 is kept locally at a distance from the flange 1A.
- the introduction of a cannula is also easy, from an opening formed on one of the walls of the container, as the opening 5 of the figure 3 . It should be noted that, because of the overpressure in the package, the film 2 is then remote products contained in the package, so that the introduction of the cannula does not damage these products.
- the film 2 is further deformed, further increasing the interior volume of the package.
- the package After the introduction of the gaseous fluid, the package is completely closed. On the figure 6 this closing is performed by completing the weld bead 4, as indicated by the hatched area 4B.
- the opening 4A can in particular be made and closed as recommended by the French patent application no. 2,852,921 .
- this closure is achieved by closing the piercing 5 with a pellet 5 '.
- the gaseous fluid is introduced through the opening through which the steam is allowed to escape during holding at temperature.
- another port may be used.
- the steam can be introduced by a cannula forming a needle which, for the introduction of the gaseous fluid, pierces a wall of the package. The pierce thus formed is then closed, for example by placing a pellet across this piercing; the opening through which the vapor V has escaped is also closed, for example by sealing or by affixing a pellet.
- the gaseous fluid which is introduced into the package at the end of the temperature maintenance stage has a temperature which is between 80% and 130%, preferably between 90% and 110%, of the temperature of the steam during the temperature holding step.
- a gaseous fluid temperature at least close to the temperature of the steam is advantageous.
- a higher temperature is chosen for this gaseous fluid, especially when it is close to 130% of the temperature of the vapor, one can use the gaseous fluid and heated to promote cooking, pasteurization or sterilization.
- Tests carried out under different conditions of introduction of vapor packaging at the end of the temperature maintenance stage make it possible to determine what are the optimal conditions for introducing the gaseous fluid so that, once the package is closed, and after the cooling of its contents, the pressure balance between the inside and the outside of the package is such that the walls of this package remain substantially undeformed with respect to the figure 1 or that they are only slightly deformed in the desired manner, only the film 2, for example, being slightly concave.
- the conditions for introducing the gaseous fluid are defined by parameters such as: the temperature of the gaseous fluid introduced, its composition, the volume of the introduced fluid or, to indirectly determine this volume, the duration of the introduction step, the flow of fluid at the outlet of the injection system and entering the packaging, ....
- Tests may also be performed for different types of openings of the package, knowing that the size of the opening obviously influences the volume of vapor escaping from the package during the temperature maintenance step.
- This volume of vapor can be indirectly determined by knowing the time during which the evolution of gas takes place, and the dimensions of the opening, knowing that the pressure of this vapor is generally known elsewhere.
- a volume of gaseous fluid corresponding at least approximately to the volume of vapor that escapes from the packaging during heating and temperature maintenance is introduced.
- these volumes of vapor and gaseous fluid can be determined by tests, empirically and by comparison between different tests.
- volume that escapes For example, one can evaluate the volume that escapes and then introduce a corresponding volume. It is also possible to test under the same conditions by introducing different volumes of gaseous fluid and by comparing the initial mass of the package with its content and mass after closure and cooling which, by calculation gives the difference between the volume of vapor that escaped and the volume of gas introduced.
- the volume of gaseous fluid introduced is determined such that this volume is substantially equal to the volume of vapor that escapes from the packaging during heating and temperature maintenance, preferably being less than this volume.
- the volume of gaseous fluid introduced into the package may be less than 5 to 10% of the volume of vapor that escaped from the latter.
- this concavity is then light enough not to constitute a troublesome deformation for the consumer but, as indicated above, it has certain advantages.
- this concavity is light enough for the package to be considered “substantially undeformed" after cooling.
- the volume of gaseous fluid introduced into the packaging and the volume of vapor that escaped from it are compared under conditions allowing this comparison, in particular by computationally reducing these volumes to volumes equivalent to the same temperature, in particular the ambient temperature.
- the gaseous fluid is introduced into the package, causing deformation of the deformable wall, and the package is closed when it is found that this deformation has reached a given level.
- the introduction of the gaseous fluid can cause deformation of the film 2 (see figure 5 ).
- the level of the deformation is in particular reflected by the amplitude thereof.
- this wall also deforms, but to a lesser extent.
- the flow of steam escaping through the opening 4A or 5 is stabilized, so that the deformation of the film 2 also stabilizes. It is possible to choose to measure the level of deformation at which the package is closed in a relative manner, by comparison between the stabilized deformation during temperature maintenance and the deformation obtained just before closing, after introduction of the gaseous fluid.
Abstract
Description
La présente invention concerne un procédé de traitement thermique d'un produit, en particulier un produit alimentaire, contenu dans un emballage tel qu'une barquette ayant au moins une paroi déformable, dans lequel on chauffe le produit contenu dans l'emballage en le portant à une temperature souhaitée, on réalise une étape de maintien à temperature en laissant la vapeur produite par le chauffage s'échapper par une ouverture de l'emballage.The present invention relates to a method of heat treatment of a product, in particular a food product, contained in a packaging such as a container having at least one deformable wall, in which the product contained in the packaging is heated by carrying it at a desired temperature, a temperature holding step is carried out by allowing the steam produced by the heating to escape through an opening in the package.
On connaît déjà un procédé de ce type, par la demande de brevet français n°
Le chauffage du produit sert à favoriser sa conservation. Il peut s'agir une simple cuisson, complète ou partielle, ou bien d'une pasteurisation, voire d'une stérilisation.Heating the product serves to promote its conservation. It can be a simple cooking, complete or partial, or a pasteurization or sterilization.
Comme on le sait, la pasteurisation et la stérilisation servent à détruire certaines bactéries par chauffage, pour repousser la date limite de consommation du produit.As is known, pasteurization and sterilization are used to destroy certain bacteria by heating, to push back the deadline for consumption of the product.
Le produit consommable est en particulier un produit alimentaire, tels que des légumes, des fruits ou d'autres aliments frais, blanchis ou pré-cuits, ou encore surgelés. Il peut également s'agir de plats cuisinés, comprenant par exemple de la viande ou du poisson, ou bien d'une préparation alimentaire quelconque.The consumable product is in particular a food product, such as vegetables, fruits or other fresh foods, blanched or pre-cooked, or frozen. It can also be cooked dishes, including for example meat or fish, or any food preparation.
On sait que lors du chauffage d'un produit de ce type, de la vapeur est produite. Il s'agit notamment de vapeur d'eau, produite par l'eau qui s'évapore du produit chauffé sous l'effet de la température. De plus, le gaz initialement contenu dans l'emballage est dilaté du fait de l'élévation de température, le volume de gaz en excès formant une partie de la vapeur que l'on laisse s'échapper de l'ouverture de l'emballage lors du chauffage pour éviter qu'il ne se produise dans ce dernier une surpression qui pourrait conduire à un éclatement ou en tout cas à une détérioration de l'emballage, et à un échec du procédé de chauffage.It is known that when heating a product of this type, steam is produced. These include water vapor, produced by water evaporating from the heated product under the effect of temperature. In addition, the gas initially contained in the package is dilated due to the rise in temperature, the excess gas volume forming part of the vapor that is allowed to escape from the opening of the package during heating to prevent it from occurring in the latter an overpressure that could lead to bursting or in any case to a deterioration of the packaging, and a failure of the heating process.
La demande de brevet français précitée s'applique notamment à un emballage constitué par une barquette ou bien par une poche souple. Selon cette demande de brevet, l'ouverture de l'emballage par laquelle la vapeur peut s'échapper est formée par une zone provisoirement non soudée entre deux parois de cet emballage, et cette ouverture est fermée à l'issue du chauffage par une soudure.The aforementioned French patent application applies in particular to a package consisting of a tray or a flexible bag. According to this patent application, the opening of the package through which the steam can escape is formed by a zone provisionally not welded between two walls of this package, and this opening is closed at the end of the heating by welding.
A l'issue du chauffage, l'emballage est donc refermé alors que son contenu est encore chaud. Lors du refroidissement, qu'il soit brutal ou progressif, le volume du gaz contenu à l'intérieur de l'emballage diminue ce qui, la paroi de l'emballage étant déformable, provoque une déformation de celle-ci. Lorsque l'emballage est formé par une poche souple, cette rétractation peut être un effet recherché.After heating, the packaging is closed while its content is still hot. During cooling, be it sudden or gradual, the volume of gas contained inside the package decreases which, the wall of the package being deformable, causes deformation thereof. When the package is formed by a flexible bag, this retraction can be a desired effect.
Il n'en va pas de même lorsque l'emballage est formé par une barquette, qui doit normalement présenter une forme sensiblement parallélépipédique. En effet, le consommateur serait perturbé par la déformation d'un tel emballage.This is not the case when the packaging is formed by a tray, which should normally have a substantially parallelepiped shape. Indeed, the consumer would be disturbed by the deformation of such a package.
Pour tenter d'éviter de telles déformations, le brevet européen n°
Cette méthode présente un certain intérêt, mais elle impose d'une part de surveiller très précisément la température du produit à l'intérieur de l'emballage, ce qui est extrêmement difficile sur un plan industriel et, d'autre part, de s'assurer que l'ouverture de l'emballage a initialement une dimension telle qu'une surpression maîtrisée sera assurée à l'intérieur de l'emballage au moment où celui-ci sera refermé.This method is of some interest, but it requires on the one hand to monitor very precisely the temperature of the product inside the package, which is extremely difficult on an industrial scale and, on the other hand, of ensure that the opening of the packaging initially has a dimension such that controlled overpressure will be ensured inside the packaging at the time when it is closed.
Ainsi, cette méthode présente des difficultés pratiques de mise en oeuvre.Thus, this method presents practical difficulties of implementation.
La présente invention a pour but de proposer une solution différente pour permettre un dégagement de vapeur lors du chauffage et éviter une déformation permanente excessive de la paroi déformable de l'emballage issue du chauffage.The object of the present invention is to propose a different solution to allow a release of steam during heating and to avoid excessive permanent deformation of the deformable wall of the packaging resulting from the heating.
Ce but est atteint grâce au fait que l' on introduit un fluide gazeux dans l'emballage à la fin de cette étape de maintien à température, et on ferme totalement l'emballage.This goal is achieved thanks to the fact that we introduce a fluid in the package at the end of this temperature maintenance step, and the packaging is completely closed.
Selon l'invention, le chauffage comprend une étape de maintien à température ou de « chambrage » permettant d'obtenir la valeur cuisatrice (c'est-à-dire une valeur permettant la cuisson désirée), pasteurisatrice ou stérilisatrice souhaitée, et pendant laquelle on laisse la vapeur s'échapper. A la fin de cette étape, un fluide gazeux est introduit dans l'emballage pour provoquer une augmentation de son volume intérieur par une déformation provisoire de sa paroi déformable et/ou provoquer une surpression augmentée. L'emballage peut alors être fermé et, lorsque le gaz contenu à l'intérieur de cet emballage aura retrouvé son volume « normal » à température ambiante, l'emballage aura retrouvé une forme voisine de sa forme initiale, sans déformation excessive. Comme on le verra dans la suite, on peut déterminer le volume de gaz introduit à la fin de l'étape de maintien à température de telle sorte que la forme finale de l'emballage soit sensiblement sa forme initiale, sans déformation notable par rapport à elle. On peut aussi déterminer ce volume de telle sorte que la forme finale soit volontairement légèrement différente de la forme initiale. Par exemple, l'emballage peut être une barquette semi-rigide fermée par un film souple et on peut choisir d'injecter un volume de gaz légèrement insuffisant pour qu'après refroidissement, la surface extérieure du film soit légèrement concave, témoignant ainsi que le produit a effectivement subi un traitement thermique, tandis que les parois de la barquette conservent leur forme initiale.According to the invention, the heating comprises a step of holding at temperature or "chambering" to obtain the value cooker (that is to say a value for cooking desired), pasteurizer or sterilizer desired, and during which let the steam escape. At the end of this step, a gaseous fluid is introduced into the package to cause an increase in its internal volume by a temporary deformation of its deformable wall and / or cause increased pressure. The packaging can then be closed and, when the gas contained inside this package has regained its "normal" volume at room temperature, the packaging will have found a shape close to its initial shape, without excessive deformation. As will be seen in the following, it is possible to determine the volume of gas introduced at the end of the temperature holding step such that the final shape of the package is substantially its initial shape, without significant deformation with respect to she. This volume can also be determined so that the final shape is intentionally slightly different from the initial shape. For example, the package may be a semi-rigid tray closed with a flexible film and it is possible to choose to inject a slightly insufficient volume of gas so that after cooling, the outer surface of the film is slightly concave, thereby testifying that the product has actually undergone a heat treatment, while the walls of the tray retain their original shape.
En d'autres termes, l'invention permet d'éviter ou de maîtriser les déformations de l'emballage. La forme finale est appréciée à température ambiante et à la pression atmosphérique « normale ».In other words, the invention makes it possible to avoid or control the deformations of the package. The final form is appreciated at room temperature and at "normal" atmospheric pressure.
Au sens de la présente invention, la température ambiante est la température normale de stockage des produits contenus dans l'emballage soit, pour des produits surgelés, de l'ordre de - 18°C, pour les produits stockés en chambre froide, de l'ordre de 4°C et pour des produits stockés sans refroidissement, de l'ordre de 20°C.For the purposes of the present invention, the ambient temperature is the normal storage temperature of the products contained in the package, ie, for frozen products, of the order of -18 ° C., for products stored in a cold room, order of 4 ° C and for products stored without cooling, of the order of 20 ° C.
Avantageusement, le fluide gazeux introduit a une température au moins voisine de la température de la vapeur de l'emballage pendant l'étape de maintien à température.Advantageously, the gaseous fluid introduced has a temperature at least close to the temperature of the vapor of the package during the temperature maintenance step.
On évite ainsi un choc thermique entre le contenu de l'emballage et le fluide gazeux introduit dans ce dernier. De plus, on s'assure ainsi que ce fluide gazeux corresponde, du point de vue de sa température, aux critères de cuisson, de pasteurisation ou de stérilisation recherchés. La température de ce fluide peut même être mise à profit pour favoriser la pasteurisation ou la stérilisation.This avoids a thermal shock between the contents of the packaging and the gaseous fluid introduced into the latter. In addition, it ensures that the gaseous fluid corresponds, from the point of view of its temperature, the desired cooking, pasteurization or sterilization criteria. The temperature of this fluid can even be used to promote pasteurization or sterilization.
Avantageusement, le fluide gazeux est un gaz neutre, tel que de l'azote, un mélange gazeux azote/dioxyde d'oxygène ou de l'air, avantageusement filtré. Ce fluide gazeux est choisi en fonction des produits traités.Advantageously, the gaseous fluid is a neutral gas, such as nitrogen, a gas mixture nitrogen / oxygen dioxide or air, preferably filtered. This gaseous fluid is chosen according to the products treated.
L'introduction du fluide gazeux est gérée de telle sorte que, lorsque l'emballage une fois fermé retrouvera la température ambiante, la paroi de celui-ci soit sensiblement non déformée ou déformée de manière maîtrisée. On peut procéder de manière empirique, en introduisant, dans les mêmes conditions d'introduction, différents volumes de fluides gazeux dans différents emballages, et en déterminant ensuite quel est le volume de fluide introduit qui conduit à la forme finale souhaitée, de manière à retenir ce volume comme devant être introduit de manière industrielle.The introduction of the gaseous fluid is managed so that when the package once closed will return to ambient temperature, the wall thereof is substantially undeformed or deformed in a controlled manner. It is possible to proceed empirically, by introducing, under the same conditions of introduction, different volumes of gaseous fluids in different packages, and then determining what is the volume of fluid introduced which leads to the desired final shape, so as to retain this volume as to be introduced industrially.
On peut également évaluer le volume de vapeur qui s'échappe de l'emballage pendant le chauffage et le maintien à température et introduire dans cet emballage un volume de fluide gazeux correspondant. L'évaluation du volume de vapeur qui s'échappe peut être réalisée par mesure directe ou, indirectement, en fonction de la durée pendant laquelle la vapeur s'échappe, et en tenant compte de la dimension de l'ouverture de l'emballage.It is also possible to evaluate the volume of vapor that escapes from the packaging during heating and temperature maintenance and to introduce into this package a corresponding volume of gaseous fluid. The evaluation of the volume of vapor that escapes can be carried out by direct measurement or, indirectly, depending on the time during which the steam escapes, and taking into account the size of the opening of the package.
On peut encore, à partir d'essais, déterminer le volume de fluide devant être injecté en fonction de la déformation qu'il provoque sur la paroi de l'emballage.It is also possible, from tests, to determine the volume of fluid to be injected as a function of the deformation it causes on the wall of the package.
Ayant ainsi déterminé les meilleures conditions d'introduction du fluide gazeux, en particulier ayant trait à la durée pendant laquelle ce fluide est introduit ou à la quantité de fluide directement mesurée qui est introduite, on peut ensuite industrialiser le procédé.Having thus determined the best conditions for introducing the gaseous fluid, in particular relating to the duration during which this fluid is introduced or to the directly measured quantity of fluid that is introduced, the process can then be industrialized.
Pour obtenir une déformation maîtrisée, d'amplitude limitée et affectant seulement certaines zones (film) de l'emballage, on peut injecter une quantité de gaz légèrement différente de celle qui serait nécessaire pour éviter une déformation et avantageusement légèrement inférieure à cette dernière pour obtenir une déformation concave maîtrisée. La différence mesurée en volume peut par exemple être de l'ordre de ± 5 % à ± 10%.To obtain controlled deformation, of limited amplitude and affecting only certain zones (film) of the package, it is possible to inject a quantity of gas slightly different from that which would be necessary to avoid deformation and advantageously slightly less than the latter to obtain a controlled concave deformation. The difference measured in volume may for example be of the order of ± 5% to ± 10%.
L'invention sera bien comprise et ses avantages apparaîtront mieux à la lecture de la description détaillée qui suit, d'un mode de réalisation représenté à titre d'exemple non limitatif. La description se réfère aux dessins annexés sur lesquels :
- la
figure 1 est une vue en coupe verticale d'une barquette contenant un produit, avant le traitement thermique ; - les
figures 2 et 3 sont des vues de dessus d'une telle barquette, pour deux variantes de réalisation de son ouverture ; - la
figure 4 illustre l'étape de chauffage du produit contenu dans l'emballage ; - la
figure 5 illustre l'introduction d'un fluide gazeux à l'intérieur de l'emballage ; et - les
figures 6 et 7 montrent la fermeture finale de l'emballage, pour les deux variantes desfigures 2 et 3 .
- the
figure 1 is a vertical sectional view of a container containing a product, before the heat treatment; - the
Figures 2 and 3 are top views of such a tray, for two variants of its opening; - the
figure 4 illustrates the step of heating the product contained in the package; - the
figure 5 illustrates the introduction of a gaseous fluid inside the package; and - the
Figures 6 and 7 show the final closure of the packaging, for both variants of theFigures 2 and 3 .
La barquette de la
Le film constituant la paroi supérieure 2 forme une paroi qui est aisément déformable. Toutefois, dans la mesure où la paroi du réceptacle 1 est relativement fine, en réalité toutes les parois de la barquette sont déformables, mais le film 2 l'est davantage.The film constituting the
Avant de soumettre le produit 3 contenu dans la barquette au traitement thermique, on ferme cette barquette de manière incomplète, en laissant une ouverture. Sur la
Sur la
De manière générale, l'ouverture par laquelle la vapeur peut s'échapper lors du scellage a des dimensions relativement faibles pour que l'intérieur de l'emballage soit mis en surpression lors du chauffage, car cette surpression favorise le chauffage à coeur des produits alimentaires.In general, the opening through which the vapor can escape during sealing has relatively small dimensions so that the inside of the packaging is put under overpressure during heating, because this overpressure favors the heart heating of the products. food.
Comme indiqué précédemment, la vapeur qui se dégage provient, d'une part, de la vaporisation de l'eau contenue initialement dans l'emballage, en particulier dans les produits qui sont disposés à l'intérieur, et d'autre part de la dilatation du gaz contenu initialement dans l'emballage. Au sens de la présentes invention, on désigne ces deux sources de gaz de dégagement par « vapeur ».As indicated above, the vapor that emerges comes from, on the one hand, the vaporization of the water initially contained in the package, in particular in the products which are arranged inside, and on the other hand the expansion of the gas initially contained in the package. For the purpose of the present invention, these two sources of off-gas are designated by "steam".
Sur la
La barquette et son contenu sont soumis au chauffage pour, d'une part, permettre une montée en température du produit contenu dans la barquette et, d'autre part, réaliser une étape de maintien en température. Classiquement, pour une pasteurisation, l'étape de maintien en température est conduite de telle sorte que le produit alimentaire reste maintenu à une température de l'ordre de 80°C à 100°C pendant un temps donné, par exemple de l'ordre 3 à 5 minutes. Pour une stérilisation, on porte le produit à une température de l'ordre de 120°C à 130°C pendant la durée nécessaire, par exemple de l'ordre de 3 à 5 minutes. Les étapes de chauffage et de maintien en température peuvent être réalisées dans la même enceinte à micro-ondes. En variante, on peut utiliser deux tunnels à micro-ondes disposés bout à bout, le premier utilisant une puissance plus importante pour réaliser l'étape de montée en température, tandis que le deuxième ne réalise que l'étape de maintien à température, avec une puissance moins importante.The tray and its contents are subjected to heating to, on the one hand, allow a rise in temperature of the product contained in the tray and, on the other hand, perform a temperature maintenance step. Conventionally, for a pasteurization, the temperature maintenance stage is conducted in such a way that the food product remains maintained at a temperature of the order of 80 ° C. to 100 ° C. for a period of given time, for example of the order of 3 to 5 minutes. For sterilization, the product is brought to a temperature of the order of 120 ° C to 130 ° C for the necessary time, for example of the order of 3 to 5 minutes. The steps of heating and temperature maintenance can be performed in the same microwave chamber. Alternatively, two microwave tunnels arranged end to end may be used, the first using a larger power to perform the temperature rise step, while the second only carries out the temperature holding step, with less power.
Bien entendu, le chauffage par des micro-ondes n'est qu'un exemple, sachant que d'autres modes de chauffage peuvent être utilisés, en particulier un chauffage par d'autres ondes électromagnétiques telles que des ondes à haute fréquence, ou bien un chauffage à la vapeur.Of course, heating by microwaves is only one example, knowing that other heating modes can be used, in particular heating by other electromagnetic waves such as high frequency waves, or else steam heating.
L'étape de maintien en température peut être réalisée conformément à ce que montre la
A la fin de l'étape de maintien en température, on introduit un fluide gazeux dans l'emballage comme le montre la
Dans l'exemple de la
L'introduction d'une canule est également aisée, à partir d'une ouverture formée sur l'une des parois du récipient, comme l'ouverture 5 de la
Toutefois, au lieu d'introduire une canule dans l'ouverture, on peut disposer un système d'injection de gaz au voisinage immédiat de cette ouverture, qu'il s'agisse de l'ouverture 4A ou de l'ouverture 5, en faisant en sorte que la pression et le débit de fluide gazeux soient suffisants pour que celui-ci pénètre dans l'emballage.However, instead of introducing a cannula into the opening, it is possible to have a gas injection system in the immediate vicinity of this opening, whether it be the
Comme on le voit en comparant les
Après l'introduction du fluide gazeux, on ferme totalement l'emballage. Sur la
Sur la
Avantageusement, comme indiqué précédemment, le fluide gazeux est introduit par l'ouverture par laquelle on laisse la vapeur s'échapper pendant le maintien à température. En variante, on peut utiliser un autre orifice. En particulier, on peut introduire la vapeur par une canule formant une aiguille qui, pour l'introduction du fluide gazeux, perce une paroi de l'emballage. Le perçage ainsi formé est ensuite refermé, par exemple en disposant une pastille en travers de ce perçage ; l'ouverture par laquelle la vapeur V s'est échappée est également fermée, par exemple par scellage ou par apposition d'une pastille.Advantageously, as indicated above, the gaseous fluid is introduced through the opening through which the steam is allowed to escape during holding at temperature. Alternatively, another port may be used. In particular, the steam can be introduced by a cannula forming a needle which, for the introduction of the gaseous fluid, pierces a wall of the package. The pierce thus formed is then closed, for example by placing a pellet across this piercing; the opening through which the vapor V has escaped is also closed, for example by sealing or by affixing a pellet.
Avantageusement, le fluide gazeux qui est introduit dans l'emballage à la fin de l'étape de maintien en température a une température qui est comprise entre 80 % et 130 %, de préférence entre 90 % et 110%, de la température de la vapeur pendant l'étape de maintien à température. Comme indiqué précédemment, le choix d'une température de fluide gazeux au moins voisine de la température de la vapeur est avantageux. Lorsque l'on choisit même une température plus élevée pour ce fluide gazeux, en particulier lorsque celle-ci est voisine de 130 % de la température de la vapeur, on peut utiliser le fluide gazeux ainsi chauffé pour favoriser la cuisson, la pasteurisation ou la stérilisation.Advantageously, the gaseous fluid which is introduced into the package at the end of the temperature maintenance stage has a temperature which is between 80% and 130%, preferably between 90% and 110%, of the temperature of the steam during the temperature holding step. As indicated above, the choice of a gaseous fluid temperature at least close to the temperature of the steam is advantageous. When even a higher temperature is chosen for this gaseous fluid, especially when it is close to 130% of the temperature of the vapor, one can use the gaseous fluid and heated to promote cooking, pasteurization or sterilization.
Des essais réalisés dans différentes conditions d'introduction de vapeur l'emballage à la fin de l'étape de maintien en température permettent de déterminer quelles sont les conditions optimales d'introduction du fluide gazeux pour que, une fois l'emballage fermé, et après le refroidissement de son contenu, l'équilibre des pressions entre l'intérieur et l'extérieur de l'emballage soit tel que les parois de cet emballage restent sensiblement non déformées par rapport à ce que montre la
Les conditions d'introduction du fluide gazeux sont définies par des paramètres tels que : la température du fluide gazeux introduit, sa composition, le volume du fluide introduit ou bien, pour déterminer indirectement ce volume, la durée de l'étape d'introduction, le débit de fluide en sortie du système d'injection et entrant dans l'emballage, ....The conditions for introducing the gaseous fluid are defined by parameters such as: the temperature of the gaseous fluid introduced, its composition, the volume of the introduced fluid or, to indirectly determine this volume, the duration of the introduction step, the flow of fluid at the outlet of the injection system and entering the packaging, ....
Des essais peuvent également être réalisés pour différents types d'ouvertures de l'emballage, sachant que la taille de l'ouverture influence évidemment le volume de vapeur qui s'échappe de l'emballage pendant le l'étape de maintien en température. On peut déterminer indirectement ce volume de vapeur en connaissant le temps pendant lequel le dégagement gazeux se produit, et les dimensions de l'ouverture, sachant que l'on connaît généralement par ailleurs la pression de cette vapeur.Tests may also be performed for different types of openings of the package, knowing that the size of the opening obviously influences the volume of vapor escaping from the package during the temperature maintenance step. This volume of vapor can be indirectly determined by knowing the time during which the evolution of gas takes place, and the dimensions of the opening, knowing that the pressure of this vapor is generally known elsewhere.
Ainsi, avantageusement, on introduit un volume de fluide gazeux correspondant au moins approximativement au volume de vapeur qui s'échappe de l'emballage pendant le chauffage et le maintien à température.Thus, advantageously, a volume of gaseous fluid corresponding at least approximately to the volume of vapor that escapes from the packaging during heating and temperature maintenance is introduced.
Comme indiqué précédemment, ces volumes de vapeur et de fluide gazeux peuvent être déterminés par des essais, de manière empirique et par comparaison entre différents essais.As indicated previously, these volumes of vapor and gaseous fluid can be determined by tests, empirically and by comparison between different tests.
On peut par exemple évaluer le volume qui s'échappe et introduire ensuite un volume correspondant. On peut également procéder à des essais dans les'mêmes conditions en introduisant différents volumes de fluide gazeux et en comparant la masse initiale de l'emballage avec son contenu et la masse après fermeture et refroidissement ce qui, par calcul donne la différence entre le volume de vapeur qui s'est échappé et le volume de gaz introduit.For example, one can evaluate the volume that escapes and then introduce a corresponding volume. It is also possible to test under the same conditions by introducing different volumes of gaseous fluid and by comparing the initial mass of the package with its content and mass after closure and cooling which, by calculation gives the difference between the volume of vapor that escaped and the volume of gas introduced.
Avantageusement, on détermine le volume de fluide gazeux introduit de telle sorte que ce volume soit sensiblement égal au volume de vapeur qui s'échappe de l'emballage pendant le chauffage et le maintien à température, en étant de préférence inférieur à ce volume. Par exemple, le volume de fluide gazeux introduit dans l'emballage peut être inférieur de l'ordre de 5 à 10 % au volume de vapeur qui s'est échappé de ce dernier. Ceci permet de faire en sorte que, après le refroidissement du contenu de l'emballage, la paroi la plus déformable de ce dernier, en particulier le film 2 qui forme la paroi supérieure, présente une légère concavité, ce qui favorise les étapes de manipulations ultérieures de l'emballage, en particulier l'empilement de plusieurs emballages de ce type. Cette paroi qu'on garde légèrement concave peut également être le fond du récipient. Cette concavité est alors suffisamment légère pour ne pas constituer une déformation gênante pour le consommateur mais, comme indiqué précédemment, elle présente certains avantages. Au sens de la présente invention, cette concavité est suffisamment légère pour que l'emballage soit considéré comme étant « sensiblement non déformé » à l'issue du refroidissement.Advantageously, the volume of gaseous fluid introduced is determined such that this volume is substantially equal to the volume of vapor that escapes from the packaging during heating and temperature maintenance, preferably being less than this volume. For example, the volume of gaseous fluid introduced into the package may be less than 5 to 10% of the volume of vapor that escaped from the latter. This makes it possible to ensure that, after the cooling of the contents of the package, the most deformable wall of the latter, in particular the
Le volume de fluide gazeux introduit dans l'emballage et le volume de vapeur qui s'en est échappé sont comparés dans des conditions permettant cette comparaison, en particulier en ramenant par calcul ces volumes à des volumes équivalents à une même température, en particulier la température ambiante.The volume of gaseous fluid introduced into the packaging and the volume of vapor that escaped from it are compared under conditions allowing this comparison, in particular by computationally reducing these volumes to volumes equivalent to the same temperature, in particular the ambient temperature.
En variante, on introduit le fluide gazeux dans l'emballage en provoquant une déformation de la paroi déformable, et on ferme l'emballage lorsque l'on constate que cette déformation a atteint un niveau donné.As a variant, the gaseous fluid is introduced into the package, causing deformation of the deformable wall, and the package is closed when it is found that this deformation has reached a given level.
Comme on l'a indiqué précédemment, l'introduction du fluide gazeux peut provoquer une déformation du film 2 (voir
On a indiqué précédemment que, lors du chauffage, cette paroi se déforme également, mais de manière moindre. Lors de l'étape de maintien à température, le débit de vapeur s'échappant par l'ouverture 4A ou 5 se stabilise, de sorte que la déformation du film 2 se stabilise également. On peut choisir de mesurer le niveau de déformation auquel on ferme l'emballage de manière relative, par comparaison entre la déformation stabilisée lors du maintien en température et la déformation obtenue juste avant la fermeture, après introduction du fluide gazeux.It has been indicated previously that, during heating, this wall also deforms, but to a lesser extent. During the temperature holding step, the flow of steam escaping through the
On peut encore choisir d'introduire le fluide gazeux dans l'emballage pendant une durée déterminée, à l'issue de laquelle on ferme l'emballage. Là encore, des essais permettent de vérifier, en tenant compte de conditions d'introduction (en particulier pression, débit et température) et déterminer quel est celui de ces essais qui a conduit à la meilleure géométrie finale de l'emballage. Ceci permet de retenir une durée normale d'introduction, que l'on utilise lors de l'industrialisation du procédé.It is also possible to choose to introduce the gaseous fluid into the package for a determined period of time, after which the package is closed. Again, tests make it possible to check, taking into account the conditions of introduction (in particular pressure, flow and temperature) and determine which of these tests led to the best final geometry of the package. This makes it possible to retain a normal duration of introduction, which is used during industrialization of the process.
Claims (13)
- Method for heat treatment of a product, in particular a food product, contained in a pack such as a tray (1, 2) having at least one deformable wall (2), in which the product (3) contained in the pack is heated by taking it to a desired temperature, a temperature-holding stage is carried out, vapour produced by the heating being allowed to escape through an opening (4A, 5) of the pack (1, 2), characterized in that a gaseous fluid (F) is introduced into the pack at the end of this temperature-holding stage, and the pack is totally closed.
- Method according to claim 1, characterised in that the gaseous fluid introduced is at a temperature at least close to the temperature of the pack vapour during the temperature-holding stage.
- Method according to claim 2, characterised in that the temperature of the gaseous fluid introduced is between 80% and 130%, preferably between 90% and 110%, of the vapour temperature during the temperature-holding stage.
- Method according to any of claims 1 to 3, characterised in that a volume of gaseous fluid (F) is introduced, corresponding at least approximately to the volume of vapour (V) which escapes from the pack during heating and temperature holding.
- Method according to claim 4, characterised in that the volume of gaseous fluid introduced is determined in such a way that this volume is substantially equal to the said volume of vapour, preferably slightly lower than this volume, when the said volumes are adjusted to the same temperature.
- Method according to any of claims 1 to 3, characterised in that the gaseous fluid (F) is introduced into the pack (1, 2), causing deformation of the said deformable wall (2) and in that the pack is closed when it is found that the said deformation has reached a given level.
- Method according to any of claims 1 to 3, characterised in that the gaseous fluid is introduced into the pack for a predetermined length of time, at the end of which the pack is closed.
- Method according to any of claims 1 to 7, characterised in that the gaseous fluid (F) is a neutral gas.
- Method according to any of claims 1 to 7, characterised in that the gaseous fluid (F) is air, advantageously filtered.
- Method according to any of claims 1 to 9, characterised in that the gaseous fluid (F) is introduced through the said opening (4A) in the pack.
- Method according to any of claims 1 to 10, characterised in that the opening is formed by at least one interruption (4A) in a sealing strip (4) between two walls of the pack and in that, at the end of the stage of introducing the gaseous fluid into the pack, the latter is closed by completion of this welding strip (4, 4B).
- Method according to any of claims 1 to 10, characterised in that the opening is formed by at least one hole (5) in a pack wall and in that, at the end of the stage of introducing the gaseous fluid into the pack, this hole is closed by means of a cap (5').
- Method according to any of claims 1 to 12, characterised in that the pack is a tray made of plastic (1, 2), the top wall (2) of which is formed by a film sealed at the tray edge (1A).
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0503688A FR2884493B1 (en) | 2005-04-13 | 2005-04-13 | METHOD FOR THERMALLY PROCESSING A PRODUCT CONTAINED IN A PACKAGING SUCH AS A TRAY |
PCT/FR2006/050340 WO2006109000A1 (en) | 2005-04-13 | 2006-04-12 | Method for heat treating a product contained in a package such as a tray |
Publications (2)
Publication Number | Publication Date |
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EP1874632A1 EP1874632A1 (en) | 2008-01-09 |
EP1874632B1 true EP1874632B1 (en) | 2009-01-21 |
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Family Applications (1)
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---|---|---|---|
EP06743801A Not-in-force EP1874632B1 (en) | 2005-04-13 | 2006-04-12 | Method for heat treating a product contained in a package such as a tray |
Country Status (8)
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US (1) | US20100062126A1 (en) |
EP (1) | EP1874632B1 (en) |
AT (1) | ATE421460T1 (en) |
CA (1) | CA2611432C (en) |
DE (1) | DE602006004983D1 (en) |
ES (1) | ES2321556T3 (en) |
FR (1) | FR2884493B1 (en) |
WO (1) | WO2006109000A1 (en) |
Families Citing this family (3)
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FR2916185B1 (en) * | 2007-05-14 | 2012-01-13 | Mecaplastic | PROCESS FOR THERMALLY PROCESSING VACUUM PRODUCTS AND PACKAGING OBTAINED BY CARRYING OUT SAID METHOD |
IT201800005266A1 (en) * | 2018-05-11 | 2019-11-11 | METHOD TO CARRY OUT THE PASTEURIZATION TREATMENT OF FOOD PRODUCTS AND PLANT SUITABLE TO PERFORM THIS TREATMENT | |
CH716621A1 (en) * | 2019-09-20 | 2021-03-31 | Gigatherm Mikrowellen Ag | Process for preserving food in transport and sales packaging. |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
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US4667454A (en) * | 1982-01-05 | 1987-05-26 | American Can Company | Method of obtaining acceptable configuration of a plastic container after thermal food sterilization process |
US4590078A (en) * | 1983-06-09 | 1986-05-20 | Umina Anthony P | Process and apparatus for preparing canned baked products |
CH665605A5 (en) * | 1986-01-28 | 1988-05-31 | Christophe Aubert | METHOD FOR PACKAGING, WITH PASTEURIZATION, PERISHABLE FOOD PRODUCTS. |
DE3840104C1 (en) * | 1988-11-15 | 1990-05-31 | Klaus H. 1000 Berlin De Gleitz | |
US5234126A (en) * | 1991-01-04 | 1993-08-10 | Abbott Laboratories | Plastic container |
GB2252712B (en) * | 1991-02-13 | 1994-04-27 | United Biscuits Ltd | Improvements in and relating to preserving food products |
US5283033A (en) * | 1991-11-29 | 1994-02-01 | Advanced Retort Systems, Inc. | Process for sterilizing the contents of a sealed deformable package |
US5307985A (en) * | 1991-12-17 | 1994-05-03 | Societe De Constructions De Materiel Metallique Et Electrique | Container and process for its manufacture |
FR2698082B1 (en) * | 1992-11-13 | 1994-12-23 | Mat Metallique Elec Const | Gas tight container. |
US5457939A (en) * | 1993-09-01 | 1995-10-17 | Optimal Food Processing Research, Inc. | Process for vacuum-packaging foodstuffs in rigid containers |
FR2729366B3 (en) * | 1995-01-12 | 1997-03-21 | Carre Bleu Sa | PROCESS FOR SEALING A TRAY FOR FOOD PREPARATIONS AND CLOSED TRAY OBTAINED BY THE PROCESS |
SE9802212L (en) * | 1998-06-23 | 1999-09-20 | Joel Haamer | Method and apparatus for boiling and vacuum packing of microwaves with microwaves |
FR2813583B1 (en) * | 2000-09-01 | 2003-07-18 | Microondes Syst Sa | CONTAINER FOR HOMOGENEOUS HEATING OF ITS CONTENTS BY MICROWAVE |
-
2005
- 2005-04-13 FR FR0503688A patent/FR2884493B1/en not_active Expired - Fee Related
-
2006
- 2006-04-12 DE DE602006004983T patent/DE602006004983D1/en active Active
- 2006-04-12 EP EP06743801A patent/EP1874632B1/en not_active Not-in-force
- 2006-04-12 WO PCT/FR2006/050340 patent/WO2006109000A1/en active Application Filing
- 2006-04-12 US US11/911,482 patent/US20100062126A1/en not_active Abandoned
- 2006-04-12 ES ES06743801T patent/ES2321556T3/en active Active
- 2006-04-12 AT AT06743801T patent/ATE421460T1/en not_active IP Right Cessation
- 2006-04-12 CA CA2611432A patent/CA2611432C/en not_active Expired - Fee Related
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DE602006004983D1 (en) | 2009-03-12 |
FR2884493B1 (en) | 2007-08-24 |
CA2611432A1 (en) | 2006-10-19 |
FR2884493A1 (en) | 2006-10-20 |
CA2611432C (en) | 2011-07-26 |
ES2321556T3 (en) | 2009-06-08 |
ATE421460T1 (en) | 2009-02-15 |
US20100062126A1 (en) | 2010-03-11 |
WO2006109000A1 (en) | 2006-10-19 |
EP1874632A1 (en) | 2008-01-09 |
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